The present invention relates to a novel process for preparing an isolate of cationic whey proteins containing high purity lactoferrin.

The present invention relates to a novel process for preparing an isolate of cationic whey proteins containing high purity lactoferrin.

The invention relates to a method of producing a dairy concentrate, comprising the steps of: providing an ingredient composition comprising micellar caseins and whey proteins and having a pH of 6.1-7.1 and a concentration of 3-25 wt. % of proteins, and wherein the ingredient composition has a casein to whey protein ratio of 90/10-60/40, adding 3-25 mM divalent cations to provide a concentration of 3-8 mM free divalent cations in the ingredient composition, homogenising the ingredient composition; and subsequently pasteurising and stirring the ingredient composition at a temperature of 80-105 C. for a period of 0.5-3 min to form agglomerated proteins comprising caseins and beta-lactoglobulin from the whey proteins, the agglomerates having a size of 3-50 microns as measured by D(4,3) mean diameter. The invention also relates to a method with an ultra-high temperature treatment of the ingredient mix. Furthermore, the invention relates to a dairy concentrate comprising aggregated proteins comprising micellar casein and whey protein aggregates, wherein the product has a pH of 6.0-7.1, a concentration of 6-55 wt. % milk solids, a casein to whey protein ratio of 90/10-60/40, and a concentration of 3-8 mM free divalent cations, and wherein the agglomerates having a size of 3-50 microns mean diameter D(4,3) as measured by laser diffraction.

The invention relates to a method of producing a dairy concentrate, comprising the steps of: providing an ingredient composition comprising micellar caseins and whey proteins and having a pH of 6.1-7.1 and a concentration of 3-25 wt. % of proteins, and wherein the ingredient composition has a casein to whey protein ratio of 90/10-60/40, adding 3-25 mM divalent cations to provide a concentration of 3-8 mM free divalent cations in the ingredient composition, homogenising the ingredient composition; and subsequently pasteurising and stirring the ingredient composition at a temperature of 80-105 C. for a period of 0.5-3 min to form agglomerated proteins comprising caseins and beta-lactoglobulin from the whey proteins, the agglomerates having a size of 3-50 microns as measured by D(4,3) mean diameter. The invention also relates to a method with an ultra-high temperature treatment of the ingredient mix. Furthermore, the invention relates to a dairy concentrate comprising aggregated proteins comprising micellar casein and whey protein aggregates, wherein the product has a pH of 6.0-7.1, a concentration of 6-55 wt. % milk solids, a casein to whey protein ratio of 90/10-60/40, and a concentration of 3-8 mM free divalent cations, and wherein the agglomerates having a size of 3-50 microns mean diameter D(4,3) as measured by laser diffraction.

Phospholipid concentration methods involve use of a dairy composition, such as buttermilk or butter serum, as a starting material. The dairy composition is subjected to a first ultrafiltration, yielding a first permeate and a first retentate. The first retentate is treated with carbon dioxide and subjected to microfiltration, yielding a second permeate and a second retentate. The second retentate is treated with carbon dioxide and subjected to a second ultrafiltration, yielding a third permeate and a third retentate. The third retentate includes at least 30 wt % phospholipids.

Phospholipid concentration methods involve use of a dairy composition, such as buttermilk or butter serum, as a starting material. The dairy composition is subjected to a first ultrafiltration, yielding a first permeate and a first retentate. The first retentate is treated with carbon dioxide and subjected to microfiltration, yielding a second permeate and a second retentate. The second retentate is treated with carbon dioxide and subjected to a second ultrafiltration, yielding a third permeate and a third retentate. The third retentate includes at least 30 wt % phospholipids.

A device for heating a concentrate comprises a drying tower comprises a plurality of pressurized spray nozzles, a feed tank fluidly connected with an inlet of a low-pressure heat, a feed pump, and a high-pressure piston pump connected on an inlet side with the outlet of the low-pressure heat exchanger. A first high-pressure line section of the high-pressure line is configured to connect the outlet of the high-pressure piston pump with the inlet of the additional high-pressure heat exchanger. A second high-pressure line section of the high-pressure line is configured to connect the outlet of the additional high-pressure heat exchanger with the pressurized spray nozzles. A means for defined shear loading of the concentrate is located in an outlet-side channel and comprises an annular-shaped space.

A device for heating a concentrate comprises a drying tower comprises a plurality of pressurized spray nozzles, a feed tank fluidly connected with an inlet of a low-pressure heat, a feed pump, and a high-pressure piston pump connected on an inlet side with the outlet of the low-pressure heat exchanger. A first high-pressure line section of the high-pressure line is configured to connect the outlet of the high-pressure piston pump with the inlet of the additional high-pressure heat exchanger. A second high-pressure line section of the high-pressure line is configured to connect the outlet of the additional high-pressure heat exchanger with the pressurized spray nozzles. A means for defined shear loading of the concentrate is located in an outlet-side channel and comprises an annular-shaped space.

A method for heating a concentrate in an installation for spray drying comprises increasing a pressure of the concentrate from a low pressure level at a flow temperature to a high pressure level. The concentrate is heated at a high pressure level to a spraying temperature using a high-pressure heat exchanger. The concentrate is shear loaded using a shearing device and immediately transferring the concentrate to a location of pressurized spraying, wherein a transfer time for the immediate transfer is determined by a fluidic effective distance between the shearing device and the location of the pressurized spraying.

A method for heating a concentrate in an installation for spray drying comprises increasing a pressure of the concentrate from a low pressure level at a flow temperature to a high pressure level. The concentrate is heated at a high pressure level to a spraying temperature using a high-pressure heat exchanger. The concentrate is shear loaded using a shearing device and immediately transferring the concentrate to a location of pressurized spraying, wherein a transfer time for the immediate transfer is determined by a fluidic effective distance between the shearing device and the location of the pressurized spraying.