Patent classifications
D01D5/40
Preparation method of para-aramid nanofibers
The present invention relates to a preparation method of para-aramid nanofibers, and belongs to the technical field of novel polymer materials. The para-aramid nanofibers prepared in the present invention have a diameter of 10-100 nm, and a length of hundreds of microns. The preparation method includes: adding a certain amount of surfactant in a PPTA low-temperature polymerization process, and controlling aggregation of PPTA molecules along with growth of a PPTA molecule chain, thereby preparing the para-aramid fibers with a uniform size and an adjustable nano-scale diameter under assistance of other means (e.g., a coagulator and high-speed shearing dispersion). The present invention is short in production process and simple in equipment, can realize stable batch production to meet needs of large-scale production of the para-aramid nanofibers, has wide application prospects and can be applied to preparing a lithium-ion battery separator, a high-performance composite material and the like.
Cellulose xanthate nanofiber
Nanofiber that keep crystallinity are obtained from a cellulose material under light load. The nanofiber are obtained by treating a material containing cellulose with 4% by mass or more and 9% by mass or less of an aqueous alkali metal hydroxide solution to produce alkali cellulose, reacting the alkali cellulose with carbon disulfide to give cellulose xanthate, and defibrating the cellulose xanthate. Then, the xanthate is treated with acid or heat to be regenerated into cellulose nanofiber.
Cellulose xanthate nanofiber
Nanofiber that keep crystallinity are obtained from a cellulose material under light load. The nanofiber are obtained by treating a material containing cellulose with 4% by mass or more and 9% by mass or less of an aqueous alkali metal hydroxide solution to produce alkali cellulose, reacting the alkali cellulose with carbon disulfide to give cellulose xanthate, and defibrating the cellulose xanthate. Then, the xanthate is treated with acid or heat to be regenerated into cellulose nanofiber.
Fibers with filler
The present invention is directed to articles of manufacture, including fibers and films, and methods of making thereof. In accordance with the present invention, the article includes a binder impregnated with or encapsulating a filler. The binder is a polyvinyl alcohol (PVOH), cellulose nanofibrils, or a combination of the PVOH and cellulose nanofibrils. The filler is deinking waste solids comprising ash and cellulose fines.
Fibers with filler
The present invention is directed to articles of manufacture, including fibers and films, and methods of making thereof. In accordance with the present invention, the article includes a binder impregnated with or encapsulating a filler. The binder is a polyvinyl alcohol (PVOH), cellulose nanofibrils, or a combination of the PVOH and cellulose nanofibrils. The filler is deinking waste solids comprising ash and cellulose fines.
Shear spun sub-micrometer fibers
A process including shearing a first dispersion medium and a second dispersion medium under conditions that precipitate a plurality of polymeric fibers; and collecting the plurality of polymeric fibers at a rate of at least 300 grams/hour. The first dispersion medium is a solution including at least one polymeric component. The at least one polymeric component includes a polyetherimide component selected from the group consisting of polyetherimide homopolymers, polyetherimide co-polymers, polyetherether ketones homopolymers, polyetherether ketones copolymers, polyphenylene sulfones homopolymers, polyphenylene sulfones copolymers, and combinations thereof. Products produced by the process can be non-woven paper, medical implants, ultra-fine filters, membranes, hospital gowns, electrical insulation paper, honeycomb structures and personal hygiene products, dialyzers, blood, oxygenator filters, intravenous (IV) filters, diagnostic test filters, and blood/apheresis filters.
Shear spun sub-micrometer fibers
A process including shearing a first dispersion medium and a second dispersion medium under conditions that precipitate a plurality of polymeric fibers; and collecting the plurality of polymeric fibers at a rate of at least 300 grams/hour. The first dispersion medium is a solution including at least one polymeric component. The at least one polymeric component includes a polyetherimide component selected from the group consisting of polyetherimide homopolymers, polyetherimide co-polymers, polyetherether ketones homopolymers, polyetherether ketones copolymers, polyphenylene sulfones homopolymers, polyphenylene sulfones copolymers, and combinations thereof. Products produced by the process can be non-woven paper, medical implants, ultra-fine filters, membranes, hospital gowns, electrical insulation paper, honeycomb structures and personal hygiene products, dialyzers, blood, oxygenator filters, intravenous (IV) filters, diagnostic test filters, and blood/apheresis filters.
HIGH TEMPERATURE MELT INTEGRITY BATTERY SEPARATORS VIA SPINNING
A method for preparing a high temperature melt integrity separator, the method comprising spinning a polymer by one or more of a mechanical spinning process and an electro-spinning process to produce fine fibers.
HIGH TEMPERATURE MELT INTEGRITY BATTERY SEPARATORS VIA SPINNING
A method for preparing a high temperature melt integrity separator, the method comprising spinning a polymer by one or more of a mechanical spinning process and an electro-spinning process to produce fine fibers.
FRACTAL-LIKE POLYMERIC PARTICLES AND THEIR USE IN DIVERSE APPLICATIONS
Fractal-like polymeric particles having a hierarchical, branched structure are disclosed. The particles have fibers with nanometer-scale diameters on their peripheries, which enables a number of unique and highly desirable properties. The particles are fabricated by a method combining phase separation and shear forces of different solutions, in particular a polymer solution. In addition, the particles may be used as coatings, nonwovens, textiles and viscosity modifiers and adhesives, among other applications.