C04B2235/5244

CMAS-RESISTANT ENVIRONMENTAL BARRIER COATING SYSTEM
20220371967 · 2022-11-24 ·

An article may include a substrate, such as a silicon-containing ceramic matrix composite, an environmental barrier coating (EBC) layer on the substrate, and a CMAS-resistant EBC layer on the EBC layer. The EBC layer may include at least one rare-earth disilicate (REDS). The CMAS-resistant EBC layer may include at least one rare-earth monosilicate (REMS) configured to react with CMAS to form crystalline reaction products. The CMAS-resistant EBC layer may include a plurality of vertical cracks extending from a surface of the CMAS-resistant EBC layer at least partially into the CMAS-resistant EBC layer. Additionally, or alternatively, the EBC layer may include a plurality of vertical cracks extending from a surface of the EBC layer into at least a portion of the EBC layer.

Automated preparation method of a SiC.SUB.f./SiC composite flame tube
11591267 · 2023-02-28 · ·

An automated preparation method of a SiC.sub.f/SiC composite flame tube, comprising the following steps: preparing an interface layer for a SiC fiber by a chemical vapor infiltration process, and obtaining the SiC fiber with a continuous interface layer; laying a unidirectional tape on the SiC fiber with the continuous interface layer and winding the SiC fiber with the continuous interface layer to form and obtaining a preform of a net size molding according to a fiber volume and a fiber orientation obtained in a simulation calculation; and adopting a reactive melt infiltration process and the chemical vapor infiltration process successively for a densification and obtaining a high-density SiC.sub.f/SiC composite flame tube in a full intelligent way. The SiC.sub.f/SiC composite flame tube prepared by the present disclosure not only has a high temperature resistance, but also has a low thermal expansion coefficient, high thermal conductivity and high thermal shock resistance.

Doped silicon carbide ceramic matrix composite

A method for forming ceramic matrix composite (CMC) component includes forming a fiber preform, positioning the fiber preform into a chemical vapor infiltration reactor chamber, and densifying the fiber preform. Densification includes infiltrating the fiber preform with a first gas comprising precursors of silicon carbide and infiltrating the fiber preform with a second gas comprising a first rare earth element, wherein the steps of infiltrating the fiber preform with the first gas and infiltrating the fiber preform with the second gas are conducted simultaneously to produce a first rare earth-doped silicon carbide matrix in a first region of the component.

Airfoil with serpentine fiber ply layup

An airfoil includes an airfoil section that is formed of a fiber-reinforced composite that has fiber plies. The fiber plies include at least one overwrap fiber ply, first and second support fiber plies, and a serpentine fiber ply. The overwrap fiber ply circumscribes an internal cavity and defines first and second sides and leading and trailing ends of the airfoil section. The first and second support fiber plies define respective first and second radial tubes in the internal cavity. The serpentine fiber ply winds from the first side and around the first radial tube to the second side, then from the second side back to the first side, and then from the first side and around the second radial tube back to the second side.

Method for treating silicon carbide fibres

A method of treating at least one silicon carbide fibre, the method including a) formation of a silica layer at the surface of a silicon carbide fibre having an oxygen content less than or equal to 1% in atomic percentage, the silica layer being formed by contacting this fibre with an oxidizing medium having a temperature greater than or equal to 50° C. and pressure greater than or equal to 1 MPa, and b) removal of the silica layer formed by hydrothermal treatment of the fibre obtained after implementation of step a) in which the fibre is treated with water at a pressure between saturating vapour pressure and 30 MPa and at a temperature less than or equal to 400° C.

METHOD FOR MANUFACTURING AN ELASTIC CERAMIC MATRIX COMPOSITE
20230093876 · 2023-03-30 ·

Disclosed are: damage-resistant ECMCs that need to work and remain elastic between minus 120° C. and positive 300° C.; ECMCs that need to be able to contain a flame of 1900° C. for more than 90 minutes; and composite structures, especially highly stressed structures. One of the characteristic problems of ceramic matrices is their fragility. Indeed, when a fracture starts, it propagates easily in the matrix. Disclosed are elastic ceramic matrix composites (ECMCs), for which: the ceramic matrix is split into solid “ceramic microdomains” (CMDs); the CMDs are connected to one another by a dense network of “elastic microelements” (EMEs); and the bonds between the EMEs and the CMDs are strong chemical bonds, preferably covalent.

CONSTANT CROSS SECTION MANDREL FOR CMC COMPONENTS
20230100487 · 2023-03-30 ·

A mandrel for a molding process includes a first portion and a second portion that form a mandrel having a channel between the first and second portions. At least one locking pin is configured to urge the first and second portions away from each other to establish a gap in response to inserting the locking pin into the channel along a respective end of the mandrel. A molding apparatus and method of forming a matrix composite component are also disclosed.

CERAMIC MATRIX COMPOSITE WITH INTERFACIAL COATING SYSTEM

A ceramic matrix composite includes a ceramic matrix, fibers embedded in the ceramic matrix, and an interfacial coating system on each of the fibers. The interfacial coating system includes alternating layers of boron nitride layers of individual thicknesses of about 50 nanometers to 200 nanometers and carbon layers of individual thicknesses of less than 5 nanometers.

CVD FUNCTIONALIZED PARTICLES FOR CMC APPLICATIONS
20230036697 · 2023-02-02 ·

A method of manufacturing ceramic matrix composites includes producing chemical vapor deposition functionalized ceramic particles before injecting the functionalized ceramic particles into the CMC fabric. The functionalized ceramic particles are mixed with a binder solution and then dispensed into voids present between adjacent tows of the CMC fabric. Injecting the particles in the center of the voids reduces the size and volume fraction of the voids/defects, improving the homogeneity of surface texture, homogeneity of microstructure, and part model shape conformity.

CONTACT JOULE HEATING FOR SINTERING HIGH TEMPERATURE COATINGS
20220348513 · 2022-11-03 ·

A method for forming a high temperature coating includes forming a pre-sintered ceramic coating on a ceramic composite substrate. The pre-sintered ceramic coating includes a plurality of ceramic particles. The method further includes sintering at least a portion of the pre-sintered ceramic coating by heating the portion of the pre-sintered ceramic coating to a sintering temperature of the plurality of ceramic particles using joule heating. The sintering temperature is greater than about 1000 degrees Celsius (° C.).