Patent classifications
C07C309/08
Method for recycling taurine mother liquor
The present disclosure relates to a method for recycling a taurine mother liquor, which includes: adding a base to the taurine mother liquor, heating to a first temperature, carrying out a hydrolysis reaction, removing ammonia produced, and evaporating and concentrating the ammonia-removed solution to obtain an alkali metal hydroxyethyl sulfonate solution. When applying the method provided by the present disclosure for the recycling of the taurine mother liquor, the taurine mother liquor can be further converted into the alkali metal hydroxyethyl sulfonate solution, impurities are removed from the obtained alkali metal hydroxyethyl sulfonate solution, the impurity-removed alkali metal hydroxyethyl sulfonate solution is concentrated and crystallized, and the alkali metal hydroxyethyl sulfonate is separated out. The method provided by the present disclosure is an efficient and simple method for recycling the taurine mother liquor, which is very easy to implement industrially and can effectively recycle the taurine mother liquor.
Method for recycling taurine mother liquor
The present disclosure relates to a method for recycling a taurine mother liquor, which includes: adding a base to the taurine mother liquor, heating to a first temperature, carrying out a hydrolysis reaction, removing ammonia produced, and evaporating and concentrating the ammonia-removed solution to obtain an alkali metal hydroxyethyl sulfonate solution. When applying the method provided by the present disclosure for the recycling of the taurine mother liquor, the taurine mother liquor can be further converted into the alkali metal hydroxyethyl sulfonate solution, impurities are removed from the obtained alkali metal hydroxyethyl sulfonate solution, the impurity-removed alkali metal hydroxyethyl sulfonate solution is concentrated and crystallized, and the alkali metal hydroxyethyl sulfonate is separated out. The method provided by the present disclosure is an efficient and simple method for recycling the taurine mother liquor, which is very easy to implement industrially and can effectively recycle the taurine mother liquor.
UNSATURATED FATTY ALCOHOL DERIVATIVES FROM NATURAL OIL METATHESIS
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D. Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives. Microscopy studies indicate that the unsaturated sodium sulfates in particular have a lamellar phase that should enable formulation at high actives levels. Sulfate compositions comprising 40 to 60 wt. % of a monounsaturated fatty primary alcohol sulfate and 40 to 60 wt. % of a secondary hydroxyalkyl primary alcohol sulfate are also disclosed. The derivatives and sulfate compositions are valuable for many end-use applications, including, for example, agricultural dispersants, water-soluble herbicides, anionic emulsifiers for agricultural use, hard surface cleaners, light-duty liquid detergents, personal cleansers, gas well foamers for oilfield applications, laundry detergents, enhanced oil recovery compositions, latex paints, and specialty foams.
UNSATURATED FATTY ALCOHOL DERIVATIVES FROM NATURAL OIL METATHESIS
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D. Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives. Microscopy studies indicate that the unsaturated sodium sulfates in particular have a lamellar phase that should enable formulation at high actives levels. Sulfate compositions comprising 40 to 60 wt. % of a monounsaturated fatty primary alcohol sulfate and 40 to 60 wt. % of a secondary hydroxyalkyl primary alcohol sulfate are also disclosed. The derivatives and sulfate compositions are valuable for many end-use applications, including, for example, agricultural dispersants, water-soluble herbicides, anionic emulsifiers for agricultural use, hard surface cleaners, light-duty liquid detergents, personal cleansers, gas well foamers for oilfield applications, laundry detergents, enhanced oil recovery compositions, latex paints, and specialty foams.
LIQUID DETERGENT COMPOSITION FOR TEXTILE PRODUCTS
The present invention relates to a liquid detergent composition for textile products containing the following component (A) in an amount of 10% by mass or more and 60% by mass or less), the following component (B), and water: component (A): an internal olefin sulfonate having 17 or more and 24 or less carbon atoms, wherein the mass ratio of an internal olefin sulfonate having 17 or more and 24 or less carbon atoms with the sulfonate group at position 2 or higher and position 4 or lower (IO-1S) to an internal olefin sulfonate having 17 or more and 24 or less carbon atoms with the sulfonate group at position 5 or higher (IO-2S), (IO-1S)/(IO-2S), is 0.75 or more and 5.5 or less; and component (B): an organic solvent having a hydroxy group.
Unsaturated fatty alcohol derivatives from natural oil metathesis
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives.
Unsaturated fatty alcohol derivatives from natural oil metathesis
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives.
CYCLOALKYL-HYDROXYL COMPOUNDS AND COMPOSITIONS FOR CHOLESTEROL MANAGEMENT AND RELATED USES
The present invention relates to novel cycloalkyl-hydroxyl compounds, compositions comprising hydroxyl compounds, and methods useful for treating and preventing a variety of diseases and conditions such as, but not limited to aging, Alzheimer's Disease, cancer, cardiovascular disease, diabetic nephropathy, diabetic retinopathy, a disorder of glucose metabolism, dyslipidemia, dyslipoproteinemia, hypertension, impotence, inflammation, insulin resistance, lipid elimination in bile, obesity, oxysterol elimination in bile, pancreatitis, Parkinson's disease, a peroxisome proliferator activated receptor-associated disorder, phospholipid elimination in bile, renal disease, septicemia, Syndrome X, thrombotic disorder. Compounds and methods of the invention can also be used to modulate C reactive protein or enhance bile production in a patient. In certain embodiments, the compounds, compositions, and methods of the invention are useful in combination therapy with other therapeutics, such as hypocholesterolemic and hypoglycemic agents.
CYCLOALKYL-HYDROXYL COMPOUNDS AND COMPOSITIONS FOR CHOLESTEROL MANAGEMENT AND RELATED USES
The present invention relates to novel cycloalkyl-hydroxyl compounds, compositions comprising hydroxyl compounds, and methods useful for treating and preventing a variety of diseases and conditions such as, but not limited to aging, Alzheimer's Disease, cancer, cardiovascular disease, diabetic nephropathy, diabetic retinopathy, a disorder of glucose metabolism, dyslipidemia, dyslipoproteinemia, hypertension, impotence, inflammation, insulin resistance, lipid elimination in bile, obesity, oxysterol elimination in bile, pancreatitis, Parkinson's disease, a peroxisome proliferator activated receptor-associated disorder, phospholipid elimination in bile, renal disease, septicemia, Syndrome X, thrombotic disorder. Compounds and methods of the invention can also be used to modulate C reactive protein or enhance bile production in a patient. In certain embodiments, the compounds, compositions, and methods of the invention are useful in combination therapy with other therapeutics, such as hypocholesterolemic and hypoglycemic agents.
Method for producing taurine and method for removing impurity from reaction system for producing taurine
Provided is a method for producing taurine including: providing a reaction solution comprising alkali metal taurinate and/or alkali metal isethionate, passing at least a portion of the reaction solution through a column of basic anion exchange resin, adsorbing anions of alkali metal taurinate and/or alkali metal isethionate to the basic anion exchange resin, and collecting an eluate comprising at least one impurity, desorbing anions of alkali metal taurinate and/or alkali metal isethionate from the basic anion exchange resin with an alkaline solution, and collecting a desorption liquid comprising alkali metal taurinate and/or alkali metal isethionate, subjecting the desorption liquid comprising alkali metal taurinate to acidification or subjecting the desorption liquid comprising alkali metal isethionate to aminolysis and acidification, thereby obtaining taurine.