Patent classifications
D01F2/02
A PROCESS AND A SPINNING LINE UNIT FOR WET SPINNING OF CELLULOSE FIBERS FROM AN ALKALINE SPIN BATH
A process for forming a fiber tow, involves a wet spinning procedure comprising the steps of: dissolving cellulose pulp N in an alkaline aqueous solvent to form a cellulose spin dope composition, spinning the cellulose spin dope composition in a coagulation having a p H of more than 7.0, preferably a pH of at least 10, to produce a fiber tow, and passing the produced fiber tow through a sequence of consecutive stretching and washing steps in which the formed fiber tow is washed with a washing liquid by a counter-current flow washing procedure.
METHOD AND SYSTEM FOR THE PRODUCTION OF A SPINNING DOPE COMPOSITION
The present invention describes a method for the production of a spinning dope composition, said method comprising a homogenization involving vigorous mixing of a cellulosic pulp material in alkali solution, vigorous mixing implying supplying a power density to agitators used in the homogenization step of at least 150 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume), and thereafter a dissolution involving mixing of the cellulosic pulp material in the alkali solution to obtain a spinning dope composition, wherein the power density supplied to agitators used in the dissolution step is maximum 75 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume); and wherein the cellulosic pulp material in alkali solution is kept at a temperature of less than 0° C. during the homogenization and during at least part of the dissolution. The present invention is also directed to a system intended for the production of a spinning dope composition.
METHOD AND SYSTEM FOR THE PRODUCTION OF A SPINNING DOPE COMPOSITION
The present invention describes a method for the production of a spinning dope composition, said method comprising a homogenization involving vigorous mixing of a cellulosic pulp material in alkali solution, vigorous mixing implying supplying a power density to agitators used in the homogenization step of at least 150 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume), and thereafter a dissolution involving mixing of the cellulosic pulp material in the alkali solution to obtain a spinning dope composition, wherein the power density supplied to agitators used in the dissolution step is maximum 75 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume); and wherein the cellulosic pulp material in alkali solution is kept at a temperature of less than 0° C. during the homogenization and during at least part of the dissolution. The present invention is also directed to a system intended for the production of a spinning dope composition.
Nanocellulosic compositions
The invention relates to a method of manufacturing a nanocellulosic composition comprising cellulose nanoparticles and/or nanoparticles. The nanocellulosic compositions are useful in the manufacturing of biodegradable plastics. The invention also includes a method of manufacturing biodegradable plastics using such nanocellulosic compositions.
Nanocellulosic compositions
The invention relates to a method of manufacturing a nanocellulosic composition comprising cellulose nanoparticles and/or nanoparticles. The nanocellulosic compositions are useful in the manufacturing of biodegradable plastics. The invention also includes a method of manufacturing biodegradable plastics using such nanocellulosic compositions.
RETRIEVING AND REPOLYMERIZING TEXTILE FIBERS
The present disclosure relates to methods and systems for recovering and repolymerizing textile fibers. Textile fibers, such as those containing cellulose or elastomers, can undergo multiple rounds of recovery and regeneration. During the regeneration process, the textile fibers are isolated from non-desired material, repolymerized or reformed, and then extruded to form a second set of textile fibers. The degree of polymerization of the textile fiber decreases with each regeneration cycle. Regeneration and production can be repeated any appropriate number of times until the regenerated textile fibers do not have the necessary or appropriate degree of polymerization for textile production.
RETRIEVING AND REPOLYMERIZING TEXTILE FIBERS
The present disclosure relates to methods and systems for recovering and repolymerizing textile fibers. Textile fibers, such as those containing cellulose or elastomers, can undergo multiple rounds of recovery and regeneration. During the regeneration process, the textile fibers are isolated from non-desired material, repolymerized or reformed, and then extruded to form a second set of textile fibers. The degree of polymerization of the textile fiber decreases with each regeneration cycle. Regeneration and production can be repeated any appropriate number of times until the regenerated textile fibers do not have the necessary or appropriate degree of polymerization for textile production.
METHOD FOR PREPARING CELLULOSE DOPE
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
METHOD FOR PREPARING CELLULOSE DOPE
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
METHOD FOR PREPARING FLAME-RETARDANT CELLULOSIC FIBERS
A type of flame-retardant cellulosic fiber and a preparation method thereof are disclosed. The preparation method includes extruding the cellulosic solution through a spinneret, coagulating, stretching, and water-washing to obtain a water-washed filament, which is then treated with a flame-retardant solution, and then rinsed and dried to prepare the flame-retardant cellulosic fiber. The water-washing temperature is 90° C., the temperature of the flame-retardant solution during treatment is 60-90° C., and the rinsing temperature is 20-40° C. The flame retardant contains more than one of a group that forms a covalent bond with a hydroxy group of the cellulosic macromolecule, a group having the ability of self-crosslinking reaction, and a group that forms a hydrogen bond with a hydroxy group of the cellulosic macromolecule. The prepared flame-retardant cellulosic fiber is mainly composed of the cellulosic fiber matrix and the flame retardant dispersed in the matrix.