Embodiments relate to systems and methods for gas delivery for personal medical consumption having safety features. A hydrogen or oxygen gas delivery system herein can include electrolytic cores performing electrolysis-based reactions, and obtain free hydrogen (H2) gas for collection and delivery to a user. In aspects, the electrolytic core(s) can be scaled to produce a sufficient amount of hydrogen (H2) or oxygen (O2) gas so that the user can ingest that gas directly, without a need for storage. The system can be portable, and configured with a delivery tube for transmitting hydrogen or oxygen gas to a user. While safety risks are generally minimal, the system can be configured with sensors to detect fault conditions or hazards such as combustion or overpressure, which can only be caused by deliberate user action to expose gaseous products to flame or spark, and even then would not be likely to trigger violent combustion.

Embodiments relate to systems and methods for gas delivery for personal medical consumption having safety features. A hydrogen or oxygen gas delivery system herein can include electrolytic cores performing electrolysis-based reactions, and obtain free hydrogen (H2) gas for collection and delivery to a user. In aspects, the electrolytic core(s) can be scaled to produce a sufficient amount of hydrogen (H2) or oxygen (O2) gas so that the user can ingest that gas directly, without a need for storage. The system can be portable, and configured with a delivery tube for transmitting hydrogen or oxygen gas to a user. While safety risks are generally minimal, the system can be configured with sensors to detect fault conditions or hazards such as combustion or overpressure, which can only be caused by deliberate user action to expose gaseous products to flame or spark, and even then would not be likely to trigger violent combustion.

A copper-palladium-loaded mesoporous silicon carbide-based catalyst, a preparation method, and an application thereof are provided. First, a mesoporous silicon carbide material is prepared by using mesoporous silica as a hard template; subsequently, the mesoporous silicon carbide material is mixed with a copper-palladium precursor mixed solution, and dried after the solvent is completely volatilized. The dried powder is successively subjected to calcination with N.sub.2 and reduction with H.sub.2 to finally obtain the copper-palladium-loaded mesoporous silicon carbide-based catalyst. The catalyst is made into an electrode, and the nitrate in water body is catalytically reduced by electrochemical method. The preparation method of the catalyst of the present invention is simple. The catalyst can realize high-efficiency catalytic denitrification at a low metal loading amount, with high selectivity of nitrogen. Moreover, the catalyst has the advantages of high activity, good stability, wide application range and low cost.

A copper-palladium-loaded mesoporous silicon carbide-based catalyst, a preparation method, and an application thereof are provided. First, a mesoporous silicon carbide material is prepared by using mesoporous silica as a hard template; subsequently, the mesoporous silicon carbide material is mixed with a copper-palladium precursor mixed solution, and dried after the solvent is completely volatilized. The dried powder is successively subjected to calcination with N.sub.2 and reduction with H.sub.2 to finally obtain the copper-palladium-loaded mesoporous silicon carbide-based catalyst. The catalyst is made into an electrode, and the nitrate in water body is catalytically reduced by electrochemical method. The preparation method of the catalyst of the present invention is simple. The catalyst can realize high-efficiency catalytic denitrification at a low metal loading amount, with high selectivity of nitrogen. Moreover, the catalyst has the advantages of high activity, good stability, wide application range and low cost.

An embodiment provides a catalyst for water electrolysis which includes an iridium mixed phase formed by physical mixing of two or more selected from metal iridium (Ir), iridium(III) oxide (Ir.sub.2O.sub.3), or iridium(IV) oxide (IrO.sub.2) and has a structure in which nanosheets composed of the iridium mixed phase are stacked. The catalyst for water electrolysis may exhibit high activity and stability for the oxygen evolution reaction in water electrolysis.

An embodiment provides a catalyst for water electrolysis which includes an iridium mixed phase formed by physical mixing of two or more selected from metal iridium (Ir), iridium(III) oxide (Ir.sub.2O.sub.3), or iridium(IV) oxide (IrO.sub.2) and has a structure in which nanosheets composed of the iridium mixed phase are stacked. The catalyst for water electrolysis may exhibit high activity and stability for the oxygen evolution reaction in water electrolysis.

The invention relates to an electrochemical cell partitioned by a cation-exchange membrane suitable for production of high purity hydrogen and oxygen by electrolysis of alkaline solutions comprising a cathode in form of porous web including a platinum or palladium catalyst. The cell can be used as an element of a modular filter-press electrolyzer.

The invention relates to an electrochemical cell partitioned by a cation-exchange membrane suitable for production of high purity hydrogen and oxygen by electrolysis of alkaline solutions comprising a cathode in form of porous web including a platinum or palladium catalyst. The cell can be used as an element of a modular filter-press electrolyzer.

An ion exchange membrane separated two electrode flow analyzer for continuous aqueous electrochemical heavy metal detection is disclosed. The electrochemical cell includes a gas diffusion counter/reference electrode, a flooded flow through working electrode, and an ion exchange membrane that separates the gas diffusion counter/reference electrode and the flooded flow through working electrode. A method of continuous fluid analysis using a multi-electrode flow analyzer is also disclosed, including passing an aqueous sample through a first inlet flow area and into a working electrode of a multi-electrode flow analyzer, passing a gas mixture through a second inlet flow area and into a counter/reference electrode of the multi-electrode flow analyzer, depositing an analyte onto a surface of the working electrode, stripping the analyte from the surface of the working electrode by sweeping a range of a potential applied to the surface of the working electrode.

An ion exchange membrane separated two electrode flow analyzer for continuous aqueous electrochemical heavy metal detection is disclosed. The electrochemical cell includes a gas diffusion counter/reference electrode, a flooded flow through working electrode, and an ion exchange membrane that separates the gas diffusion counter/reference electrode and the flooded flow through working electrode. A method of continuous fluid analysis using a multi-electrode flow analyzer is also disclosed, including passing an aqueous sample through a first inlet flow area and into a working electrode of a multi-electrode flow analyzer, passing a gas mixture through a second inlet flow area and into a counter/reference electrode of the multi-electrode flow analyzer, depositing an analyte onto a surface of the working electrode, stripping the analyte from the surface of the working electrode by sweeping a range of a potential applied to the surface of the working electrode.