A method for a carbon nanofiber composite, which can obtain a carbon nanofiber composite with high productivity and high activity, and which does not require removal of fluidizing materials or dispersing materials, provides a carbon nanofiber composite having improved dispersibility. The method for producing the carbon nanofiber composite includes bringing at least one catalyst and at least one particulate carbon material into contact with at least one gas containing at least one gaseous carbon-containing compound while mechanically stirring the catalyst and the particulate carbon material in a reactor. The carbon nanofiber composite includes carbon nanofibers and at least one particulate carbon material, wherein the particulate carbon material has 70% by volume or more of particles with a particle diameter of 1 μm or less, and/or a median diameter D50 by volume of 1 μm or less.

A method of manufacturing a stabilized fiber bundle is described, which includes subjecting an acrylic fiber bundle aligned, to a heat treatment in an oxidizing atmosphere, with the acrylic fiber bundle being turned around by a guide roller placed on each of both ends outside a hot air heating-type oxidation oven, wherein an air velocity Vm of first hot air sent through a supply nozzle(s) disposed above and/or under a fiber bundle travelled in the oxidation oven, in a substantially horizontal direction to a travelling direction of the fiber bundle, and an air velocity Vf of second hot air flowing in a fiber bundle passing a flow channel in which the fiber bundle is travelled that satisfies expression 1)

0.2≤Vf/Vm≤2.0   1)

to produce a high-quality stabilized fiber bundle and a high-quality carbon fiber bundle at high efficiencies without any process troubles.

An oxidation furnace for the oxidative treatment of fibers having a housing which is gas-tight, apart from passage areas for the fibers, and a process chamber located in the interior of the housing. A hot working atmosphere can be generated by an atmosphere-generating device, can be blown into the process chamber and flows through the process chamber in processing conditions in a main direction of flow. Deflecting rollers guide the fibers through the process chamber in a serpentine manner in such a way that the fibers lie next to one another as a fiber carpet (22a), wherein the fiber carpet spans a plane between opposite deflecting rollers. A flow measuring system is provided, by means of which a flow profile of the working atmosphere in processing conditions can be generated, and which comprises at least one sensor system for determining the speed of flow, the sensor system being arranged in a sensor region between two adjacent fiber carpets.

An oxidation furnace for the oxidative treatment of fibers having a housing which is gas-tight, apart from passage areas for the fibers, and a process chamber located in the interior of the housing. A hot working atmosphere can be generated by an atmosphere-generating device, can be blown into the process chamber and flows through the process chamber in processing conditions in a main direction of flow. Deflecting rollers guide the fibers through the process chamber in a serpentine manner in such a way that the fibers lie next to one another as a fiber carpet (22a), wherein the fiber carpet spans a plane between opposite deflecting rollers. A flow measuring system is provided, by means of which a flow profile of the working atmosphere in processing conditions can be generated, and which comprises at least one sensor system for determining the speed of flow, the sensor system being arranged in a sensor region between two adjacent fiber carpets.

The invention relates to a furnace for the treatment of material, in particular for the oxidative treatment of fiber material, in particular for producing carbon fibers, comprising a housing (12) having, a housing inner space (14), which is gas-tight with the exceptions of passage areas (18, 20) for the fibers (22), In the housing hiller space (14) of the housing (12), a process chamber (28) is located. A hot working atmosphere (40) can be generated by means of an atmosphere device (42). The atmosphere device (42) comprises a flow system (46) having flow channels (48), which are arranged in the housing inner space (14) each defining, one flow chamber (50), and are provided with flow passages such that the respective flow chambers (50) are fluidically connected to the process chamber (28) in such a way that hot working atmosphere (40) can he delivered to the process chamber (28) in at least one main flow direction (44) and can be discharged from the process chamber (28). A revision system (72) is provided, through which flow chambers (50) of flow channels (48) are accessible through the housing (12).

The invention relates to a furnace for the treatment of material, in particular for the oxidative treatment of fiber material, in particular for producing carbon fibers, comprising a housing (12) having, a housing inner space (14), which is gas-tight with the exceptions of passage areas (18, 20) for the fibers (22), In the housing hiller space (14) of the housing (12), a process chamber (28) is located. A hot working atmosphere (40) can be generated by means of an atmosphere device (42). The atmosphere device (42) comprises a flow system (46) having flow channels (48), which are arranged in the housing inner space (14) each defining, one flow chamber (50), and are provided with flow passages such that the respective flow chambers (50) are fluidically connected to the process chamber (28) in such a way that hot working atmosphere (40) can he delivered to the process chamber (28) in at least one main flow direction (44) and can be discharged from the process chamber (28). A revision system (72) is provided, through which flow chambers (50) of flow channels (48) are accessible through the housing (12).

Compact module for wet spinning of chemical fibres of the type comprising a spinning head (F) of 2-8 tows (S), each one consisting of a plurality of continuous filaments, relative supply pumps (P) of the spinning solution, a coagulation tank (V) containing a coagulation solution, and a plurality of drive rollers (2) and respective idle diverter rollers (3) which determine a zigzag path of the tows (S) downstream of the spinning area, in the rectilinear lengths of which liquid-based treatments are carried out on said tows (S). The rectilinear lengths of said zigzag path are horizontal and said liquid-based treatments on the tows (S) are carried out in horizontal treatment trays (4) of the spillway type.

A method for producing a carbon material, the method including a step of performing a carbonization treatment by heating an organic polymer material to a temperature higher than 400° C. in a non-oxidizing atmosphere containing a gaseous substance (A) composed of at least one of acetylene and an acetylene derivative.

Systems and methods are provided for fabricating carbon nanostructures by low voltage near-field electromechanical spinning (LV-NFEMS). Processes described herein can produce ˜2-5 nm carbon nanowires with ultrahigh electrical conductivity using top-down and controlled reductive techniques from a polymer. Configurations are also provided to allow for deposition control and fiber elongation/alignment. One embodiment uses a low voltage near-field electromechanical spinning process to produce a polymer fiber from a polymer solution. Another embodiment of the method uses pyrolysis to convert the produced polymer fiber into a ˜2-5 nm carbon nanowire. System configurations provide advancements in polymer droplet control and control of a sustained jet of polymer solution with the use low voltages. Systems and processes described herein can include use of an array of polymer precursor nanofibers suspended onto a silicon substrate and converted to carbon nanowires. In another embodiment, ultra-thin carbon fibers can be integrated onto a carbon electrode scaffold.

A carbon fiber manufacturing method includes joining first and second target fiber bundles with a joining fiber bundle, and carbonizing the joined bundles by feeding them through one or more carbonization furnaces. The joining includes forming an overlap between a first end of the joining fiber bundle and a second end of the first target fiber bundle and jetting a fluid to the overlap to form a first entangled portion, and forming an overlap between a second end of the joining fiber bundle and a first end of the second target fiber bundle and jetting a fluid to the overlap to form a second entangled portion. When the first and second entangled portions each have two or more entangling points with a tensile strength not less than 400 N, the relationship defined by the inequality is satisfied: 40>{L2/(L2−A)}×(S+13), where L2 is a length (mm) of an elongation section inside a first carbonization furnace upstream in a feeding direction of the fiber bundles, A is a maximum distance (mm) between an entangling point in the first entangled portion and an entangling point in the second entangled portion, and S is an elongation (%) of the joined fiber bundles fed through the carbonization furnace.