Patent classifications
D21C3/02
Method of digesting lignocellulosic material
A method of digesting lignocellulosic material includes the steps of providing the lignocellulosic material and a caustic composition having a pH of at least about 10. The caustic composition includes water, an alkaline- or alkaline earth-metal hydroxide, and up to about 1 percent by weight based on a total weight of the composition of a branched digestion additive. The branched digestion additive has the structure: wherein A is at least one alkyleneoxy group and each alkyleneoxy group has from 2 to 4 carbon atoms, n is 0 or 1, B is a branched aliphatic hydrocarbon group having from 8 to 15 carbon atoms, X is H or B-0-(A).sub.m, and each m is independently an average value from 3 to 30, and wherein the caustic composition has a Draves Wetting Time of less than 100 seconds as determined using ASTM D2281. ##STR00001##
Method of digesting lignocellulosic material
A method of digesting lignocellulosic material includes the steps of providing the lignocellulosic material and a caustic composition having a pH of at least about 10. The caustic composition includes water, an alkaline- or alkaline earth-metal hydroxide, and up to about 1 percent by weight based on a total weight of the composition of a branched digestion additive. The branched digestion additive has the structure: wherein A is at least one alkyleneoxy group and each alkyleneoxy group has from 2 to 4 carbon atoms, n is 0 or 1, B is a branched aliphatic hydrocarbon group having from 8 to 15 carbon atoms, X is H or B-0-(A).sub.m, and each m is independently an average value from 3 to 30, and wherein the caustic composition has a Draves Wetting Time of less than 100 seconds as determined using ASTM D2281. ##STR00001##
METHOD FOR PROCESSING STRAW
Described herein is a method for processing straw into an intermediate straw product. The method comprises: (a) treating straw with an alkaline solution having a p H of between about 10 and about 14, at a temperature of between about 20° C. and about 80° C., for a period of between about 6 hours and about 30 hours; (b) separating excess alkaline solution and the treated straw from each other; and (c) maintaining the treated straw in an anaerobic environment at a temperature of between about 30° C. and about 45° C., for a period of between about 6 hours and about 30 hours to produce an intermediate straw product. Also described is an intermediate product produced by the method; a method for extracting lignin from straw; lignin thereby produced; a method for extracting cellulose fibres from straw to produce paper pulp; cellulose fibres and paper pulp thereby produced; a method for producing a paper pulp product or a paper product; a product thereby produced; and a container and apparatus for processing straw according to the methods described.
METHOD FOR PROCESSING STRAW
Described herein is a method for processing straw into an intermediate straw product. The method comprises: (a) treating straw with an alkaline solution having a p H of between about 10 and about 14, at a temperature of between about 20° C. and about 80° C., for a period of between about 6 hours and about 30 hours; (b) separating excess alkaline solution and the treated straw from each other; and (c) maintaining the treated straw in an anaerobic environment at a temperature of between about 30° C. and about 45° C., for a period of between about 6 hours and about 30 hours to produce an intermediate straw product. Also described is an intermediate product produced by the method; a method for extracting lignin from straw; lignin thereby produced; a method for extracting cellulose fibres from straw to produce paper pulp; cellulose fibres and paper pulp thereby produced; a method for producing a paper pulp product or a paper product; a product thereby produced; and a container and apparatus for processing straw according to the methods described.
Method of processing and fractionating biomass and use of fractions thus obtained
The present invention relates to a method of treating biomass, comprising providing a lignocellulosic biomass feedstock; contacting the biomass feedstock in a mixture, which is formed by the biomass, water and an alkaline agent, with an oxidizing agent at an elevated temperature; and continuing the contacting of the biomass feedstock with the oxidizing agent until a notable part of the lignin is solubilised. The step of providing the biomass feedstock comprises contacting a biomass raw-material containing cellulose, hemicellulose and lignin in an aqueous phase with an alkaline agent; continuing the contacting of the biomass with the alkaline agent until a significant portion of the hemicellulose is dissolved in the aqueous phase to provide a modified biomass; recovering the modified biomass; optionally opening the structure of the modified biomass by mechanical treatment; and using the modified biomass as a lignocellulosic biomass feedstock. Treating the biomass provides hemicellulose, lignin and cellulose fractions that have a multitude of applications in the bioeconomy.
Method of processing and fractionating biomass and use of fractions thus obtained
The present invention relates to a method of treating biomass, comprising providing a lignocellulosic biomass feedstock; contacting the biomass feedstock in a mixture, which is formed by the biomass, water and an alkaline agent, with an oxidizing agent at an elevated temperature; and continuing the contacting of the biomass feedstock with the oxidizing agent until a notable part of the lignin is solubilised. The step of providing the biomass feedstock comprises contacting a biomass raw-material containing cellulose, hemicellulose and lignin in an aqueous phase with an alkaline agent; continuing the contacting of the biomass with the alkaline agent until a significant portion of the hemicellulose is dissolved in the aqueous phase to provide a modified biomass; recovering the modified biomass; optionally opening the structure of the modified biomass by mechanical treatment; and using the modified biomass as a lignocellulosic biomass feedstock. Treating the biomass provides hemicellulose, lignin and cellulose fractions that have a multitude of applications in the bioeconomy.
PREPARATION OF LACTIC ACID AND/OR A LACTATE SALT FROM LIGNOCELLULOSIC MATERIAL BY SEPARATE SACCHARIFICATION AND FERMENTATION STEPS
A process for preparing lactic acid and/or a lactate salt via the fermentation of carbohydrates obtained from lignocellulosic material. In particular the process includes: a) treating a lignocellulosic material with an alkaline agent including a caustic magnesium salt in the presence of water to provide a treated aqueous lignocellulosic material; b) saccharifying the treated aqueous lignocellulosic material in the presence of a hydrolytic enzyme to provide a saccharified aqueous lignocellulosic material including fermentable carbohydrates and a solid lignocellulosic fraction; c) fermenting the fermentable carbohydrates in the saccharified aqueous lignocellulosic material by way of lactic acid producing microorganism in the presence of an alkaline agent including a caustic magnesium salt to provide an aqueous fermentation broth including a magnesium lactate; and d) isolating lactic acid and/or lactate salt from the fermentation broth; wherein the saccharification step b) and the fermentation step c) are performed as two separate steps.
PREPARATION OF LACTIC ACID AND/OR A LACTATE SALT FROM LIGNOCELLULOSIC MATERIAL BY SEPARATE SACCHARIFICATION AND FERMENTATION STEPS
A process for preparing lactic acid and/or a lactate salt via the fermentation of carbohydrates obtained from lignocellulosic material. In particular the process includes: a) treating a lignocellulosic material with an alkaline agent including a caustic magnesium salt in the presence of water to provide a treated aqueous lignocellulosic material; b) saccharifying the treated aqueous lignocellulosic material in the presence of a hydrolytic enzyme to provide a saccharified aqueous lignocellulosic material including fermentable carbohydrates and a solid lignocellulosic fraction; c) fermenting the fermentable carbohydrates in the saccharified aqueous lignocellulosic material by way of lactic acid producing microorganism in the presence of an alkaline agent including a caustic magnesium salt to provide an aqueous fermentation broth including a magnesium lactate; and d) isolating lactic acid and/or lactate salt from the fermentation broth; wherein the saccharification step b) and the fermentation step c) are performed as two separate steps.
Process for refining fiber and deriving chemical co-products from biomass
The invention herein disclosed and claimed is a process for refining fiber from lignocellulosic biomass. The process provides refined fiber and agriculturally amenable co-products, with a virtually waste-free systems design.
Process for refining fiber and deriving chemical co-products from biomass
The invention herein disclosed and claimed is a process for refining fiber from lignocellulosic biomass. The process provides refined fiber and agriculturally amenable co-products, with a virtually waste-free systems design.