C08J3/092

METHOD OF MAKING A GREASE THICKENER AND THE THICKENER MADE BY THE METHOD

A continuous process for producing a polyurea concentrate or powder. The process includes combing at least one amine and an isocayante in the presence of a liquid diluent or a base oil in a rotor stator mixer. The concentrate comprises a polyurea in a base oil wherein the concentration of from about 20 weight percent to about 50, or 40 or 35 or 30 weight percent of polyurea based on total weight of grease thickener. The powder has particle size of 2 to 400 microns. This concentrate or powder can then be formulated by grease manufacturers to the desired final properties without the need for handling of the isocyanate and amine raw materials.

Inverse emulsion thickeners

An inverse emulsion copolymer composition comprises (A) an aqueous phase comprising a cross-linked hydrophilic polyelectrolyte copolymer (A′) obtained by the free radical copolymerisation of: (i) at least one anionic ethylenically unsaturated monomer bearing a negatively charged group and one polymerisable C═C double bond, or at least one cationic ethylenically unsaturated monomer bearing a positively charged group and one polymerisable C═C double bond, and (ii) at least one non-ionic ethylenically unsaturated cross-linking monomer bearing at least two polymerisable C═C double bonds, and (iii) optionally, one or more hydrophilic non-ionic ethylenically unsaturated monomers bearing one polymerisable C═C double bond, (B) an oil phase comprising a carrier oil (C), (D) (i) at least one water-in-oil emulsifying surfactant, and (D) (ii) at least one oil-in-water emulsifying surfactant; characterised in that the carrier oil component (C) of the oil phase comprises from 75% to 100%, by weight of the said carrier oil component (C), of farnesane (2, 6, 10-trimethyldodecane). The compositions are effective for use as thickeners for thickening aqueous solutions, including solutions which contain dissolved salts. The compositions also show excellent thickening in acidic solutions than counterpart compositions containing paraffinic oils.

BIODEGRADABLE POLYMER FINE PARTICLE FOR FILLER, MANUFACTURING METHOD THEREOF, FREEZE-DRIED BODY INCLUDING THE SAME, AND FILLER INJECTION INCLUDING THE SAME

Disclosed herein are a biodegradable polymer microparticle for a filler comprising a core and a shell, wherein the core contains secondary particles including aggregates of a plurality of primary particles, the shell has a raspberry shaped structure, an average particle diameter (D.sub.50) of the biodegradable polymer microparticle ranges from 20 to 200 μm, a manufacturing method thereof, a freeze-dried body including the same, and filler injection including the same.

Method of making a grease thickener and the thickener made by the method

A continuous process for producing a polyurea concentrate or powder. The process includes combing at least one amine and an isocyanate in the presence of a liquid diluent or a base oil in a rotor stator mixer. The concentrate comprises a polyurea in a base oil wherein the concentration of from about 20 weight percent to about 50, or 40 or 35 or 30 weight percent of polyurea based on total weight of grease thickener. The powder has particle size of 2 to 400 microns. This concentrate or powder can then be formulated by grease manufacturers to the desired final properties without the need for handling of the isocyanate and amine raw materials.

Green fabrication of polytetrafluoroethylene and expanded polytetrafluoroethylene and uses thereof

Green, fast and easy evaporating organic solvent for use as a lubricant in the processing of polytetrafluoroethylene (PTFE) and expanded polytetrafluoroethylene (ePTFE) products and processes of using the solvents to fabricate the products are disclosed herein. The products can be used in the field of bio- and medical applications, such as for use in vascular grafts, cardiovascular and soft tissue patches, facial implants, surgical sutures, and endovascular prosthesis, and for any products known in the aerospace, electronics, fabrics, filtration, industrial and sealant arts.

Composition based on at least one biodegradable polymer and use thereof as a binder for coating products

A composition including at least one polyhydroxyalkanoate (PHA) having saturated side chains dissolved in at least one aromatic solvent between 50 g/1 and 200 g/l and preferably between 80 g/l and 180 g/l. The at least one PHA has a weight-average molecular weight (M.sub.w) not greater than 250,000 Da and preferably not greater than 150,000 Da. This composition is particularly suitable as a binder for coating products. The composition can be produced by mixing the PHA with the aromatic organic solvent and heating the mixture at a temperature close to the PHA melting temperature, maintaining the mixture under stirring until complete dissolution of the polymer. Alternatively, the composition can be produced by dissolution of the PHA in a non-aromatic organic solvent having low boiling temperature where the PHA is highly soluble, subsequent addition of the aromatic organic solvent and subsequent removal of the non-aromatic organic solvent by fractional distillation.

EMULSION COMPOSITION AND METHOD FOR PRODUCING SAME

Provided are an emulsion composition which can be produced more easily than a conventional method and has excellent emulsion stability, and a method for producing the same. The emulsion composition contains a liquid conjugated diene rubber, a diluent having a vapor pressure at 20° C. of 10 Pa or less, a surfactant, and water.

Emulsion of nitrogen atom-containing polymer or salt thereof, production method therefor, and production method for particles

An emulsion of a nitrogen atom-containing polymer or salt thereof and a method for producing it are provided. The emulsion has high stability and low dispersity of the particle diameter of emulsified particles. A method for producing particles including a crosslinked nitrogen atom-containing polymer or sat thereof using the emulsion is also provided. The method for producing the emulsion includes a step of mixing a first solution that includes a nitrogen atom-containing polymer or salt thereof and a hydrophilic solvent and has a viscosity of 10 to 2,000 mPa.Math.s, and a second solution that includes a hydrophobic solvent and has a viscosity of 1 to 100 mPa.Math.s, stirring the mixture, and thus obtaining an emulsion of the nitrogen atom-containing polymer or salt thereof, wherein a ratio between the viscosity of the first and second solutions is in a range of 0.1:1 to 300:1.

Green fabrication of polytetrafluoroethylene and expanded polytetrafluoroethylene and uses thereof

Green, fast and easy evaporating organic solvent for use as a lubricant in the processing of polytetrafluoroethylene (PTFE) and expanded polytetrafluoroethylene (ePTFE) products and processes of using the solvents to fabricate the products are disclosed herein. The products can be used in the field of bio- and medical applications, such as for use in vascular grafts, cardiovascular and soft tissue patches, facial implants, surgical sutures, and endovascular prosthesis, and for any products known in the aerospace, electronics, fabrics, filtration, industrial and sealant arts.

Method of producing composite resin material and method of producing shaped product
11161946 · 2021-11-02 · ·

Provided is a method of producing a composite resin material that has excellent shapeability and enables supply of a shaped product having good properties. The method of producing a composite resin material includes: a mixing step of mixing a fluororesin, fibrous carbon nanostructures, and a dispersion medium to obtain a slurry; and a formation step of removing the dispersion medium from the slurry and forming a particulate composite resin material. The particulate composite resin material has a D50 diameter of at least 20 μm and not more than 500 μm and a D90 diameter/D10 diameter value of at least 1.2 and not more than 15. The D10 diameter, D50 diameter, and D90 diameter are particle diameters respectively corresponding to cumulative volumes of 10%, 50%, and 90% calculated from a small particle end of a particle diameter distribution of the particulate composite resin material.