The present invention relates to a method of manufacturing a metal-polymer resin bonded body, including: degreasing metal using a degreasing solution; etching the metal using an etching solution; electrolyzing the metal using an electrolyte solution; and performing a polymer resin injection to bond a polymer resin to the metal, wherein the electrolyte solution includes a compound containing distilled water, oxalic acid, sulfuric acid, and carboxylic acid.

The present invention relates to a method of manufacturing a metal-polymer resin bonded body, including: degreasing metal using a degreasing solution; etching the metal using an etching solution; electrolyzing the metal using an electrolyte solution; and performing a polymer resin injection to bond a polymer resin to the metal, wherein the electrolyte solution includes a compound containing distilled water, oxalic acid, sulfuric acid, and carboxylic acid.

An object of the present invention is to enhance the thermal efficiency of an engine, to provide a film having low thermal conductivity and low heat capacity and being free from separation, drop-off and the like and excellent in durability and reliability. According to the present invention, an engine combustion chamber structure, wherein an anodic oxide film having a thickness of from more than 20 μm to 500 μm and a porosity of 20% or more is formed on the inner surface of the engine combustion chamber, and a manufacturing method thereof are provided.

An object of the present invention is to enhance the thermal efficiency of an engine, to provide a film having low thermal conductivity and low heat capacity and being free from separation, drop-off and the like and excellent in durability and reliability. According to the present invention, an engine combustion chamber structure, wherein an anodic oxide film having a thickness of from more than 20 μm to 500 μm and a porosity of 20% or more is formed on the inner surface of the engine combustion chamber, and a manufacturing method thereof are provided.

The invention relates to a vacuum chamber element obtained by machining and surface treatment of a plate of thickness at least equal to 10 mm made of aluminium alloy composed as follows (as percentages by weight), Si: 0.4-0.7, Mg: 0.4-1.0; the Mg/Si ratio as a percentage by weight being less than 1.8; Ti: 0.01-0.15, Fe 0.08-0.25; Cu <0.35; Mn <0.4; Cr: <0.25; Zn <0.04; other elements <0.05 each and <0.15 in total, the rest aluminium, characterized in that the grain size of said plate is such that the mean linear intercept length , measured in plane L/TC according to standard ASTM E112, is at least equal to 350 μm between surface and ½ thickness. The invention also relates to the method of manufacturing of such a vacuum chamber element. The products according to the invention are particularly advantageous, particularly in terms of resistance to creep deformation at high temperature, while having high properties of corrosion resistance, homogeneity of properties in thickness and machinability.

The invention relates to a vacuum chamber element obtained by machining and surface treatment of a plate of thickness at least equal to 10 mm made of aluminium alloy composed as follows (as percentages by weight), Si: 0.4-0.7, Mg: 0.4-1.0; the Mg/Si ratio as a percentage by weight being less than 1.8; Ti: 0.01-0.15, Fe 0.08-0.25; Cu <0.35; Mn <0.4; Cr: <0.25; Zn <0.04; other elements <0.05 each and <0.15 in total, the rest aluminium, characterized in that the grain size of said plate is such that the mean linear intercept length , measured in plane L/TC according to standard ASTM E112, is at least equal to 350 μm between surface and ½ thickness. The invention also relates to the method of manufacturing of such a vacuum chamber element. The products according to the invention are particularly advantageous, particularly in terms of resistance to creep deformation at high temperature, while having high properties of corrosion resistance, homogeneity of properties in thickness and machinability.

An aluminum member includes: a substrate formed of aluminum or an aluminum alloy that contains 0 to 10% by mass of magnesium, 0.1% by mass or less of iron, and 0.1% by mass or less of silicon and a balance of which is aluminum and unavoidable impurities; and an anodic oxide coating formed on a surface of the substrate. A surface of the substrate on the anodic oxide coating side has an arithmetical mean height Sa of 0.1 to 0.5 μm, a maximum height Sz of 0.2 to 5 μm, and an mean width of roughness profile elements Rsm of 0.5 to 10 μm, where the arithmetical mean height Sa, the maximum height Sz, and the mean width of roughness profile elements Rsm are measured after the anodic oxide coating is removed.

An aluminum member includes: a substrate formed of aluminum or an aluminum alloy that contains 0 to 10% by mass of magnesium, 0.1% by mass or less of iron, and 0.1% by mass or less of silicon and a balance of which is aluminum and unavoidable impurities; and an anodic oxide coating formed on a surface of the substrate. A surface of the substrate on the anodic oxide coating side has an arithmetical mean height Sa of 0.1 to 0.5 μm, a maximum height Sz of 0.2 to 5 μm, and an mean width of roughness profile elements Rsm of 0.5 to 10 μm, where the arithmetical mean height Sa, the maximum height Sz, and the mean width of roughness profile elements Rsm are measured after the anodic oxide coating is removed.

A method of forming a micro-structure involves forming a multi-layered structure including i) an oxidizable material layer on a substrate and ii) another oxidizable material layer on the oxidizable material layer. The oxidizable material layer is formed of an oxidizable material having an expansion coefficient, during oxidation, that is more than 1. The method further involves forming a template, including a plurality of pores, from the other oxidizable material layer, and growing a nano-pillar inside each pore. The nano-pillar has a predefined length that terminates at an end. A portion of the template is selectively removed to form a substantially even plane that is oriented in a position opposed to the substrate. A material is deposited on at least a portion of the plane to form a film layer thereon, and the remaining portion of the template is selectively removed to expose the nano-pillars.

A method of forming a micro-structure involves forming a multi-layered structure including i) an oxidizable material layer on a substrate and ii) another oxidizable material layer on the oxidizable material layer. The oxidizable material layer is formed of an oxidizable material having an expansion coefficient, during oxidation, that is more than 1. The method further involves forming a template, including a plurality of pores, from the other oxidizable material layer, and growing a nano-pillar inside each pore. The nano-pillar has a predefined length that terminates at an end. A portion of the template is selectively removed to form a substantially even plane that is oriented in a position opposed to the substrate. A material is deposited on at least a portion of the plane to form a film layer thereon, and the remaining portion of the template is selectively removed to expose the nano-pillars.