A nitrogen recovery apparatus for recovering nitrogen from natural gas comprises a separator having a liquid fraction port and a vapour fraction port in fluid communication with a split flow arrangement, the split flow arrangement having a sub-cooled fluid path and an expanded fluid path. A fractionating column has a reflux inlet port in fluid communication with the subcooled fluid path above a middle feed port thereof, the middle feed port being in fluid communication with the expanded fluid path. A bottom feed port of the fractionating column is in fluid communication with the liquid fraction port of the separator. A side reboiler circuit and a reboiler circuit are operably coupled to the fractionating column below the bottom feed port. A bottom hydrocarbon product stream path is in fluid communication with a bottom hydrocarbon port of the fractionating column.

The present invention relates to a method of cooling and separating a hydrocarbon stream: (a) passing an hydrocarbon feed stream (7) through a first cooling and separation stage to provide a methane enriched vapour overhead stream (110) and a methane depleted liquid stream (10); (b) passing the methane depleted liquid stream (10) to a fractionation column (200) to obtain a bottom condensate stream (210), a top stream enriched in C1-C2 (220) and a midstream enriched in C3-C4 (230), (c) cooling the upper part of the fractionation column (201) by a condenser (206), (d) obtaining a split stream (112) from the methane enriched vapour overhead stream (110) and obtaining a cooled split stream (112) by expansion-cooling the split stream (112), (e) providing cooling duty to the top of the fractionation column (201) using the cooled split stream (112).

A system and method for removing nitrogen and producing a high pressure methane product stream and an NGL product stream from natural gas feed streams where at least 90%, and preferably at least 95%, of the ethane in the feed stream is recovered in the NGL product stream. The system and method of the invention are particularly suitable for use with feed streams in excess of 5 MMSCFD and up to 300 MMSCFD and containing around 5% to 80% nitrogen. The system and method preferably combine use of strategic heat exchange between various process streams with a high pressure rectifier tower and the ability to divert all or a portion of a nitrogen rejection unit feed stream to optionally bypass a nitrogen fractionation column to reduce capital costs and operating expenses.

A system and method for removing nitrogen and producing a high pressure methane product stream and an NGL product stream from natural gas feed streams where at least 90%, and preferably at least 95%, of the ethane in the feed stream is recovered in the NGL product stream. The system and method of the invention are particularly suitable for use with feed streams in excess of 5 MMSCFD and up to 300 MMSCFD and containing around 5% to 80% nitrogen. The system and method preferably combine use of strategic heat exchange between various process streams with a high pressure rectifier tower and the ability to divert all or a portion of a nitrogen rejection unit feed stream to optionally bypass a nitrogen fractionation column to reduce capital costs and operating expenses.

Enhancements to a dual column, nitrogen producing cryogenic air separation unit are provided. Such enhancements include an improved air separation cycle that uses multiple condenser-reboilers and recycles a portion of the vapor from one or more of the condenser-reboilers to the incoming feed stream and or the compressed purified air streams to yield improvements in such dual column, nitrogen producing cryogenic air separation units. The multiple condenser-reboilers preferably include an integrated condenser-reboiler arrangement comprising a heat exchanger having a set of nitrogen condensing passages, a first set and second set of boiling passages, and a phase separator.

Process and apparatus for the separation of a compressed feed air stream to produce an oxygen product using a distillation column having a lower-pressure column and a higher-pressure column, a higher-pressure heat exchanger and a lower-pressure heat exchanger where the gaseous nitrogen expander receives a nitrogen-enriched fraction from a position intermediate the warmer end and the colder end of the higher-pressure heat exchanger.

A system for conditioning a sour gas feed stream for a cryogenic distillation tower. A dehydration unit separates the sour gas feed stream into a first stream including water and a feed stream. A sequential cooling assembly is coupled to both the dehydration unit and the cryogenic distillation tower. The sequential cooling assembly includes: a first stage that separates the feed stream into a partially cooled feed stream and a second stream including acid gas; a second stage that cools the partially cooled feed stream into a cooled feed stream and a third stream including acid gas; and a cooled feed stream header coupled to a cryogenic distillation tower feed inlet. The first stage, the second stage, or both send at least one of the second and third streams to a bottom section of the cryogenic distillation tower.

A process for producing an olefin having N carbon atoms is proposed in which using a dehydrogenation a process gas is formed which contains at least the olefin having N carbon atoms, a paraffin having N carbon atoms and a hydrocarbon having N1 carbon atoms and in which using at least a portion of the process gas a separation input is formed which is subjected to a low temperature separation in which the separation input is cooled stepwise over a plurality of temperature levels and condensates are separated from the separation input, wherein the condensates are at least partly subjected to a first low temperature rectification to obtain a first gas fraction and a first liquid fraction, wherein the first gas fraction contains at least the olefin having N carbon atoms in a lower proportion than in the condensates and the hydrocarbon having N1 in a higher proportion than in the condensates. It is provided that the first gas fraction is at least partly subjected to a second low temperature rectification using a liquid reflux containing predominantly or exclusively the hydrocarbon having N1 carbon atoms in which the first gas fraction undergoes depletion in the olefin having N carbon atoms. A corresponding plant (100) likewise forms part of the subject matter of the invention.

A moderate pressure air separation unit and air separation cycle is disclosed that provides for up to about 96% recovery of argon, an overall nitrogen recovery of 98% or greater and limited gaseous oxygen production. The air separation is configured to produce a first high purity oxygen enriched stream and a second lower purity oxygen enriched stream from the lower pressure column, one of which is used as the refrigerant to condense the argon in the argon condenser, with the resulting vaporized oxygen stream used to regenerate the temperature swing adsorption pre-purifier unit. All or a portion of the first high purity oxygen enriched stream is vaporized in the main heat exchanger to produce the gaseous oxygen products.

A portion of feed air is expanded and cooled in front of a main heat exchanger, and is used as cold for precooling the remaining unexpanded feed air inside the main heat exchanger. A portion of the feed air precooled inside the main heat exchanger is removed to outside the main heat exchanger, expanded and cooled, and used as cold to cool the remaining unexpanded precooled feed air inside the main heat exchanger.