Patent classifications
C04B35/62615
SPINEL-REINFORCED MAGNESIUM OXIDE-BASED FOAM CERAMIC FILTER AND PREPARATION METHOD THEREFOR
A spinel-reinforced magnesium oxide-based foam ceramic filter that is obtained by by coating onto a polyurethane foam carrier a slurry of light calcined magnesium oxide-based ceramic comprising a nanometer lanthanum oxide sintering aid, and then drying and sintering. A method for preparing the foam ceramic filter comprising: 1) preparing a ceramic slurry having a solid content of 60%-70% by dosing 15%-25% by mass of a nanometer alumina sol, 0.8%-1.5% by mass of a rheological agent, and the balance magnesium oxide ceramic powder comprising a nanometer lanthanum oxide sintering aid, and then adding absolute ethanol and ball milling to mix until uniform; 2) soaking a polyurethane foam template into the ceramic slurry, squeezing by a roller press the polyurethane foam template to remove redundant slurry therein to make a biscuit, and then removing the ethanol solvent in a ventilation chamber at a temperature of 40 C.-50 C. to dry the biscuit; 3) putting the dried biscuit into a sintering furnace, elevating the temperature to 1350 C.-1550 C. and performing a high temperature sintering, cooling to the room temperature with the furnace to obtain the magnesium oxide-based ceramic foam filter.
Proton conductor and membrane electrode assembly
A proton conductor of the present disclosure has a composition formula of Ba.sub.aZr.sub.1-x-yYb.sub.xNi.sub.yO.sub.3- (0.95a1.05, 0.1x0.4, and 0.15y0.30).
Method For Manufacturing Spherical Ceramic-Glass Nanocomposite Dielectrics For Multilayer Ceramic Capacitor Applications
Spherical ceramic-glass nanocomposite dielectrics made from ceramics and glasses that are separately pre-milled by mechanical ball milling using selected ball-to-powder weight ratios and combined to form a mixture that is ball milled. A stable liquid suspension of the milled mixture including an added dispersant such as polyacrylic acid to improve uniformity is spray dried through a nozzle and recovered product is annealed. The novel dielectrics have a microstructure where ceramic primary particles are uniformly distributed and fully embedded in a glass matrix. The dielectrics have a mean particle size of about 1-20 um and a sphericity of about 0.8 or higher which are suitable for fabricating multilayer ceramic capacitors for high temperature applications. The novel dielectrics afford decreased sintering temperature, enhanced breakdown strength, lower dielectric lose tangent, and lower costs. Calcium titanate zirconate with manganese-doping-based or barium titanate-based dielectric ceramics and alkali-free borosilicate glass produce superior nanocomposite dielectrics.
HYDROGEN-SUBSTITUTED GARNET-TYPE OXIDE, MANUFACTURING METHOD OF SINTERED BODY AND MANUFACTURING METHOD OF HYDROGEN-SUBSTITUTED GARNET-TYPE OXIDE
There is provided a hydrogen-substituted garnet-type oxide containing at least Li, H, La and Zr and has an amount of hydrogen a (moll unit) per one unit of a garnet-type oxide in a range of 1.85.
ELECTROLYTE, BATTERY, ELECTRONIC APPARATUS, AND METHODS FOR PRODUCING ELECTROLYTE AND BATTERY
An electrolyte according to the present disclosure contains a lithium composite metal oxide represented by the following compositional formula.
Li.sub.7-xLa.sub.3(Zr.sub.2-xA.sub.x)O.sub.12-yF.sub.y
In the formula, 0.1x1.0, 0.0<y1.0, and A represents two or more types of Ta, Nb, and Sb.
ANGULAR CERAMIC PARTICLES AND METHODS OF MAKING AND USING SAME
The present disclosure provides processes for forming angular ceramic particles. In at least one embodiment, a process for forming angular ceramic particles includes providing a slurry having a ceramic raw material having alumina. The process includes atomizing the slurry into droplets and coating seeds comprising alumina with the droplets to form green pellets. The process includes sintering the preen pellets to form sintered pellets. The process includes breaking the sintered pellets to form the angular ceramic particles comprising a sintered ceramic material. The angular ceramic particles can have an abrasion loss that is less than that of angular ceramic particles formed by crushing the green pellets prior to sintering.
BORON ALUMINUM SILICATE MINERAL MATERIAL, LOW TEMPERATURE CO-FIRED CERAMIC COMPOSITE MATERIAL, LOW TEMPERATURE CO-FIRED CERAMIC, COMPOSITE SUBSTRATE AND PREPARATION METHODS THEREOF
The present invention relates to a boroaluminosilicate mineral material, a low temperature co-fired ceramic composite material, a low temperature co-fired ceramic, a composite substrate and preparation methods thereof. A boroaluminosilicate mineral material for a low temperature co-fired ceramic, the boroaluminosilicate mineral material comprises the following components expressed in mass percentages of the following oxides: 0.41%-1.15% of Na2O, 14.15%-23.67% of K2O, 1.17%-4.10% of CaO, 0-2.56% of Al2O3, 13.19%-20.00% of B.sub.2O.sub.3, and 53.47%-67.17% of SiO.sub.2. The aforementioned boroaluminosilicate mineral material is chemically stable; a low temperature co-fired ceramic prepared from it not only has excellent dielectric properties, but also has a low sintering temperature, a low thermal expansion coefficient, and high insulation resistance; it is also well-matched with the LTCC process and can be widely used in the field of LTCC package substrates.
PREPARATION METHOD OF NANOMETRIC SIZE METAL OXIDE ADDITIVES THAT REDUCE THE TEMPERATURE OF SINTERIZED AND/OR INCREASE PRODUCTIVITY IN THE MANUFACTURE OF CERAMIC PARTS, IMPROVING MECHANICAL PROPERTIES WITHOUT AFFECTING THE GRESIFICATION PROPERTIES OF CERAMIC BODIES, TILES OR COATINGS
The object of this invention is a process for manufacturing, conditioning and stabilization of a family of base additives sodium, potassium, boron, silicon, zinc, calcium oxides, among others, prepared by physicochemical and chemical synthesis methods that form nanometric structures, reformulated with deflocculant, sequestrants and dispersants additives that allow to obtain a dispersion or powder capable to decrease the sintering temperature of a ceramic body due to the high fluxing power, which is maximized by the use of nanotechnology in the structures obtained. The process consists in the preparation of nucleation seeds of metal, silicates and carbonates oxides by means of a physicochemical process, and which allow nanometric structures to grow by means of a chemical process in a chemical synthesis process wet basis of sodium, boron, silicon, zinc, potassium and calcium oxides. The combination of these oxides allows structuring elements of high fluxing power due to their high surface area and physicochemical composition. The additives prepared in this invention are chemically stabilized with deflocculating agents, which allow the additives to be incorporated into the aqueous medium grinding process of the ceramic body. Applications made with the additives of this invention allow the sintering temperature of a red body to be reduced from 1150 C. to 1000 C. and in porcelain bodies from 1180 C. to 1050 C., with the use of 0.2 to 5% of the additive, or increasing the speed of the heat treatment by up to 20%, and it can be used in the manufacture of bathroom fittings, molding parts, components for tooling, coatings, valances, enamels, vitrified pastes and other ceramic components. The present invention proposes several nanostructured additive formulations with high performance fluxing properties, which allow to optimize and standardize the sintering process and to improve the mechanical properties of the ceramic body. It also proposes different methods of application of the additive in ceramic formulations.
LIGHT-EMITTING CERAMIC AND WAVELENGTH CONVERSION DEVICE
A light-emitting ceramic that includes a pyrochlore type compound that contains 0.01 mol % or more of Bi with respect to 100 mol % of the general formula M1.sub.xM2.sub.yM3.sub.zO.sub.w, wherein M1 is at least one of La, Y, Gd, Yb, and Lu, M2 is at least one of Zr, Sn, and Hf, M3 is at least one of Ta, Nb, and Sb, X, Y, Z, and W are positive numbers that maintain electrical neutrality, X+Y+Z=2.0, 0.005Z0.2, and 3X+4Y+5Z is 7.02 or less.
METHOD OF PRODUCING POLYCRYSTALLINE Y-358 SUPERCONDUCTOR
A method of producing polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y (Y-358) whereby powders of yttrium (III) oxide, a barium (II) salt, and copper (II) oxide are pelletized, calcined at 850 to 950 C. for 8 to 16 hours, ball milled under controlled conditions, pelletized again and sintered in an oxygen atmosphere at 900 to 1000 C. for up to 72 hours. The polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y thus produced is in the form of elongated crystals having an average length of 2 to 10 m and an average width of 1 to 2 m, and embedded with spherical nanoparticles of yttrium deficient Y.sub.3Ba.sub.5Cu.sub.8O.sub.y having an average diameter of 5 to 20 nm. The spherical nanoparticles are present as agglomerates having flower-like morphology with an average particles size of 30 to 60 nm. The ball milled polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y prepared under controlled conditions shows significant enhancement of superconducting and flux pinning properties.