C03B37/01228

METHOD OF MANUFACTURING OPTICAL FIBER PREFORM AND OPTICAL FIBER PREFORM

The present invention relates to a method of manufacturing an optical fiber preform for obtaining an optical fiber with low transmission loss. A core preform included in the optical fiber preform comprises three or more core portions, which are each produced by a rod-in-collapse method, and in which both their alkali metal element concentration and chlorine concentration are independently controlled. In two or more manufacturing steps of the manufacturing steps for each of the three or more core portions, an alkali metal element is added. As a result, the mean alkali metal element concentration in the whole core preform is controlled to 7 atomic ppm or more and 70 atomic ppm or less.

MANUFACTURING METHOD OF OPTICAL FIBER PREFORM
20190248695 · 2019-08-15 · ·

A manufacturing method of an optical fiber preform used to produce an optical fiber includes: etching a surface of a core preform that forms a core of the optical fiber with a plasma flame in a chamber; obtaining a porous preform by depositing glass particles on an etched surface of the core preform to form an outside vapor-deposited layer that forms a cladding of the optical fiber in a state where the core preform is put into the chamber; and heating and sintering the porous preform. When obtaining the porous preform, the outside vapor-deposited layer is formed by repeatedly performing the deposition of the glass particles multiple times through supply of source material gas. In a first deposition among the multiple times of deposition of the glass particles, a flow rate of the source material gas is less than or equal to 50% of a stable value.

Method for forming a glass preform

A method of forming a glass preform of predetermined length comprises providing a length of glass material to be separated to form a preform length and a remaining length; forming a notch in the glass material; inducing a tensile stress in excess of the tensile strength of the glass in an area adjacent to the notch; and separating the preform length from the remaining length at the notch.

Optical fibers and production methods therefor

An optical fiber, manufacturing intermediate for forming an optical fiber and a method for forming an optical fiber. The method includes providing a manufacturing intermediate having an elongate body and having an aperture extending through the elongate body along an axial dimension of the elongate body, a boundary of the aperture defining an internal surface of the manufacturing intermediate. The method further includes etching the internal surface of the manufacturing intermediate using an etching substance, and drawing the manufacturing intermediate along the axial dimension so as to form the optical fiber.

Micro-nozzle array

The invention relates to a micro-nozzle array comprising a plurality of capillaries comprising a first silica-based material and a second silica-based material substantially surrounding the first silica-based material of the plurality of capillaries, and a plurality of nozzles extending beyond a face of the micro-nozzle array, each nozzle corresponding to a single capillary, wherein each nozzle comprises the first silica-based material. The micro-nozzle array may be used in hydrodynamic or electro-osmotic applications. In one embodiment the micro-nozzle array is a multiple electrospray emitter. The invention also relates to methods for preparing and using micro-nozzle arrays.

PREPARATION AND POST-TREATMENT OF A QUARTZ GLASS BODY

One aspect relates to a process for preparing a quartz glass body, including providing a silicon dioxide granulate, making a glass melt from the silicon dioxide granulate in a melting crucible, making a quartz glass body from at least a part of the glass melt, and treating the quartz glass body with at least one procedure selected from the group consisting of chemical, thermal or mechanical treatment to obtain a treated quartz glass body. One aspect also relates to a quartz glass body which is obtainable by this process. One aspect also concerns a light guide, an illuminant and a formed body each obtainable by processing the quartz glass body further.

NEUTRALIZING GAS SYSTEM FOR FURNACE

A method of preparing an optical preform, comprises the steps of: positioning an optical preform comprising silica within a cavity of a furnace; passing an etchant gas into the furnace and at least one of through an open channel defined in the optical preform and around the optical preform; and passing a neutralizing gas into the cavity of the furnace, the neutralizing gas configured to neutralize the etchant gas.

Quartz glass tube as a semi-finished product for an optical component

A quartz glass tube as a semi-finished product for an optical component that has an inner bore extending along a tube center axis for the acceptance of a core rod and a tube wall limited by an inner casing surface and an outer casing surface is already known; within said tube wall an inner region made of a first quartz glass and an outer region made of a second quartz glass with a different index of refraction surrounding the inner region contact one another at a contact surface which runs around the center axis. In order to provide a quartz glass on this basis that facilitates the production of optical components for special applications such as laser-activated optical components in wand or fiber form, the invention states that the contact surface has a non-round course in the radial cross-section and the inner casing surface has a circular course.

OPTICAL FIBER PREFORM

An optical fiber preform includes a silica-glass core portion, and a cladding portion surrounding the core portion, the cladding portion being composed of a fluorine-containing silica glass having a lower refractive index than the core portion, the core portion including a first region that does not include the central axis thereof, the first region containing a first dopant selected from sodium, potassium, and compounds thereof, and a second region that includes the central axis, the second region containing a second dopant that reduces the viscosity of the silica glass, the second dopant having a diffusion coefficient of 110.sup.12 cm.sup.2/s or more and less than the first dopant at 2,000 C. to 2,300 C., in which the entire core portion has an average first dopant concentration of 10 atomic ppm or more and 2,000 atomic ppm or less and an average second dopant concentration of 10 atomic ppm or more.

Tubular semifinished product for producing an optical fiber

Methods for producing an optical fiber by elongating a silica glass blank or a coaxial group of silica glass components, on the basis of which a fiber is obtained that comprises a core zone, an inner jacket zone enclosing the core zone and a ring zone surrounding the inner jacket zone, are known. In order to provide, proceeding from this, a method, a tubular semi-finished product and a group of coaxial components for the cost-effective production of an optical fiber, which is characterized by a high quality of the boundary between the core and jacket and by low bending sensitivity, according to the invention, the silica glass of the ring zone is provided in the form of a ring zone tube made of silica glass having a mean fluorine content of at least 6000 weight ppm and the tube has an inner tube surface and an outer tube surface, wherein via the wall of the ring zone tube, a radial fluorine concentration profile is adjusted which has an inner fluorine depletion layer with a layer thickness of at least 1 m and no more than 10 m, in which the fluorine content decreases toward the inner tube surface and is no more than 3000 weight ppm in a region close to the surface which has a thickness of 1 m.