F25J2200/72

NITROGEN PROCESS FOR PRODUCTION OF AMMONIA AND LIQUID HYDROGEN

A method of co-producing liquid hydrogen and ammonia, including a hydrogen generator, a nitrogen generator, and a HLU is presented. The method includes pressurizing a hydrogen stream from the hydrogen generator in a hydrogen compressor, dividing the pressurized hydrogen into at least a first portion and a second portion, wherein the first portion includes at least part of the flow of a first refrigeration cycle in the HLU, and the second part comprises at least part of the feed to an ammonia plant. The method also includes pressurizing a nitrogen stream from the nitrogen generator in a HP nitrogen compressor, dividing the pressurized nitrogen stream into at least a first part and a second part, wherein the first part comprises at least part of the flow of a second refrigeration cycle in the HLU, and the second part comprises at least part of the feed to the ammonia plant.

METHOD FOR RECYCLING ARGON
20210310733 · 2021-10-07 · ·

A method for recycling argon from an industrial process; in which the gaseous argon is compressed after the use thereof in the industrial process, is fed to a main heat exchanger and is cooled there in contact with a first cooling medium. The compressed and cooled argon is fed to a rectification column or another cryogenic separating device and is liquefied there by direct heat exchange with a second cooling medium and is freed of low-boiling substances by rectification. The liquefied argon is drawn from the bottom of the rectification column and, after use as the first cooling medium in the main heat exchanger, is fed back into the industrial process, the raw argon being brought into thermal contact with cryogenically liquefied pure argon in the main heat exchanger and/or the rectification column. The product argon that results is highly pure and can be fed back to the industrial process.

METHOD FOR PRODUCING A SEPARATION PRODUCT CONTAINING PREDOMINANTLY HYDROCARBONS WITH TWO CARBON ATOMS

The invention relates to a method (100) for the recovery of a separation product which contains predominantly hydrocarbons with two carbon atoms, with the use of a separation feedstock which contains predominantly methane, hydrogen and hydrocarbons with two carbon atoms, wherein the methane content of the separation feedstock is up to 20%, and the separation feedstock is provided in a gaseous state. It is provided that, at a first pressure level, the separation feedstock is partially condensed in a single step by cooling from a first temperature level to a second temperature level, thereby obtaining precisely one first liquid fraction and precisely one first gaseous fraction; at least one part of the first gaseous fraction is partially condensed in a single step through further cooling from the second temperature level to a third temperature level, thereby obtaining precisely one second liquid fraction and precisely one second gaseous fraction; at least one part of the second gaseous fraction at the second pressure level is subjected to a contraflow absorption in the contraflow to an absorption liquid containing predominantly methane, thereby obtaining precisely one third liquid fraction and precisely one third gaseous fraction; the first, the second and the third liquid fraction are at least partially combined and, at least partially, at a second pressure level above the first pressure level, subjected to a low-temperature rectification, thereby obtaining a sump liquid and an overhead gas; at least one part of the overhead gas at the second pressure level is partially condensed in a single step through further cooling from the second temperature level to the third temperature level, thereby obtaining a fourth liquid fraction and a fourth gaseous fraction; and the absorption liquid containing predominantly methane is formed through further cooling of at least a part of the fourth gaseous fraction to a fourth temperature level. A corresponding plant also forms the subject matter of the invention.

System and method for separating natural gas liquid and nitrogen from natural gas streams
11125497 · 2021-09-21 · ·

A system and method for removing nitrogen and producing a high pressure methane product stream and an NGL product stream from natural gas feed streams where at least 90%, and preferably at least 95%, of the ethane in the feed stream is recovered in the NGL product stream. The system and method of the invention are particularly suitable for use with feed streams in excess of 5 MMSCFD and up to 300 MMSCFD and containing around 5% to 80% nitrogen. The system and method preferably combine use of strategic heat exchange between various process streams with a high pressure rectifier tower and the ability to divert all or a portion of a nitrogen rejection unit feed stream to optionally bypass a nitrogen fractionation column to reduce capital costs and operating expenses.

Method and system for obtaining one or more olefins

The invention relates to a method (100, 200) of obtaining one or more olefins, in which, using an oxidative coupling of methane (10), a gas mixture comprising hydrogen, methane, carbon monoxide and higher-boiling hydrocarbons than methane is formed and is subjected to a low-temperature separation (1-5), characterized in that the low-temperature separation (1-5) is conducted using a rectification column (2) having a first separation region (21), a second separation region (22) arranged above the first separation region (21), and a condenser-evaporator (23), wherein the gas mixture is cooled, fed at least partly as first separation feed into the first separation region (21) and subjected to a first rectification in the first separation region (21) to form a first tops gas and a first bottoms liquid, wherein, using a first proportion of the first tops gas in the condenser-evaporator (23), a condensate which is recycled to the first separation region and, using a second proportion of the tops gas, a second separation feed which is fed into the second separation region (22) are formed, and wherein the second separation feed is subjected to a second rectification in the second separation region to form a second tops gas and a second bottoms liquid.

Methods and Systems for Separating Compounds

Methods and systems for separating a desublimatable compound from hydrocarbons is disclosed. A feed fluid stream, consisting of a hydrocarbon and a desublimatable compound, is passed into an upper chamber of a vessel. The feed fluid stream is cooled in the upper chamber, thereby desublimating a portion of the desublimatable compound out of the feed liquid stream to form a product gas stream and a desublimatable compound snow which is collected in the lower chamber of the vessel. A lower portion of the desublimatable compound snow is melted to form a liquid desublimatable compound stream such that an upper portion of the solid desublimatable compound snow remains as an insulative barrier between the upper chamber and the liquid desublimatable compound stream. The liquid desublimatable compound stream is removed at a rate that matches a production rate of the solid desublimatable compound snow, thereby maintaining the insulative barrier.

CRYOGENIC PROCESS FOR REMOVING NITROGEN FROM A DISCHARGE GAS
20210172677 · 2021-06-10 ·

A process for producing biomethane by scrubbing a biogas feed stream including introducing a feed gas stream into a pretreatment unit wherein the gas stream is partially separated from a CO.sub.2 stream and an oxygen stream, thereby producing a CO.sub.2-depleted gas stream, which is compressed, thereby producing a pressurized CO.sub.2-depleted gas stream; separating the pressurized CO.sub.2-depleted gas stream by cryogenic separation by introducing the pressurized CO.sub.2-depleted gas stream into a distillation column thereby producing a nitrogen stream and a CH.sub.4-enriched stream, recovering a pressurized CH.sub.4-enriched stream by pumping the CH.sub.4-enriched stream; wherein the separation of the CO.sub.2 stream and the oxygen stream from the feed gas stream is performed by a unit comprising at least two separating membrane stages in order that the CO.sub.2-depleted gas stream comprises between 0.3 mol % and 2 mol % of CO.sub.2.

LNG Production with Nitrogen Removal

A method and system for liquefying a natural gas feed stream and removing nitrogen therefrom.

SYSTEMS AND RELATED METHODS FOR SEPARATING NITROGEN FROM A NATURAL GAS STREAM CONTAINING LESS THAN 25% NITROGEN
20210270524 · 2021-09-02 · ·

A method for separating nitrogen from an inlet gas having less than 25 mole % nitrogen includes supplying the inlet gas having less than 25 mole % nitrogen to a nitrogen separation system configured with cryogenic refrigeration.

System and Method for Separating Methane and Nitrogen with Reduced Horsepower Demands
20210180863 · 2021-06-17 ·

A system and method for removing nitrogen from natural gas using two fractionating columns, that may be stacked, and a plurality of separators and heat exchangers, with horsepower requirements that are 50-80% of requirements for prior art systems. The fractionating columns operate at different pressures. A feed stream is separated with a vapor portion feeding the first column to produce a first column bottoms stream that is split into multiple portions at different pressures and first column overhead stream that is cooled and separated into vapor and liquid portions to control subcooling of the vapor portion prior to feeding the second column. Heat exchange between first column and second column streams provides first column reflux and reboil heat for a second column ascending vapor stream. Three sales gas streams are produced, each at a different pressure.