F25J2200/78

Method and apparatus for separating air by cryogenic distillation

The invention relates to a method for separating air by cryogenic distillation in a column system, comprising a first column operating at a first pressure and a second column operating at a second pressure, in which an argon-enriched flow is sent from an intermediate point of the first column to the tank of the second column and an argon-rich flow is drawn off at the top of the second column, wherein a nitrogen-enriched flow of the first column is compressed in a compressor, the compressed flow is sent to a head condenser of the second column after an expansion step and the vaporized flow is expanded in the condenser in a turbine where it at least partially liquefies.

Pretreatment of natural gas prior to liquefaction

Method and system for removing high freeze point components from natural gas. Feed gas is cooled in a heat exchanger and separated into a first vapor portion and a first liquid portion. The first liquid portion is reheated using the heat exchanger and separated into a high freeze point components stream and a non-freezing components stream. A portion of the non-freezing components stream may be at least partially liquefied and received by an absorber tower. The first vapor portion may be cooled and received by the absorber tower. An overhead vapor product which is substantially free of high freeze point freeze components and a bottoms product liquid stream including freeze components and non-freeze components are produced using the absorber tower.

Method and apparatus for separating hydrocarbons

The claimed invention provides a method and an apparatus for separating hydrocarbons, wherein the method and the apparatus are used for separating a hydrocarbon having 3 or more carbon atoms including at least propane (hereinafter sometimes called “C3+ NGL”. NGL: Natural Gas Liquid) from liquefied natural gas (LNG).

Systems and processes for upgrading natural gas liquids from shale gas
11402153 · 2022-08-02 · ·

Systems and processes for upgrading natural gas liquids (NGL). A natural gas, preferably a shale gas, comprising methane and one or more natural gas liquids can be converted to one or more liquid hydrocarbons. Methane can be separated from the one or more liquid hydrocarbons using a liquid absorbent to provide a first separated stream comprising the methane from the converted stream and a second separated stream comprising the one or more liquid hydrocarbons from the converted stream. At least a portion of the one or more liquid hydrocarbons can be recycled as the liquid absorbent.

Hydrocarbon gas processing

A process and an apparatus are disclosed for separation of a hydrocarbon gas stream containing methane and heavier hydrocarbons and significant quantities of nitrogen and carbon dioxide. The gas stream is cooled and expanded, then fractionated in a first distillation column into a first overhead vapor and a hydrocarbon liquid stream containing the majority of the carbon dioxide. The hydrocarbon liquid stream is fractionated into a hydrocarbon vapor stream and a less volatile fraction comprised of heavier hydrocarbons. The first overhead vapor is cooled, expanded, and separated into vapor and liquid streams. Both streams are cooled and expanded before feeding a second distillation column that produces a second overhead vapor that is predominantly nitrogen and a bottom liquid that is predominantly methane. The bottom liquid is vaporized and combined with the hydrocarbon vapor stream to form a volatile residue gas fraction containing the majority of the methane.

Apparatus for separation and recovery of hydrocarbons from LNG

Provided are an apparatus and a method for separation and recovery of propane and heavier hydrocarbons from LNG. The apparatus has, from the upstream side toward the downstream side of LNG supply, first column (3) equipped with first column overhead condenser (2), first column bottom reboiler (4) and side reboiler (5), and second column (14) equipped with second column overhead condenser (11) and second column bottom reboiler (15). The first column (3) separates methane and a part of ethane as an overhead vapor and separates remaining ethane and C3 or higher hydrocarbons as a bottom liquid. The second column (14) separates ethane as an overhead vapor and separates C3 or higher hydrocarbons as a bottom liquid.

METHOD FOR PRODUCING A SEPARATION PRODUCT CONTAINING PREDOMINANTLY HYDROCARBONS WITH TWO CARBON ATOMS

The invention relates to a method (100) for the recovery of a separation product which contains predominantly hydrocarbons with two carbon atoms, with the use of a separation feedstock which contains predominantly methane, hydrogen and hydrocarbons with two carbon atoms, wherein the methane content of the separation feedstock is up to 20%, and the separation feedstock is provided in a gaseous state. It is provided that, at a first pressure level, the separation feedstock is partially condensed in a single step by cooling from a first temperature level to a second temperature level, thereby obtaining precisely one first liquid fraction and precisely one first gaseous fraction; at least one part of the first gaseous fraction is partially condensed in a single step through further cooling from the second temperature level to a third temperature level, thereby obtaining precisely one second liquid fraction and precisely one second gaseous fraction; at least one part of the second gaseous fraction at the second pressure level is subjected to a contraflow absorption in the contraflow to an absorption liquid containing predominantly methane, thereby obtaining precisely one third liquid fraction and precisely one third gaseous fraction; the first, the second and the third liquid fraction are at least partially combined and, at least partially, at a second pressure level above the first pressure level, subjected to a low-temperature rectification, thereby obtaining a sump liquid and an overhead gas; at least one part of the overhead gas at the second pressure level is partially condensed in a single step through further cooling from the second temperature level to the third temperature level, thereby obtaining a fourth liquid fraction and a fourth gaseous fraction; and the absorption liquid containing predominantly methane is formed through further cooling of at least a part of the fourth gaseous fraction to a fourth temperature level. A corresponding plant also forms the subject matter of the invention.

Process and device for the cryogenic separation of synthesis gas
11125496 · 2021-09-21 · ·

The invention relates to a process and device for the cryogenic separation of a methane-containing feed gas predominantly consisting of hydrogen and carbon monoxide, that is partially condensed in this case by cooling, in order to obtain a hydrogen-containing first liquid phase predominantly consisting of carbon monoxide and methane, from which first liquid phase, in an H.sub.2 separation column that is heated via a circulation heater, a second liquid phase is generated by separating off hydrogen, from which second liquid phase, in a CO/CH.sub.4 separation column, a carbon monoxide-rich gas phase is obtained having a purity that permits release thereof as carbon monoxide product. It is characteristic in this case that a low-methane material stream is withdrawn from the H.sub.2 separation column and is then applied to the CO/CH.sub.4 separation column as reflux.

System and method for separating natural gas liquid and nitrogen from natural gas streams
11125497 · 2021-09-21 · ·

A system and method for removing nitrogen and producing a high pressure methane product stream and an NGL product stream from natural gas feed streams where at least 90%, and preferably at least 95%, of the ethane in the feed stream is recovered in the NGL product stream. The system and method of the invention are particularly suitable for use with feed streams in excess of 5 MMSCFD and up to 300 MMSCFD and containing around 5% to 80% nitrogen. The system and method preferably combine use of strategic heat exchange between various process streams with a high pressure rectifier tower and the ability to divert all or a portion of a nitrogen rejection unit feed stream to optionally bypass a nitrogen fractionation column to reduce capital costs and operating expenses.

Phase implementation of natural gas liquid recovery plants
11112175 · 2021-09-07 · ·

Embodiments relate generally to systems and methods for operating a natural gas liquids plant in ethane rejection and in ethane recovery. A natural gas liquid plant may comprise an absorber configured to produce an ethane rich bottom stream and an ethane depleted vapor stream; a stripper fluidly coupled to the absorber configured to, during ethane rejection, fractionate the ethane rich bottom stream from the absorber into an ethane overhead product and a propane plus hydrocarbons product, and configured to, during ethane recovery, fractionate the ethane rich bottom stream into an ethane plus NGL stream and an overhead vapor stream; and an exchanger configured to, during ethane recovery, counter-currently contact the ethane rich bottom stream from the absorber with the ethane depleted vapor stream from the absorber, thereby heating the vapor stream and chilling the ethane rich bottom stream before the ethane rich bottom stream is fed to the stripper.