Patent classifications
D21C3/003
MULTI-STEP PROCESS FOR THE ISOLATION OF COMPONENTS FROM MISCANTHUS
The invention relates to a process for the isolation of components from plant material of Miscanthus. The process comprises three subsequent extractions. The first extraction yields an extract comprising one or more compounds selected from the group of antioxidants, polyphenols, proteins, sterols, acids, alcohols, ketones, aldehydes and aromatic compounds. Thereafter, the plant material is subjected to two extractions with a metal hydroxide (e.g. NaOH), the first performed at a lower pH than the second. These steps yield a sugar fraction and a lignin fraction, respectively. Finally, from the residue after the third extraction, cellulose is isolated.
EFFICIENT METHODS AND COMPOSITIONS FOR RECOVERY OF PRODUCTS FROM ORGANIC ACID PRETREATMENT OF PLANT MATERIALS
Provided are compositions and processes concerning efficient downstream processing of products derived from organic acids pretreatment of plant materials.
Method for separating cellulose
A method for separating cellulose from a wood-based raw material including hemicellulose, cellulose, and lignin as principal components, includes injecting the wood-based raw material into a dissolution reservoir in which ethylene glycol is stored as a separating agent, and heating the separating agent in the dissolution reservoir at atmospheric pressure to a temperature in a range of 260 C. to 280 C., and reacting the wood-based raw material with the separating agent, evaporating a hemicellulose component from the separating agent and condensing the hemicellulose component, and monitoring a pH value of the condensate of the hemicellulose component. A temperature of the condensate is held at the temperature at which a change in the pH value of the condensate decreases, lignin is dissolved in the separating agent, and crude cellulose that floats in the separating agent is separated and collected.
Efficient methods and compositions for recovery of products from organic acid pretreatment of plant materials
The invention is directed to compositions and processes concerning efficient downstream processing of products derived from organic acids pretreatment of plant materials.
METHOD FOR TREATING DISSOLVING PULP
The present invention relates to treatment of dissolving pulp with a lytic polysaccharide monooxygenase. The lytic polysaccharide monooxygenase treatment results in reduced viscosity and/or improved viscosity control in the dissolving pulp production process and/or 5 increased reactivity of the dissolving pulp.
A LIGNOCELLULOSIC BIOMASS BASED PROCESS FOR PRODUCTION OF LIGNINS AND SYNGAS, AND ELECTRICITY PRODUCTION EFFICIENT SYNGAS
A process for production of lignins and synthetic gas including the steps of extracting lignins and hemicellulose by putting solid Lignocellulosic Raw Material in contact with a mixture of water and formic acid at atmospheric pressure and at a temperature between 80 C. and 110 C.; fractionating, the primary solid fraction and the primary liquid fraction; separating the lignins from the intermediate liquid fraction; and gasifying at least part of said primary solid fraction and/or at least part of said residual liquid fraction for producing synthetic gas.
A LOW ENERGY PRODUCTION PROCESS FOR PRODUCING PAPER PULP FROM LIGNOCELLULOSIC BIOMASS
A low energy production process for producing paper pulp from lignocellulosic biomass, the process comprising the following successive steps: a) extracting lignins and hemicellulose from lignocellulosic biomass by putting at least one solid lignocellulosic raw material in the presence of a mixture, composed only of water and of formic acid, at atmospheric pressure and under controlled conditions of reaction temperature between ambient temperature and the reflux temperature of the mixture at atmospheric pressure, preferably between 80 C. and 100 C., with a weight ratio of the at least one solid lignocellulosic raw material/liquid mixture comprised between 1/1 and 1/15, and for a determined period of time of reaction; and b) separating, at atmospheric pressure and at the reaction temperature, a solid fraction, constituting raw paper pulp, from an organic phase containing in solution at least the starting formic acid and water mixture, solubilized monomeric and polymeric sugars, lignins.
Methods for the production of pulp and hemicellulose
In alternative embodiments, provided are methods and industrial processes for generating pulp from lignocellulosic feedstocks, comprising directly contacting a lignocellulosic feedstock with a system comprising a super critical or sub-super critical fluid or mixture of fluids, whereby the partial pressure of the system provides for the hydrolysis or a combination thereof of the feedstock at reduced temperatures and pressures, followed by an upgrading step wherein a low-purity cellulosic material generated in the super critical or sub-super critical reaction step is treated with an alkaline solution. In alternative embodiments, provided are systems and methods for producing a cellulose material using reduced amounts of water.
Tobacco-derived nanocellulose material
The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.
METHOD FOR PRODUCING DENSIFIED CELLULOSIC COMPOSITE MATERIAL
The present invention provides a method for obtaining densified material comprising the steps of
a. providing lignocellulosic material,
b. delignification of the lignocellulosic material providing a delignified material, wherein the delignification step is performed in such a way that the lignin of the lignocellulosic material is almost completely removed and wherein the structural integrity of the lignocellulosic material is maintained in the delignified material,
c. densification of the delignified material providing a densified material.
Furthermore, a densified material is provided. The fibers and fibrils are maintained in the structural directionality of the raw material and that the cellulosic material is whitish.