Provided is a method for preparing rutile from acid-soluble titanium slag, including: grinding acid-soluble titanium slag; adding a sodium carbonate modifier, and performing microwave irradiation treatment in a microwave device; adding an ammonium bifluoride additive; and performing acid purification and calcination to obtain rutile. By means of a microwave heating mode, the equipment investment needed by the method is low, and the energy consumption is low. The purity of artificial rutile is more than 91%, byproducts are fewer, and the environmental pollution is low.

A process for leaching a value metal from a titaniferous ore material comprising the step of leaching the ore material at atmospheric pressure with a lixiviant comprising magnesium chloride and hydrochloric acid is disclosed. Iron and titanium are leached into solution. Iron in the ferric state may be separated from titanium in solution using extraction with alkyl ketone. More effective separation of titanium with lower contamination with iron is obtained.

The present invention relates to the recovery of rare earths, scandium, niobium, tantalum, zirconium, hafnium, titanium, and the like from ores or concentrates containing fluorine. More specifically, the ores or concentrates are pretreated by carbochlorination to convert the rare earths and other metals into their chlorides and then subjected to dilute hydrochloric acid leaching to recover the valuable rare earths and other metals from the leachate. Niobium, tantalum, zirconium, hafnium, and titanium can be recovered as their chlorides or oxychlorides from the gaseous products of carbochlorination, or converted into their oxides while simultaneously regenerating chlorine.

The present disclosure relates to processes for recovering rare earth elements from an aluminum-bearing material. The processes can comprise leaching the aluminum-bearing material with an acid so as to obtain a leachate comprising at least one aluminum ion, at least one iron ion, at least one rare earth element, and a solid, and separating the leachate from the solid. The processes can also comprise substantially selectively removing at least one of the at least one aluminum ion and the at least one iron ion from the leachate and optionally obtaining a precipitate. The processes can also comprise substantially selectively removing the at least one rare earth element from the leachate and/or the precipitate.

A method for processing vanadium-titanium magnetite finished ores by using a wet process. The method comprises the steps: extracting vanadium from vanadium-titanium magnetite finished ores and processing, by using the vanadium extraction method, obtained leaching residue by using a wet process, so as to obtain titanium; and calcining the remaining liquid extracted during the vanadium extraction, so as to prepare ferric oxide. The flow of the method is short, and the energy consumption is low, thereby avoiding waste of a titanium resource.

Provided is a method for preparing rutile from acid-soluble titanium slag, including: grinding acid-soluble titanium slag; adding a sodium carbonate modifier, and performing microwave irradiation treatment in a microwave device; adding an ammonium bifluoride additive; and performing acid purification and calcination to obtain rutile. By means of a microwave heating mode, the equipment investment needed by the method is low, and the energy consumption is low. The purity of artificial rutile is more than 91%, byproducts are fewer, and the environmental pollution is low.

A method for preparing self-doped titanium-niobium oxide negative electrode material using a waste titanium dioxide carrier includes preparing self-doped TiNb.sub.2O.sub.7 negative electrode material for lithium-ion battery by using waste titanium dioxide carrier comprises the following steps: S1. converting a waste titanium dioxide carrier into TiO.sub.2 powder with the Ti content of 95% and the Al content of 0.1-4.0%, based on the weight of oxide, respectively; and S2. mixing the TiO.sub.2 powder and Nb.sub.2O.sub.5 powder to form a mixture, roasting the mixture, and collecting the generated Al self-doped TiNb.sub.2O.sub.7, so as to obtain the self-doped TiNb.sub.2O.sub.7 negative electrode material. According to the method disclosed by the present invention, impurities represented by TiO.sub.2 and Al.sub.2O.sub.3 in the waste titanium dioxide carrier can be directly recycled, a self-doped TiNb.sub.2O.sub.7 (titanium niobium oxide) negative electrode material.

There are provided processes for treating red mud. For example, the processes can comprise leaching red mud with HCl so as to obtain a leachate comprising ions of a first metal (for example aluminum) and a solid, and separating said solid from said leachate. Several other metals can be extracted from the leachate (Fe, Ni, Co, Mg, rare earth elements, rare metals, etc.). Various other components can be extracted from solid such as TiO.sub.2, SiO.sub.2 etc.

A process for recovering titanium dioxide from a titanium-bearing material, the process including the steps of: leaching the titanium-bearing material in a first leaching step at atmospheric pressure and at a temperature of 70 to 97 C. with a first lixiviant to produce a first leach solution comprising undissolved first leach solids that include a titanium content and a first leach liquor, the first lixiviant comprising hydrochloric acid at a concentration of less than 23% w/w; separating the first leach liquor and the undissolved first leach solids; leaching the first leach solids in a second leaching step at atmospheric pressure and at a temperature of 60 to 80 C. with a second lixiviant in the presence of a Fe powder reductant to produce a second leach solution comprising undissolved second each solids and a second leach liquor that includes a leached titanium content and iron content, the second lixiviant comprising a mixed chloride solution comprising less than 23% w/w hydrochloric acid and an additional chloride selected from alkali metal chlorides, magnesium chloride and calcium chloride, or mixtures thereof; separating the second leach liquor and the undissolved second leach solids; and thereafter separating the titanium dioxide and the iron content from the second leach liquor by precipitation, and regenerating the second lixiviant for recycle to the second leaching step.

A method of making upgraded synthetic rutile (100) can include binding ilmenite ultrafine particles together with a binder to form green pellets (110). Iron can be reduced in the green pellets by heating the green pellets to a reducing temperature under a reducing atmosphere (120). The ilmenite ultrafine particles within the green pellets can be at least partially sintered together by heating the green pellets at a sintering temperature to form at least partially sintered pellets (130). Iron can be removed from the at least partially sintered pellets by leaching to form upgraded synthetic rutile (140).