The application describes a process for the preparation of microcapsules, wherein the microcapsules have a volume average diameter d of 15 to 90 μηη and a percentage of the shell weight of 3 to 40%, with reference to the total weight of capsules, wherein the shell of the microcapsules comprises at least one polyurea and the core comprises at least one lipophilic component, comprising the step of adding hydroxyalkylcellulose to a dispersion of polyurea microcapsules, microcapsules and their uses.

A process for flocculating filler particles in water is provided. The process comprises adding a flocculant to a mixture comprising filler particles and water, wherein the flocculant has a reduced specific viscosity (“RSV”) of from about 5 dL/g to about 16 dL/g, a viscosity average molecular weight of from about 1,200,000 to about 7,500,000, and a cationic charge of from about 5 mol % to about 50 mol %. Flocs formed by flocculation of the filler particles and the flocculant have a median particle size of from about 10 um to about 150 um. The filler is not precipitated calcium carbonate alone. The flocs provided by the process are useful in increasing ash content of a paper product.

A process for flocculating filler particles in water is provided. The process comprises adding a flocculant to a mixture comprising filler particles and water, wherein the flocculant has a reduced specific viscosity (“RSV”) of from about 5 dL/g to about 16 dL/g, a viscosity average molecular weight of from about 1,200,000 to about 7,500,000, and a cationic charge of from about 5 mol % to about 50 mol %. Flocs formed by flocculation of the filler particles and the flocculant have a median particle size of from about 10 um to about 150 um. The filler is not precipitated calcium carbonate alone. The flocs provided by the process are useful in increasing ash content of a paper product.

Disclosed in one aspect is a pickled vegetable-based edible packaging paper, the raw material of which is composed of the following components in parts by weight: 92-95 parts of a high dietary fiber-level pickled vegetable, a compounding thickener (0.6-0.8 parts of pectin, 0.6-0.8 parts of potato starch, and 0.2-0.4 parts of soy protein), and a compounding plasticizer (3-4 parts of sorbitol, and 0.5-1.5 parts of citral); and further disclosed in another aspect is a method for preparing a pickled vegetable-based edible packaging paper. The pickled vegetable paper of the present invention is a novel pickled vegetable-based product having both edible and practical functions, which product is rich in dietary fibers, retains the unique flavor and color of the pickled vegetable, has toughness and non-stickiness to teeth, and is soft and easy to process after being wetted.

Disclosed in one aspect is a pickled vegetable-based edible packaging paper, the raw material of which is composed of the following components in parts by weight: 92-95 parts of a high dietary fiber-level pickled vegetable, a compounding thickener (0.6-0.8 parts of pectin, 0.6-0.8 parts of potato starch, and 0.2-0.4 parts of soy protein), and a compounding plasticizer (3-4 parts of sorbitol, and 0.5-1.5 parts of citral); and further disclosed in another aspect is a method for preparing a pickled vegetable-based edible packaging paper. The pickled vegetable paper of the present invention is a novel pickled vegetable-based product having both edible and practical functions, which product is rich in dietary fibers, retains the unique flavor and color of the pickled vegetable, has toughness and non-stickiness to teeth, and is soft and easy to process after being wetted.

Disclosed are multi-ply tissue products comprising a non-crosslinked binder that are durable, smooth and with low levels of Slough. In certain instances the creped tissue product have a geometric mean tensile (GMT) from about 700 to about 1,500 g/3″ a basis weight from about 45 to about 60 gsm and a Slough less than about 2.00 mg, more preferably less than about 1.50 mg, such as from about 0.10 to about 2.00, such as from about 0.25 to about 1.50 mg. The inventive tissue products also have good durability, such as a Durability Index from about 10.0 to about 20.0, smooth surfaces, such as a TS750 value from about 15.0 to 40.0 and low stiffness, such as a Stiffness Index less than about 10.0.

Disclosed are multi-ply tissue products comprising a non-crosslinked binder that are durable, smooth and with low levels of Slough. In certain instances the creped tissue product have a geometric mean tensile (GMT) from about 700 to about 1,500 g/3″ a basis weight from about 45 to about 60 gsm and a Slough less than about 2.00 mg, more preferably less than about 1.50 mg, such as from about 0.10 to about 2.00, such as from about 0.25 to about 1.50 mg. The inventive tissue products also have good durability, such as a Durability Index from about 10.0 to about 20.0, smooth surfaces, such as a TS750 value from about 15.0 to 40.0 and low stiffness, such as a Stiffness Index less than about 10.0.

The present invention relates to a process for the preparation of an aqueous polymer solution containing at least one cationic or amphoteric (co)polymer, comprising the following steps: Hofmann degradation reaction on a (co)polymer based on at least one non-ionic monomer chosen from the group including acrylamide, methacrylamide, N,N-dimethylacrylamide, and acrylonitrile; post-processing of the resulting aqueous polymer solution of viscosity V1; characterized in that the post processing comprises the following successive steps: obtaining of an aqueous polymer solution containing at least one cationic or amphoteric (co)polymer derived from the Hofmann degradation reaction; post-processing of this aqueous polymer solution; characterized in that the post processing comprises the following successive steps: (a) adjustment of the pH of the aqueous polymer solution to a value greater than or equal to 5.5; (b) decrease of the pH of the aqueous polymer solution to a value between 2 and 5. The invention also concerns the use of this polymer solution as a flocculant, retention and/or drainage agent, and dry strength resistance in a paper manufacturing process.

The present invention relates to a process for the preparation of an aqueous polymer solution containing at least one cationic or amphoteric (co)polymer, comprising the following steps: Hofmann degradation reaction on a (co)polymer based on at least one non-ionic monomer chosen from the group including acrylamide, methacrylamide, N,N-dimethylacrylamide, and acrylonitrile; post-processing of the resulting aqueous polymer solution of viscosity V1; characterized in that the post processing comprises the following successive steps: obtaining of an aqueous polymer solution containing at least one cationic or amphoteric (co)polymer derived from the Hofmann degradation reaction; post-processing of this aqueous polymer solution; characterized in that the post processing comprises the following successive steps: (a) adjustment of the pH of the aqueous polymer solution to a value greater than or equal to 5.5; (b) decrease of the pH of the aqueous polymer solution to a value between 2 and 5. The invention also concerns the use of this polymer solution as a flocculant, retention and/or drainage agent, and dry strength resistance in a paper manufacturing process.

The invention relates to a papermaking agent system in liquid form, which comprises (i) cationic starch solution, prepared by cooking a starch mixture comprising a starch component and a water component, and (ii) polymer composition, which has anionic and cationic groups and a cationic net charge of >0.1 meq/g. The polymer composition comprises or originates from at least one of constituents a), b) or c). Constituent a) contains an amphoteric polymer, which is a copolymer comprising structural units derived from acrylamide and/or methacrylamide monomers, and anionic and cationic groups attached to the copolymer. Constituent b) contains a first polymer, which is a copolymer comprising structural units derived from acrylamide and/or methacrylamide monomers, and anionic or cationic groups attached to the copolymer, as well as a second polymer, which comprises groups with opposite charge than the first polymer. Constituent c) contains a third polymer, which comprises a copolymer comprising structural units derived from acrylamide and/or methacrylamide monomers, as well as hydrolytically unstable cationic groups attached to the copolymer. Constituent a), b) or c) is added to one of the components of the starch mixture or to the starch mixture before the cooking of the starch mixture, and/or constituent a) or b) is added to the cationic starch solution after cooking of the starch mixture. The invention relates also to the use of the papermaking agent system and to a method for its preparation.