C04B2235/9615

Method for additive manufacturing of 3D-printed articles

The present invention provides a method of additive manufacturing a 3D-printed article, comprising: (a) printing and depositing one or more layers of a slurry by using a 3D printer, wherein the slurry comprises a ceramic powder composition; (b) further injecting an oil around the one or more layers of slurry, wherein the height of the injected oil is lower than the height of the slurry; (c) repeating steps (a) and (b) until a main body with desired geometric shape is obtained; and (d) sintering the main body by heating to obtain the 3D-printed article wherein the temperature of a printing carrier of the 3D printer is from 30 to 80° C.

MICROCHEMICAL SYSTEM APPARATUS AND RELATED METHODS OF FABRICATION
20210178387 · 2021-06-17 ·

The disclosure relates to microchemical (or microfluidic) apparatus as well as related methods for making the same. The methods generally include partial sintering of sintering powder (e.g., binderless or otherwise free-flowing sintering powder) that encloses a fugitive phase material having a shape corresponding to a desired cavity structure in the formed apparatus. Partial sintering removes the fugitive phase and produces a porous compact, which can then be machined if desired and then further fully sintered to form the final apparatus. The process can produce apparatus with small, controllable cavities shaped as desired for various microchemical or microfluidic unit operations, with a generally smooth interior cavity finish, and with materials (e.g., ceramics) able to withstand harsh environments for such unit operations.

CERAMIC SLURRIES WITH PHOTOREACTIVE-PHOTOSTABLE HYBRID BINDERS
20210269361 · 2021-09-02 ·

Ceramic slurries may include ceramic particles, a photoreactive-photostable hybrid binder, and a photoinitiator. The photoreactive-photostable hybrid binder may include a photoreactive organic resin component, a photoreactive siloxane component, and one or more photostable siloxane components. Methods of forming a ceramic part may include curing a portion of a ceramic slurry by exposing the portion of the ceramic slurry to light to form a green ceramic part, and partially firing the green ceramic part to form a brown ceramic part. The brown ceramic part may be sintered at or above a sintering temperature of the ceramic particles to form a ceramic part, wherein sintering includes heating the brown ceramic part to a sufficient temperature to promote reaction bonding that converts silica from the photoreactive-photostable hybrid binder into silicates that bond with the ceramic particles.

CERAMIC SLURRIES WITH PHOTOREACTIVE-PHOTOSTABLE HYBRID BINDERS
20210269362 · 2021-09-02 ·

Ceramic slurries may include ceramic particles, a photoreactive-photostable hybrid binder, and a photoinitiator. The photoreactive-photostable hybrid binder may include a photoreactive organic resin component, a photoreactive siloxane component, and one or more photostable siloxane components. Methods of forming a ceramic part may include curing a portion of a ceramic slurry by exposing the portion of the ceramic slurry to light to form a green ceramic part, and partially firing the green ceramic part to form a brown ceramic part. The brown ceramic part may be sintered at or above a sintering temperature of the ceramic particles to form a ceramic part, wherein sintering includes heating the brown ceramic part to a sufficient temperature to promote reaction bonding that converts silica from the photoreactive-photostable hybrid binder into silicates that bond with the ceramic particles.

THREE-DIMENSIONAL SHAPED ARTICLE PRODUCTION METHOD
20210154891 · 2021-05-27 ·

A three-dimensional shaped article production method for producing a three-dimensional shaped article by stacking layers to form a stacked body includes a constituent layer formation step of forming a constituent layer which corresponds to a constituent region of the three-dimensional shaped article, a support layer formation step of forming a support layer which is in contact with the constituent layer and supports the constituent layer, and a sintering step of sintering the constituent layer, wherein the support layer is configured such that as compared with the volume decrement accompanying the sintering step of a space surrounded by the constituent layer from at least two directions, the volume decrement accompanying the sintering step of the support layer which supports the constituent layer in the space is larger.

POLYCRYSTALLINE WAVEGUIDE

A waveguide includes a body of material having a width, a thickness, and a length, where the width is orthogonal to the thickness, and the length is orthogonal to the thickness and the width. The material includes polycrystalline ceramic that is transmissive such that the body is configured as a waveguide. The thickness is no more than 5 millimeters and at least 20 nanometers, the width is greater than or equal to the thickness, and the length is at least 100 times greater than the width. The body of material has a granular profile such that grains of the material protrude generally outward from a surface of the body with a height of at least 25 nanometers and no more than 100 micrometers relative to recessed portions of the surface of the body at boundaries between the grains.

BUILDING MATERIALS COMPRISING DIGESTATE
20210130238 · 2021-05-06 ·

The present invention relates to a process for producing building materials, such as bricks, lightweight aggregates and concrete, which building materials comprise digestate obtained from municipal solid waste (MSW) which has been added one or more enzymes to liquefy the organic fraction of MSW.

Corrosion-resistant member

A corrosion-resistant member may include alumina ceramics containing α-alumina and anorthite. The alumina ceramics may contain 0.4% by mass or more of Ca and Si in total in terms of CaO and SiO.sub.2, respectively, and a mass ratio of CaO/SiO.sub.2 may fall within a range of 0.5 to 2. Moreover, a ratio B/A of X-ray diffraction peak intensity B for (004) plane of the anorthite to X-ray diffraction peak intensity A for (104) plane of the α-alumina in a surface of the alumina ceramics, may be 0.01 or more.

CERAMIC POWDER, SINTERED BODY AND BATTERY
20210119251 · 2021-04-22 ·

This invention provides a ceramic powder capable of forming a sintered body having a high density and high ionic conductivity even at a sintering temperature lower than the temperature conventionally used, and provides a battery containing a sintered body of the ceramic powder as a constituent element. The above problem is solved by a ceramic powder containing a garnet-type oxide and compound 1, wherein the garnet-type oxide contains zirconium, lithium, and lanthanum, and compound 1 contains at least one metal element selected from the group consisting of lanthanum, lithium, zirconium, gallium, scandium, yttrium, cerium, aluminum, calcium, magnesium, barium, strontium, niobium, and tantalum.

Systems and method for four-dimensional printing of elastomer-derived ceramic structures by compressive buckling-induced method
11000991 · 2021-05-11 · ·

Systems and method of constructing a 4D-printed ceramic object, the method including extruding inks including particles and polymeric ceramic precursors through a nozzle to deposit the inks to form a first elastic structure and a second elastic structure, subjecting the first elastic structure to a tensile stress along at least one axis, attaching the second elastic structure to the first elastic structure, releasing the application of the tensile stress from the first elastic structure to allow the first elastic structure and second elastic structure to form a 4D-printed elastomeric object, and converting the 4D-printed elastomeric object into the 4D-printed ceramic object.