Patent classifications
D01F6/78
Method for producing ceramic fibers of a composition in the SiC range and for producing SiC fibers
A method for producing ceramic fibers of a composition in the SiC range, starts from a spinning material that contains a polysilane-polycarbosilane copolymer solution. The spinning material is extruded through spinnerets in a dry spinning method and spun through a spinning duct into green fibers, and the green fibers are subsequently pyrolyzed. Accordingly, the polysilane-polycarbosilane solution contains between 75 wt. % and 95 wt. %, in particular between 80 and 90 wt. %, of an indifferent solvent, and the spinnerets have a capillary diameter between 20 and 70 m, in particular between 30 and 60 m, in particular between 40 and 50 m.
Controlling crosslinking density and processing parameters of phthalonitriles
Disclosed is a composition having: a diphthalonitrile compound having at least two phthalonitrile groups; a reactive plasticizer; and an amine curing agent. Also disclosed is a composition having: a diphthalonitrile compound having at least two phthalonitrile groups; a nonreactive plasticizer; and an amine curing agent. Also disclosed is a method of: providing a composition having a phthalonitrile compound; heating the composition to a processing temperature until the composition has a viscosity of 30-40 Pa.Math.s at the processing temperature to form a partially cured composition; placing the partially cured composition into a material chamber of an extrusion machine; heating the partially cured composition and the material chamber to within 10 C. of the processing temperature; and extruding fiber from the extrusion machine.
Controlling crosslinking density and processing parameters of phthalonitriles
Disclosed is a composition having: a diphthalonitrile compound having at least two phthalonitrile groups; a reactive plasticizer; and an amine curing agent. Also disclosed is a composition having: a diphthalonitrile compound having at least two phthalonitrile groups; a nonreactive plasticizer; and an amine curing agent. Also disclosed is a method of: providing a composition having a phthalonitrile compound; heating the composition to a processing temperature until the composition has a viscosity of 30-40 Pa.Math.s at the processing temperature to form a partially cured composition; placing the partially cured composition into a material chamber of an extrusion machine; heating the partially cured composition and the material chamber to within 10 C. of the processing temperature; and extruding fiber from the extrusion machine.
POLYETHERIMIDE-BASED FIBER, METHOD FOR MANUFACTURING SAME, AND FIBER STRUCTURE CONTAINING SAME
Provided is a polyetherimide-based fiber containing a polyetherimide resin and carbon black dispersed in the resin, wherein the content of the carbon black is 0.03 wt % or greater; the carbon black has a primary particle number-mean particle size of from 30 nm to 500 nm; and the fiber has a weight reduction rate of less than 0.5% around the glass transition point (Tg) of the polyetherimide resin, where the weight reduction rate is defined by a following formula (1).
Weight reduction rate (%)={[(fiber weight at temperature T1)(fiber weight at temperature T2)]/(fiber weight at temperature T1)}100(1)
Where T1 denotes a temperature (Tg15 C.) that is 15 C. lower than the glass transition point (glass transition temperature) of the polyetherimide resin, and T2 denotes a temperature (Tg+25 C.) that is 25 C. higher than the glass transition point.
POLYETHERIMIDE-BASED FIBER, METHOD FOR MANUFACTURING SAME, AND FIBER STRUCTURE CONTAINING SAME
Provided is a polyetherimide-based fiber containing a polyetherimide resin and carbon black dispersed in the resin, wherein the content of the carbon black is 0.03 wt % or greater; the carbon black has a primary particle number-mean particle size of from 30 nm to 500 nm; and the fiber has a weight reduction rate of less than 0.5% around the glass transition point (Tg) of the polyetherimide resin, where the weight reduction rate is defined by a following formula (1).
Weight reduction rate (%)={[(fiber weight at temperature T1)(fiber weight at temperature T2)]/(fiber weight at temperature T1)}100(1)
Where T1 denotes a temperature (Tg15 C.) that is 15 C. lower than the glass transition point (glass transition temperature) of the polyetherimide resin, and T2 denotes a temperature (Tg+25 C.) that is 25 C. higher than the glass transition point.
Elastomer resins, fibers and fabrics thereof, and uses thereof
The present invention relates to elastomeric resins, fibers made from said resins, fabrics made with said fibers, and applications and uses for the resins, fibers and fabrics. The elastomer resins of the invention provide high strength fibers and well balanced fabrics with good physical properties and chemical resistance, making them attractive for use in various applications that use elastic fibers and fabrics.
Elastomer resins, fibers and fabrics thereof, and uses thereof
The present invention relates to elastomeric resins, fibers made from said resins, fabrics made with said fibers, and applications and uses for the resins, fibers and fabrics. The elastomer resins of the invention provide high strength fibers and well balanced fabrics with good physical properties and chemical resistance, making them attractive for use in various applications that use elastic fibers and fabrics.
Method for the synthesis of a chlorine-free, pre-ceramic polymer for the production of ceramic molded bodies
A method for producing a polysilane includes a disproportionation reaction of a methylchlorodisilane mixture to form chlorine-containing oligosilane, a substitution reaction of the chlorine atoms contained in the oligosilane by the reaction with a primary amine and a cross-linking reaction of the oligosilanes using a chain former to form polysilanes. The obtained polysilanes are infusible and are very suitable for being spun to form green fibers and processed to form silicon carbide fibers and fiber composites. The method is characterized in that it can be carried out cost-effectively and quickly and with very high yields.
Method for the synthesis of a chlorine-free, pre-ceramic polymer for the production of ceramic molded bodies
A method for producing a polysilane includes a disproportionation reaction of a methylchlorodisilane mixture to form chlorine-containing oligosilane, a substitution reaction of the chlorine atoms contained in the oligosilane by the reaction with a primary amine and a cross-linking reaction of the oligosilanes using a chain former to form polysilanes. The obtained polysilanes are infusible and are very suitable for being spun to form green fibers and processed to form silicon carbide fibers and fiber composites. The method is characterized in that it can be carried out cost-effectively and quickly and with very high yields.
Nonwoven webs and multi-component fibers comprising a polydiorganosiloxane polyamide and methods of melt blowing
The present invention pertains to nonwoven webs, and multi-component fibers comprising polydiorganosiloxane polyamide as well as method of making microfibers and multi-component fibers comprising a polydiorganosiloxane polyamide copolymer.