C04B2235/424

METHODS OF FORMING SiAlON IN CARBON/CARBON COMPOSITES
20230242454 · 2023-08-03 · ·

A method of making a carbon-carbon composite may comprise forming a Silicon-Aluminum-Oxygen-Nitrogen (SiAlON) precursor suspension and infiltrating a fibrous preform with the SiAlON precursor suspension. A SiAlON forming heating treatment may be performed on the fibrous preform to form SiAlON particles. The fibrous preform may be densified using chemical vapor infiltration to form a densified fibrous preform.

PROCESS FOR THE MANUFACTURE OF A FUSED BLOCK HAVING A HIGH ZIRCONIA CONTENT
20210363066 · 2021-11-25 ·

A process for the manufacture of a refractory block including more than 80% zirconia, in percentage by weight based on the oxides. The process includes the following successive stages: melting, under reducing conditions, of a charge including more than 50% zircon, in percentage by weight, such as to reduce the zircon and obtain a molten material, application of oxidizing conditions to the molten material, casting of the molten material, and cooling until at least partial solidification of the molten material in the form of a block. Also, the process can include heat treatment of the block.

Method for preparation of dense HfC(Si)—HfB.SUB.2 .composite ceramic

A method for the preparation of a dense HfC(Si)—HfB.sub.2 composite ceramic. hafnium oxide powders, nano-sized carbon black and silicon hexaboride powders are mixed in a molar ratio of (1-10):(1-20):(1-5) to obtain a powder mixture. The powder mixture is subjected to ball milling, dried and transferred to a graphite mold for spark plasma sintering. In this way, an in-situ carbon-boron reduction reaction and the sintering densification are completed in one step, and the obtained HfC(Si)—HfB.sub.2 composite ceramic has a density of 94.0%-100% and uniformly dispersed grains.

GRAPHENE MACRO-ASSEMBLY-FULLERENE COMPOSITE FOR ELECTRICAL ENERGY STORAGE

Disclosed here is a method for producing a graphene macro-assembly (GMA)-fullerene composite, comprising providing a mixture of graphene oxide and water, adding a hydroxylated fullerene to the mixture, and forming a gel of the hydroxylated fullerene and the mixture. Also described are a GMA-fullerene composite produced, an electrode comprising the GMA-fullerene composite, and a supercapacitor comprising the electrode.

Process for producing highly carbonaceous materials and the highly carbonaceous material obtained
11214523 · 2022-01-04 · ·

A process for the production of highly carbonaceous material, including combining a structured precursor including fibres and an unstructured precursor, in the form of a fluid, wherein the fluid has a viscosity of less than 45,000 mPa.Math.s.sup.−1 at the temperature at which the combination step occurs, and including at least a cyclic organic or aromatic compound in the molten state, or in solution at a concentration by weight of less than or equal to 65%, in order to obtain a combined precursor corresponding to the structured precursor covered by the unstructured precursor, wherein the process further includes step of thermal and dimensional stabilization of the combined precursor in order to obtain fibres covered with a cyclic organic or aromatic compound deposit, and a step of carbonization of the fibres covered with a cyclic organic or aromatic compound deposit in order to obtain a highly carbonaceous material.

A CORAL-LIKE COMPOSITE MATERIAL AND A METHOD OF PREPARING THE SAME
20230278868 · 2023-09-07 ·

There is provided a coral-like composite material comprising highly dispersed conductive metal nitride, metal carbide or metal carbonitride nanoparticles on mesoporous carbon nanosheets, and a method of preparing the same. There is also provided a coating material for a modified separator of a lithium-sulfur battery comprising the coral-like composite material as described herein, a conducting carbon material and a binder, and a method of preparing the same.

Induction melt infiltration processing of ceramic matrix composite components

A system and method of melt infiltrating components is provided. In one example aspect, an inductive heating system includes a heating source that inductively heats a susceptor. The susceptor defines a working chamber in which components can be received. During melt infiltration, the system can heat the susceptor and thus the components and melt infiltrants disposed within the working chamber at a first heating rate. The first heating rate can be faster than 50° C./minute. The system can then heat the components and melt infiltrants at a second heating rate. The first heating rate is faster than the second heating rate. Thereafter, the system can heat the components and infiltrants at a third heating rate. The third heating rate can be a constant rate at or above the melting point of the melt infiltrants. The infiltrants can melt and thus infiltrate into the component to densify the component.

Solid-phase-sintered Silicon Carbide Article and Preparation Method thereof
20230134960 · 2023-05-04 ·

The present application relates to the field of engineering ceramic materials, and specifically discloses a solid-phase-sintered silicon carbide article and a preparation method thereof. A method for preparing a solid-phase-sintered silicon carbide article includes the following steps: grinding of raw materials: mixing a micron-scale silicon carbide powder with a boron-containing sintering aid and wet grinding to obtain a slurry; spray granulating: adding a water-soluble carbon black and a binder to the slurry, stirring evenly, and spray granulating to obtain a granulated powder of silicon carbide; mixing; ageing: ageing the wet powder obtained by mixing to obtain a aged material; post-processing: subjecting the aged material to pugging, extruding, drying and heating.

Phase-change material and method for producing same
11795360 · 2023-10-24 ·

A method for producing a form-stable phase-change material to nucleate sugar alcohols includes directionally freezing a slurry of solid chitosan and solvent and additives, providing a frozen slurry including unidirectional pillars of frozen solvent that force suspended solid particles into interstices, exposing the frozen slurry to conditions causing sublimation of the solvent of the frozen slurry to remove frozen solvent and provide a body having pillars of vacancies therein, sintering the body to provide a scaffold including the pillars of vacancies therein, graphitizing the scaffold by heating in argon, treating the scaffold with aqueous base, and adding a molten sugar alcohol phase-change material to the scaffold such that the molten phase-change material is drawn into the pillars of vacancies by capillary action to provide the form-stable phase-change material having reduced hysteresis of the melting point of the sugar alcohol phase-change material.

COMPOSITE SHEET, LAMINATE, AND EVALUATION METHOD FOR ESTIMATING ADHESIVENESS OF COMPOSITE SHEET

One aspect of the present disclosure provides a composite sheet including a porous sintered ceramic component having a thickness of less than 2 mm and a resin filled into pores of the sintered ceramic component, wherein the resin is a semi-cured product of a resin composition including a compound having a cyanate group and the content of triazine rings in the resin is 0.6 to 4.0 mass %.