F25J2215/30

SYSTEM AND METHOD FOR RECOVERY OF NEON AND HELIUM FROM AN AIR SEPARATION UNIT

A system and method for neon recovery in a double column or triple column air separation unit is provided. The neon recovery system comprises a non-condensable stripping column configured to produce a liquid nitrogen-rich liquid column bottoms and a non-condensable gas containing overhead and one or more condensing units arranged to produce a crude neon vapor stream that contains greater than about 50% mole fraction of neon with the overall neon recovery exceeding 95%. In addition, there is minimal liquid nitrogen consumption and since much of the liquid nitrogen is recycled back to the lower pressure column of the air separation unit, there is minimal impact on the recovery of other products from the air separation unit.

Treatment of nitrogen-rich natural gas streams

Helium can be recovered from nitrogen-rich natural gas at high pressure with low helium loss by cryogenic distillation of the natural gas after pre-treatment of the gas to remove incompatible impurities and then recovery of natural gas liquid (NGL) from the pre-treated gas by distillation. Overall power consumption may be reduced, particularly if the feed to the helium recovery column system is at least substantially condensed by indirect heat exchange against a first portion of nitrogen-enriched bottoms liquid at first pressure, and a second portion of nitrogen-enriched bottoms liquid at a second pressure that is different from the first pressure.

Recovery Of Helium From Nitrogen-Rich Streams

Overall power consumption in a cryogenic distillation process for recovering helium from nitrogen-rich gases comprising helium may be reduced if the feed to the distillation column system is at least substantially condensed by indirect heat exchange against a first bottoms liquid at first pressure, and a second bottoms liquid at a second pressure that is different from the first pressure.

METHOD AND APPARATUS FOR SEPARATION OF HELIUM-3 FROM HELIUM-4 BY MEANS OF A CRYOGENIC PROCESS
20240261731 · 2024-08-08 ·

The invention provides a method for recovering 3-Helium (3He) from natural Helium (He), comprising the following steps: supplying the feed stream comprising natural liquid helium from an appropriate liquid helium source; introducing a feed stream into a rectification column system; condensing at least a first portion of a vapour stream comprising 3He enriched Helium in the intermediate section of the rectification system, condensing at least a second portion of a vapour stream comprising 3He enriched Helium in the upper section of the rectification system by heat exchange with colder liquid Helium; merging and compressing of the low-pressure vaporous streams; withdrawing an overhead stream comprising 3He enriched Helium from a top section of the rectification system as a product; withdrawing a bottom stream comprising 3He depleted Helium from a bottom section of the rectification system; withdrawing of a vaporous helium stream from the lower part of the rectification system.

Cryocooler-based gas scrubber

A cryocooler-based gas scrubber, or cryocooler-based gas purifier, utilizes the cooling power of a cryocooler to cool and condense cryogen gas forming coalesced impurities which are then filtered through a filter matrix, such as for example a fiberglass filter matrix. The scrubber may further comprise a counter-flow heat exchanger for warming the purified gas prior to dispensing at an outlet for storage or consumption.

PRODUCTION OF HELIUM FROM A GAS STREAM CONTAINING HYDROGEN
20180238618 · 2018-08-23 ·

The invention relates to a method for producing helium from a source gas stream (1) including at least helium, methane, nitrogen and hydrogen, comprising at least the following consecutive steps: step a): injecting said source gas stream (1) into at least one compressor (3); step b): eliminating the hydrogen and the methane by reacting the stream (4) obtained from step a) with oxygen; step c): eliminating at least the impurities from step b) by temperature swing adsorption (TSA); step d): partially condensing the stream (8) obtained from step c) in order to produce a stream (10) of liquid nitrogen and a gas stream (11) comprising mostly helium; step e): purifying the gas stream (11) obtained from step d) in order to increase the helium content by pressure swing adsorption (PSA) by eliminating the nitrogen and the impurities contained in the gas stream (11) obtained from step d).

METHOD FOR COOLING A PROCESS FLOW
20180202712 · 2018-07-19 ·

A method of cooling a process stream with an auxiliary stream is described, wherein the exchange of heat between the process stream and the auxiliary stream is effected in a first heat exchanger and a second heat exchanger connected downstream thereof.

HELIUM SEPARATION AND RECOVERY PROCESS

The present provides a helium gas separation and recovery process involving cryogenic fractionation process, which comprises cooling a dehydrated high-pressure gas stream while maintain velocity and pressure of the stream; reducing pressure of the dehydrated high-pressure gas stream via a Joule-Thompson's process to obtain a partially liquefied gas stream; and iii) subjecting the partially liquefied gas stream to at least one gas-liquid separation process to obtain at least one liquid stream and a gaseous stream comprising helium, and a residual amount of the gaseous components; recycling the liquid stream obtained in step iii) for use as cooling refrigerant to cool the dehydrated high-pressure gas stream; and purifying the unrefined helium gas stream using pressure swing adsorption (PSA) and/or membrane separation process to obtain a helium product stream having a purity of 98.0 mole % or more.

Cryogenic Neon Purification System and Method
20250003677 · 2025-01-02 ·

A feed gas including neon, nitrogen, and helium is cooled in a heat exchange system to a first temperature to produce a two-phase mixture that is introduced into a first phase separator and separated into a nitrogen-rich liquid and a first gaseous crude neon stream. The pressure is reduced in at least a portion of the nitrogen-rich liquid, which is vaporized in the heat exchange system to generate a portion of the refrigeration therein. The first gaseous crude neon stream is introduced into a first adsorber that removes impurities such as nitrogen. The gaseous crude neon stream is further cooled to a second temperature. A portion of the cooling duty may come from the heat exchange system and another portion may come from a cryocooler to produce a two-phase stream. The two-phase stream is separated in a second phase separator into a crude helium vapor stream and a crude neon liquid stream with the latter being introduced into a distillation column to produce a vent stream containing a helium impurity and a pure liquid neon product. The pure liquid neon product is vaporized in the heat exchange system to generate refrigeration and produce the pure gaseous neon product.

Cryogen chamber with adsorber

Disclosed is a segregating gas arrangement that generally comprises a gas segregation chamber, at least one cooling plate in the gas segregation chamber, and a carbon adsorber in an adsorption gas capturing chamber. The gas segregation chamber has a rim that when resting atop regolith defines a first interior environment. The cooling plates are in the gas segregation chamber, wherein the cooling plates are maintained at a first temperature above 5 K, which is a condensation temperature that higher temperature condensing gases will condense. The adsorption gas capturing chamber defines a second interior environment that is in communication with the first interior environment. The carbon adsorber is in the second interior environment and is maintained at a second temperature below 3 K. The carbon adsorber is configured to capture the low temperature condensing gas.