An integrated and improved, single-step, process for the production of a carbon fiber precursor is described, specifically a process which starts from the comonomers and reaches the spinning step, obtaining the final precursor fiber.

In a first embodiment, a coal treatment process includes exposing a material comprising coal to ionic liquid(s) to form a first mixture, isolating a residue from the first mixture, forming a second mixture comprising the residue, and electrospinning the second mixture to form a carbon fiber precursor material. In a second embodiment, a coal treatment process includes exposing a material comprising coal to ionic liquid(s) to form a mixture comprising solids and a liquid fraction, separating and filtering the liquid fraction from the mixture, and isolating one or more compounds from the liquid fraction. In a third embodiment, a coal treatment process includes exposing a material comprising coal to ionic liquid(s) to form a first mixture comprising residues, exposing the first mixture to (a) an acid, (b) a solvent, or (c) both to form a second mixture, and isolating rare earth elements and rare earth element compounds.

Disclosed is a treatment agent for flame-resistant fiber nonwoven fabric production or for carbon fiber nonwoven fabric production. The treatment agent contains a polyether compound in which ethylene oxide and propylene oxide are added to an alcohol. Also disclosed is a flame-resistant fiber nonwoven fabric or carbon fiber nonwoven fabric that includes the treatment agent adhered thereto.

Disclosed is a treatment agent for flame-resistant fiber nonwoven fabric production or for carbon fiber nonwoven fabric production. The treatment agent contains a polyether compound in which ethylene oxide and propylene oxide are added to an alcohol. Also disclosed is a flame-resistant fiber nonwoven fabric or carbon fiber nonwoven fabric that includes the treatment agent adhered thereto.

The present disclosure provides compositions including a carbon fiber material comprising one or more of dibromocyclopropyl or polysilazane disposed thereon; and a thermosetting polymer or a thermoplastic polymer. The present disclosure further provides metal substrates including a composition of the present disclosure disposed thereon. The present disclosure further provides vehicle components including a metal substrate of the present disclosure. The present disclosure further provides methods for manufacturing a vehicle component, including contacting a carbon fiber material with a polysilazane or a dibromocarbene to form a coated carbon fiber material; and mixing the coated carbon fiber material with a thermosetting polymer or a thermoplastic polymer to form a composition. Methods can further include depositing a composition of the present disclosure onto a metal substrate.

The present disclosure provides compositions including a carbon fiber material comprising one or more of dibromocyclopropyl or polysilazane disposed thereon; and a thermosetting polymer or a thermoplastic polymer. The present disclosure further provides metal substrates including a composition of the present disclosure disposed thereon. The present disclosure further provides vehicle components including a metal substrate of the present disclosure. The present disclosure further provides methods for manufacturing a vehicle component, including contacting a carbon fiber material with a polysilazane or a dibromocarbene to form a coated carbon fiber material; and mixing the coated carbon fiber material with a thermosetting polymer or a thermoplastic polymer to form a composition. Methods can further include depositing a composition of the present disclosure onto a metal substrate.

A manufacturing method for a carbon fiber includes the following steps. A first monomer and a second monomer are dissolved in a first solvent, and a polymerization reaction is performed to form a copolymerized polymer, in which the first monomer includes acrylonitrile, the second monomer has an unsaturated bond, the first solvent includes dimethyl sulfoxide, and based on 100 wt % of the first solvent, a content of the dimethyl sulfoxide is between 99.9 wt % and 100 wt %. A spinning step is performed on the copolymerized polymer.

A manufacturing method for a carbon fiber includes the following steps. A first monomer and a second monomer are dissolved in a first solvent, and a polymerization reaction is performed to form a copolymerized polymer, in which the first monomer includes acrylonitrile, the second monomer has an unsaturated bond, the first solvent includes dimethyl sulfoxide, and based on 100 wt % of the first solvent, a content of the dimethyl sulfoxide is between 99.9 wt % and 100 wt %. A spinning step is performed on the copolymerized polymer.

The invention relates to a method and to a device for stabilizing precursor fibers for the production of carbon fibers. In the method, precursor fibers are first heated to a first temperature and held at the temperature for a predefined duration. Subsequently, the precursor fibers are heated to at least one second temperature, which is higher than the first temperature, and held at said temperature for a predefined duration. During each heating and between the heating steps, the precursor fibers are in a gas atmosphere having a negative pressure in the range between 12 mbar and 300 mbar and having an oxygen partial pressure of 2.5 to 63 mbar. The device has at least one evacuable, elongate vacuum chamber for feeding the precursor fibers through, at least two lock units and at least one heating unit. At least one lock unit is used for the sealed insertion of precursor fibers into the at least one vacuum chamber, while at least one other lock unit is used for the sealed removal of precursor fibers from the at least one vacuum chamber. The heating unit has at least two individually controllable heating elements, which are suitable for heating the at least one vacuum chamber to at least two different temperatures in heating zones which are adjacent in the longitudinal direction.

Provided is a carbon fiber with a strand modulus of elasticity from 240 to 300 GPa, an elongation of 2.65% or more, and a strain energy density of 95 J/mm.sup.3 or more, which can improve the impact resistance of carbon fiber composite materials.