C04B35/62849

Low-shrinkage, high-strength, and large ceramic plate and manufacturing method thereof

Disclosed are a low-shrinkage, high-strength, and large ceramic plate and a manufacturing method thereof. The method comprises the following steps: (1) preparing a ceramic raw material powder; (2) subjecting an acicular wollastonite to surface coating with a silane coupling agent and to pre-dispersion with a fumed silica to obtain a pre-treated acicular wollastonite; and (3) thoroughly mixing the ceramic raw material powder and the pre-treated acicular wollastonite and granulating the resulting mixture, the amount of the pre-treated acicular wollastonite added being 10 wt % to 30 wt % of the ceramic raw material powder, and subjecting the resulting granules to dry pressing and sintering to obtain the large ceramic plate. The acicular wollastonite is incorporated into the manufacturing of the large ceramic plate to take full advantage of the reinforcing effect and low sintering shrinkage characteristics of the acicular wollastonite. The invention reduces sintering shrinkage and increases product strength.

FILAMENT WOUND HIGH DENIER ALUMINUM OXIDE FIBER COMPONENTS AND METHODS OF MAKING

An Oxide-Oxide (Ox-Ox) ceramic matrix composite (CMC) component includes a woven high denier ceramic fiber, the fiber comprising a plurality of tows, the woven fiber having interstitial spacing and the tows comprising the fiber having interstitial spacing, an aluminosilicate matrix, wherein the aluminosilicate matrix occupies the interstitial spacing between the fibers, and wherein the aluminosilicate matrix further occupies at least some of the interstitial spacing between the tows of the fiber. In another aspect, a method of fabricating an Oxide-Oxide (Ox-Ox) component includes the steps of providing a ceramic fiber, providing an aluminosilicate slurry, coating the fiber with the aluminosilicate slurry, filament winding the coated fiber over tooling, forming an uncured preform, removing the uncured Ox-Ox preform from the tooling, and curing the Ox-Ox preform, forming a near net shape Ox-Ox component.

METHOD TO ACHIEVE A SMOOTH SURFACE WITH PRECISE TOLERANCE CONTROL FOR A COMPLEX (NON-FLAT) GEOMETRY
20210147302 · 2021-05-20 ·

A method of producing a CMC having a smooth surface includes forming a fiber preform; rigidizing the preform with an interphase coating; infiltrating a ceramic slurry into the preform to form a green body; conducting secondary operations on the green body; applying a slurry-based layer onto a portion of the green body; and infiltrating the green body with a molten silicon or silicon alloy, such that the CMC exhibits a smooth surface. The application of the slurry-based surface layer onto the green body includes placing the green body into a tool fixture having upper and lower components, such that a gap is present between the green body and at least one of the upper and lower components; and delivering a surface layer slurry into at least one gap, such that the surface layer slurry forms the slurry-based layer on at least a portion of the green body.

MICROSTRUCTURED FIBER INTERFACE COATINGS FOR COMPOSITES

Disclosed is a coated ceramic fiber including a silicon carbide coating layer adjacent to the ceramic fiber and a silicon dioxide coating layer adjacent to the silicon carbide coating layer, wherein the silicon dioxide coating layer forms micro cracks after a crystal structure transformation. The coated ceramic fiber may be included in a composite material having a ceramic matrix.

Methods of forming ceramic matrix composites using sacrificial fibers and non-wetting coating

Methods for preparing ceramic matrix composites using melt infiltration are provided as well as the resulting ceramic matrix composites. The methods and products include the incorporation of a non-wetting coating to one or more sacrificial fibers. The one or more sacrificial fibers are removed, such as decomposed during pyrolysis, resulting in the formation of a plurality of functional features, in the form of regular and elongate channels along the ceramic matrix composite. During the removing of the one or more sacrificial fibers, the non-wetting coating remains on an interior surface of the plurality of functional features to block infiltration of an infiltrant to the plurality of functional features and deposition thereon. Alternatively, the sacrificial fibers may be removed subsequent to melt infiltration.

COVER-LAYER-INCLUDING CERAMIC CONTINUOUS FIBER, METHOD FOR PRODUCING THE SAME, CERAMIC MATRIX COMPOSITE MATERIAL AND METHOD FOR PRODUCING THE SAME
20230406779 · 2023-12-21 ·

Provided are a cover-layer-including ceramic continuous fiber suitable for producing a ceramic matrix composite material that can have improved damage tolerance and a ceramic matrix composite material formed from the cover-layer-including ceramic continuous fiber. The cover-layer-including ceramic continuous fiber includes a ceramic continuous fiber and a cover layer formed of an inorganic acid salt and disposed on the surface of the ceramic continuous fiber, wherein the thickness variation coefficient of the cover layer is 80% or less.

HIGH TEMPERATURE FIBER, METHOD OF MAKING AND HIGH TEMPERATURE FIBER COMPOSITES
20210039999 · 2021-02-11 ·

Disclosed is a method of making high temperature fiber including chemically bonding high temperature material to a fiber template at a first temperature to form a precursor fiber and processing the precursor fiber at a second temperature to form the high temperature fiber. The first temperature does not equal the second temperature. Also disclosed are high temperature fibers made by the method.

FORMING FEATURES IN ADDITIVELY MANUFACTURED COMPOSITE MATERIALS USING SACRIFICIAL SUPPORT MATERIALS
20210060866 · 2021-03-04 ·

A method may include depositing a sacrificial support material on or adjacent to a build surface. The sacrificial support material may be configured to support a continuous reinforcement material during an additive manufacturing technique. The method also may include extruding the continuous reinforcement material from an additive manufacturing device such that at least a portion of the continuous reinforcement material contacts and is supported by the sacrificial support material; and removing the sacrificial support material to result in a feature defined at least in part by the continuous reinforcement material at the absence of sacrificial support material.

Fibers fabricated with metals incorporated into grain boundaries for high temperature applications
20200392648 · 2020-12-17 ·

A fiber comprises a bulk material comprising: one or more of carbon, silicon, boron, silicon carbide, and boron nitride; and a metal or metal alloy whose affinity for oxygen is greater than that of the bulk material. At least a first portion of the metal or metal alloy is present at the entrance to grain boundaries at the surface of the fiber and within the fiber to a depth of at least 1 micron from the fiber surface.

A method of improving a fiber comprises heating a fiber in an inert atmosphere to 900-1300 C for sufficient time to allow at least some of a metal or metal alloy, placed on the fiber, to diffuse and/or flow into and along grain boundaries to a depth of at least 1 micron. The metal or metal alloy has a greater affinity for oxygen than that of the fiber bulk material.

METHOD FOR TREATING SILICON CARBIDE FIBRES
20200377416 · 2020-12-03 ·

A method of treating at least one silicon carbide fibre, the method including a) formation of a silica layer at the surface of a silicon carbide fibre having an oxygen content less than or equal to 1% in atomic percentage, the silica layer being formed by contacting this fibre with an oxidizing medium having a temperature greater than or equal to 50 C. and pressure greater than or equal to 1 MPa, and b) removal of the silica layer formed by hydrothermal treatment of the fibre obtained after implementation of step a) in which the fibre is treated with water at a pressure between saturating vapour pressure and 30 MPa and at a temperature less than or equal to 400 C.