C04B35/58071

METHOD FOR MANUFACTURING A REFRACTORY PART MADE OF COMPOSITE MATERIAL

A method of fabricating a part out of composite material, includes forming a fiber texture from refractory fibers; placing the texture in a mold having an impregnation chamber including in its bottom portion a part made of porous material, the impregnation chamber being closed in its top portion by a deformable impermeable diaphragm separating the impregnation chamber from a compacting chamber; injecting a slip containing a powder of refractory particles into the impregnation chamber; injecting a compression fluid into the compacting chamber, to force the slip to pass through the texture; draining the liquid of the slip via the porous material part, while retaining the powder of refractory particles inside the texture so as to obtain a fiber preform filled with refractory particles; drying the fiber preform; unmolding the preform; and sintering the refractory particles present in the preform in order to form a refractory matrix in the preform.

ABLATION-RESISTANT HIGH-ENTROPY CARBIDE-HIGH-ENTROPY DIBORIDE-SILICON CARBIDE MULTIPHASE CERAMIC AND PREPARATION THEREOF
20230167029 · 2023-06-01 ·

diboride-silicon carbide (SiC) multiphase ceramic, including: (S1) mixing a transition metal oxide mixed powder, nano carbon black and a silicon hexaboride (SiB.sub.6) powder to obtain a precursor powder; and (S2) subjecting the precursor powder to pressureless sintering to obtain the high-entropy carbide-high-entropy diboride-SiC multiphase ceramic with a relative density of 96% or more.

Method for injecting a loaded slurry into a fibrous texture

A method for manufacturing a part made of composite material includes injecting into a fibrous texture a slurry including at least one powder of refractory ceramic particles suspended in a liquid phase, filtering the liquid phase of the slurry and retaining the powder of refractory ceramic particles inside the texture so as to obtain a fibrous preform loaded with refractory ceramic particles, densifying the fibrous texture by treatment of the refractory ceramic particles present in the fibrous texture in order to form a refractory matrix in the texture. The method further includes, before injecting the slurry under pressure, pre-saturating the fibrous texture with a carrier fluid consisting in injecting into said texture a carrier fluid.

COMPOSITES WITH ONE OR MULTIPLE PRINCIPAL STRENGTHENING COMPOUNDS AND AT LEAST ONE PRINCIPAL CEMENTED REFRACTORY METAL
20170217839 · 2017-08-03 ·

A composite composed of one or a plurality of principal strengthening compounds and at least one principal cemented refractory metal that is prepared by combining a suitable binary to senary borides and/or carbides with a unitary to binary principal refractory metal is disclosed. As compared with the conventional sintered cemented carbides, the composite of the disclosure not only possess high hardness and high toughness but also has various ratios of principal components since it is not prepared with equal mole during the process.

Green ceramic tapes and method for their fabrication
09718993 · 2017-08-01 · ·

“Green”, ceramic tapes intended as building blocks for making complex, fully ceramic components and devices for electronic-, lab-on-chip-, and sensing applications, the manufacture of which comprises in sequence: I. mixing of a ceramic “green” paste, II. homogenisation of a ceramic “green” paste, III. dimensioning and optionally structuring the ceramic “green” paste, IV. drying of the dimensioned and structured ceramic paste, in which: step iii) is performed in a combination of an extruder and a calender, the extruder being provided with a circular extrusion die, splitting and unfolding the extruded tube to a flat, continuous tape strip, using methylcellulose or derivatives thereof as binder, and, an additional step chosen among cutting and punching the thus dimensioned and optionally structured “green” paste, thereby making thick, “green” tapes. A method for its manufacture is also contemplated.

Metal detectible ceramic material and method for making the same
09815743 · 2017-11-14 ·

A method for producing a cermet composition, including mixing a first predetermined amount of a yttria stabilized zirconia powder with between 2 and 8 weight percent mu-metal powder to define a homogeneous admixture, oxidizing the mu-metal in the admixture, forming the homogeneous admixture into a green body, calcining the green body in a first reducing atmosphere to remove oxygen from the oxidized mu-metal to yield a calcined body, and sintering the calcined body in a second reducing atmosphere to yield a densified body having no more than 0.8% porosity. The densified body has a plurality of mu-metal particles distributed therethrough, a hardness of at least 1450 HV, flexural strength of at least 200 kPSI, and a relative permeability μ/μ.sub.o of at least 850.

METHOD FOR MANUFACTURING A PART MADE OF COMPOSITE MATERIAL WITH COMPLIANCE CONTROL
20210387921 · 2021-12-16 ·

Method for manufacturing a composite material part includes injecting a slurry containing a refractory ceramic particle powder into a fibrous texture, draining the liquid from the slurry that passed through the fibrous texture and retaining the refractory ceramic particle powder inside said texture so as to obtain a fibrous preform loaded with refractory ceramic particles, and demoulding of the fibrous preform. The method includes, after demoulding the fibrous preform, checking the compliance of the demoulded fibrous preform. If the preform is noncompliant, the method also includes, before a sintering, immersing the demoulded fibrous preform in a bath of a liquid suitable for decompacting the refractory ceramic particles present in the fibrous preform, and additionally injecting a slurry containing a refractory ceramic particle powder into the fibrous preform present in the mould cavity.

ELECTRO-CONDUCTIVE B4C-TiB2 COMPOSITE CERAMIC AND PREPARATION METHOD THEREOF
20230271886 · 2023-08-31 ·

An electro-conductive B.sub.4C—TiB.sub.2 has a microstructure in which large B.sub.4C grains are coated by small TiB.sub.2 grains. The composite ceramic includes 10˜30% by volume of TiB.sub.2. A method for preparing the electro-conductive B.sub.4C—TiB.sub.2 composite ceramic includes: (1) weighing B.sub.4C, TiC, and amorphous B powder; (2) mixing evenly and drying thoroughly the powders; and (3) loading the mixed powder into a graphite mold; and placing the graphite mold in a spark plasma sintering furnace for sintering under vacuum, where the sintering is performed at 2000° C. and 50 MPa for 5˜20 min.

Shaping method and shaping device

An object shaping method includes a step of forming a powder layer using first powder, a step of placing second powder having an average particle diameter smaller than an average particle diameter of the first powder at a part of a region of the powder layer, and a first heating step of heating the powder layer in which the second powder is placed. The average particle diameter is equal to or larger than 1 nm and equal to or smaller than 500 nm, and the first heating step performs heating the powder layer at a temperature at which particles contained in the second powder are sintered or melted.

Diamond composites by lithography-based manufacturing

A lithography based method for the manufacture of diamond composite materials in which green bodies are prepared by a layer-by-layer construction with resulting green bodies de-bound and sintered to achieve a dense high hardness material.