C07C255/08

Biobased carbon fibers and carbon black and methods of making the same
10899622 · 2021-01-26 · ·

Bio-based materials, e.g., epoxide starting material, a beta-lactone starting material and/or a beta-hydroxy amide starting material, may be used as feedstocks in processes for making and using acrylonitrile and acrylonitrile derivatives to produce, among other products, carbon fibers and carbon black.

METHOD FOR PURIFYING NITRILE SOLVENT

A method for manufacturing a higher purity nitrile solvent by purifying a nitrile solvent containing an impurity, e.g an imine. The nitrile solvent may contain an imine and a conjugated diene, a carbonyl compound, or a high-boiling material as impurities. A method for purifying a nitrile solvent, such as isobutyronitrile, including bringing nitrile solvent containing an imine, e.g., as an impurity, into contact with an acidic aqueous solution having a pH of 3 or less, such as hydrochloric acid; bringing the nitrile solvent having been contacted with acidic aqueous solution into contact with an aqueous sodium hydrogen sulfite solution; bringing the nitrile solvent having been contacted with the aqueous sodium hydrogen sulfite solution into contact with an alkaline aqueous solution, such as an aqueous sodium hydroxide solution; and distilling the nitrile solvent having been contacted with the alkaline aqueous solution.

FLUID DISTRIBUTOR, REACTION DEVICE AND APPLICATION THEREOF
20200368707 · 2020-11-26 ·

A fluid distributor includes one or more fluid transport main pipe. The fluid transport main pipe is configured to assume a closed shape when its centerlines and/or centerline extensions are joined end-to-end. Each of the fluid transport main pipe has at least one fluid inlet and is connected with a plurality of fluid transport branch pipes. Each of the fluid transport branch pipes has a plurality of open pores disposed along the length of the fluid transport branch pipe and a connection portion. The connection portion is configured to connect the fluid transport branch pipe to the housing after the fluid transport branch pipe passes through the housing of the vessel into the inner cavity.

FLUID DISTRIBUTOR, REACTION DEVICE AND APPLICATION THEREOF
20200368707 · 2020-11-26 ·

A fluid distributor includes one or more fluid transport main pipe. The fluid transport main pipe is configured to assume a closed shape when its centerlines and/or centerline extensions are joined end-to-end. Each of the fluid transport main pipe has at least one fluid inlet and is connected with a plurality of fluid transport branch pipes. Each of the fluid transport branch pipes has a plurality of open pores disposed along the length of the fluid transport branch pipe and a connection portion. The connection portion is configured to connect the fluid transport branch pipe to the housing after the fluid transport branch pipe passes through the housing of the vessel into the inner cavity.

Using a biased electrochemical sensor for acrylonitrile detection
10816502 · 2020-10-27 · ·

An electrochemical acrylonitrile sensor comprises a housing, an electrolyte disposed within the housing, and a plurality of electrodes in contact with the electrolyte within the housing. The plurality of electrodes comprises a working electrode and a counter electrode. The electrodes comprise a catalytic material, which may comprise gold. A potential is applied between the counter electrode and the working electrode.

Method for producing catalyst, and method for producing unsaturated nitrile
10807073 · 2020-10-20 · ·

The present invention provides a method for producing a catalyst to be used for a gas-phase catalytic ammoxidation reaction of propane, the method comprising a preparation step of dissolving or dispersing a raw material to thereby obtain a prepared raw material liquid, a first drying step of drying the prepared raw material liquid to thereby obtain a dried material, a calcination step of calcining the dried material to thereby obtain a composite oxide having a predetermined composition, an impregnation step of impregnating the composite oxide with a solution containing at least one specific element selected from the group consisting of tungsten, molybdenum, tellurium, niobium, vanadium, boron, bismuth, manganese, iron, antimony, phosphorus and rare earth elements to thereby obtain an impregnated composite oxide, and a second drying step of drying the impregnated composite oxide, wherein at least one of the impregnation step o and the second drying step is a step of impregnating the composite oxide or drying the impregnated composite oxide while stirring by a specific stirring power.

Method for producing catalyst, and method for producing unsaturated nitrile
10807073 · 2020-10-20 · ·

The present invention provides a method for producing a catalyst to be used for a gas-phase catalytic ammoxidation reaction of propane, the method comprising a preparation step of dissolving or dispersing a raw material to thereby obtain a prepared raw material liquid, a first drying step of drying the prepared raw material liquid to thereby obtain a dried material, a calcination step of calcining the dried material to thereby obtain a composite oxide having a predetermined composition, an impregnation step of impregnating the composite oxide with a solution containing at least one specific element selected from the group consisting of tungsten, molybdenum, tellurium, niobium, vanadium, boron, bismuth, manganese, iron, antimony, phosphorus and rare earth elements to thereby obtain an impregnated composite oxide, and a second drying step of drying the impregnated composite oxide, wherein at least one of the impregnation step o and the second drying step is a step of impregnating the composite oxide or drying the impregnated composite oxide while stirring by a specific stirring power.

Method for separating materials by means of an extractive distillation process
10793494 · 2020-10-06 · ·

A method for separating a mixture of materials A and B by extractive distillation, using an extraction medium having a higher affinity to B than to A, collecting a liquid fraction on a collecting tray and heated and partially evaporated in a first indirect heat exchanger, collecting the resultant vapor is released into the column and a non-evaporated proportion of the liquid fraction in the sump of the column, and a series of heating, separation and cooling where partially cooled extraction medium fraction is used as heating medium for a heat exchanger.

Method for separating materials by means of an extractive distillation process
10793494 · 2020-10-06 · ·

A method for separating a mixture of materials A and B by extractive distillation, using an extraction medium having a higher affinity to B than to A, collecting a liquid fraction on a collecting tray and heated and partially evaporated in a first indirect heat exchanger, collecting the resultant vapor is released into the column and a non-evaporated proportion of the liquid fraction in the sump of the column, and a series of heating, separation and cooling where partially cooled extraction medium fraction is used as heating medium for a heat exchanger.

Method for producing oxide catalyst and method for producing unsaturated nitrile

A method for producing an oxide catalyst containing Mo, V, Sb, and Nb, the method including: a raw material preparation step including sub-step (I) of preparing an aqueous mixed liquid (A) containing Mo, V, and Sb, sub-step (II) of adding hydrogen peroxide to the aqueous mixed liquid (A), thereby facilitating oxidation of the aqueous mixed liquid (A) and obtaining an aqueous mixed liquid (A), and sub-step (III) of mixing the aqueous mixed liquid (A) and a Nb raw material liquid (B), thereby obtaining an aqueous mixed liquid (C); a drying step of drying the aqueous mixed liquid (C), thereby obtaining a dried powder; and a calcination step of calcining the dried powder under an inert gas atmosphere, wherein a time elapsed from addition of the hydrogen peroxide to the aqueous mixed liquid (A) to mixing the Nb raw material liquid (B) therewith is less than 5 minutes and the aqueous mixed liquid (A) before being subjected to the sub-step (III) has an oxidation-reduction potential of 150 to 350 mV.