F25J2245/40

METHOD AND APPARATUS FOR SEPARATING AIR BY CRYOGENIC DISTILLATION

In a method for separating air by cryogenic distillation using a column system consisting of a higher pressure column operating at a first pressure and a lower pressure column operating at a second pressure, a first air flow constituting between 75% and 98% of the air sent to the column system compressed to a third pressure above the first pressure, is sent to the higher pressure column, a second air flow constituting between 5% and 25% of the air sent to the column system is compressed to a fourth pressure above the second pressure but lower than the third pressure, is sent to the lower pressure column, a third column separates an argon-enriched flow and the air sent to the lower pressure column constitutes between 10% and 25% of the total air sent to the column system.

PROCESS FOR SUPPLYING OXYGEN AND/OR NITROGEN AND ALSO ARGON TO A GEOGRAPHIC ZONE

In a process for supplying oxygen and/or nitrogen and also argon to a geographic zone, the geographic zone comprising n units for air separation by cryogenic distillation, of which a first unit and n-1 second units produce oxygen and/or nitrogen but do not produce argon, the oxygen and/or nitrogen for at least certain clients come from at least one of the n-1 second, non-argon-producing units, and argon for these clients comes from the first unit, where the first unit operates by means of a column system comprising a double column composed of a higher pressure column operating at a first pressure and a lower pressure column, whose bottom is connected thermally to the top of the higher pressure column, operating at a second pressure, which is lower than the first pressure, and of an argon-producing column and a mixing column, wherein the mixing column is fed at the bottom with an auxiliary gas consisting of gaseous nitrogen from the first or the lower pressure column, and at the top with a liquid which is richer in oxygen than the auxiliary gas and is taken from the lower part of the low-pressure column, and impure oxygen constituting a production gas is withdrawn at the top of the mixing column, the argon-producing column is fed with an argon-enriched gas flow from the lower pressure column, and an argon-rich product is withdrawn from the argon-producing column.

ENHANCEMENTS TO A MODERATE PRESSURE NITROGEN AND ARGON PRODUCING CRYOGENIC AIR SEPARATION UNIT

Enhancements to the distillation column system and cycles for an argon and nitrogen producing cryogenic air separation unit are provided. The enhancements include systems and methods for: (i) recovery of xenon and krypton; (ii) production of oxygen product substantially free of hydrocarbons; and (iii) improvement in the design and performance of the super-stage argon column. The present systems and methods are further characterized in an oxygen enriched stream from the lower pressure column of the air separation unit is an oxygen enriched condensing medium used in the argon condenser.

SYSTEM AND METHOD FOR CRYOGENIC AIR SEPARATION USING A BOOSTER LOADED LIQUID TURBINE FOR EXPANSION OF A LIQUID AIR STREAM
20210348839 · 2021-11-11 ·

A system and method for cryogenic air separation arrangement having a booster loaded liquid turbine for expansion of a liquid air stream or other fluid having liquid-like densities is provided. The disclosed booster loaded liquid turbines are relatively small to provide an aerodynamic and speed match between the turbine and the coupled gas compressor. The coupled gas compressor is a supplemental booster compressor and may be a dedicated warm booster compressor or alternatively a cold booster compressor.

NITROGEN GENERATING DEVICE AND NITROGEN GENERATING METHOD

A nitrogen generating device comprises: a main heat exchanger; a nitrogen distillation column; at least one nitrogen condenser; a compressor; an expansion turbine; a rotation control unit for controlling rotation with respect to a rotating shaft connecting the compressor and the expansion turbine; a pressure measuring unit for measuring a pressure value of product nitrogen gas; and an optimum rotational speed calculation command unit which inputs the pressure value measured by the pressure measuring unit into a pre-installed rotational speed calculation function to calculate the rotational speed of the rotating shaft, and issues a command to the rotation control unit.

PROCESS AND APPARATUS FOR THE SEPARATION OF AIR BY CRYOGENIC DISTILLATION

An apparatus for the separation of air by cryogenic distillation comprises a column system, a heat exchanger, a turbine, means for sending compressed and purified air at a first pressure to be cooled at the first pressure in the heat exchanger, means for sending a first gaseous stream having a nitrogen content at least that of air to be cooled and liquefied or pseudo liquefied in the heat exchanger to form a liquefied stream, means for sending at least part of the liquefied stream to be warmed and vaporized in the heat exchanger to a first intermediate temperature of the heat exchanger to form a vaporized stream, means for removing the vaporized stream from an intermediate section of the heat exchanger, a conduit for sending the vaporized stream to be expanded, in the turbine to form an expanded stream, a conduit for sending at least part of the expanded stream to the column system, a conduit for sending a second gaseous stream having the same nitrogen content as the first stream to be cooled in the heat exchanger, means for removing at least part of the second gaseous stream from an intermediate section of the heat exchanger at a second intermediate temperature and sending the second gaseous stream to the turbine to be expanded with the vaporized stream.

APPARATUS AND METHOD FOR SEPARATING AIR BY CRYOGENIC DISTILLATION

An apparatus for separating air, comprising a double column, means for sending air to the purification unit at a pressure that is no more than 1 bar higher than atmospheric pressure, a pipe for sending a first air flow, the first air flow having been purified in the purification unit, to the heat exchanger at a fourth pressure that is no more than 1 bar higher than the second pressure, a pipe for sending the first purified air flow, which has been cooled in the heat exchanger, to the second column for separation, and a booster compressor, the apparatus not comprising any means for depressurizing the first flow.

METHOD FOR STARTING UP A CRYOGENIC AIR SEPARATION UNIT AND ASSOCIATED AIR SEPARATION UNIT

In a process for starting up an air separation unit, which is at a temperature of above 0° C., the air separation unit comprising a main air compressor for compressing the feed air, a booster driven by a turbine and a venting conduit connected downstream of the booster and upstream of the main heat exchanger wherein in order to start up the air separation unit, once the turbine is operating at said given speed, the venting conduit is opened to send at least part of the air compressed in the booster from the booster outlet to the atmosphere.

SYSTEM AND METHOD FOR RECOVERY OF NITROGEN, ARGON, AND OXYGEN IN MODERATE PRESSURE CRYOGENIC AIR SEPARATION UNIT
20210348842 · 2021-11-11 ·

A moderate pressure nitrogen and argon producing cryogenic air separation unit is provided that includes a three distillation column system and turbine air stream bypass arrangement or circuit. The turbine air stream bypass arrangement or circuit is configured to improve argon and nitrogen recoveries in select operating modes by optionally diverting a portion of the turbine air stream to a nitrogen waste stream circuit drawn from the lower pressure column of the cryogenic air separation unit such that the diverted portion of the turbine air stream bypasses the distillation column system.

Method for reheating an atmospheric vaporizer using a gas originating from a cryogenic air separation unit

In a method for reheating an atmospheric vaporizer, a cryogenic liquid is vaporized by heat exchange with ambient air in the atmospheric vaporizer and to reheat the vaporizer, a gas is sent thereto at a temperature of at least 0° C., this gas originating from a cryogenic distillation air separation unit.