An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.

A device for refrigerating and/or liquefying a working gas comprising helium, the device comprising a looped working circuit for the working gas includes, in series, a compression station, a cold box, a heat exchange system exchanging heat between the cooled working gas and a user, the device further comprising an additional pre-cooling system comprising at least one tank of auxiliary cryogenic fluid, such as liquid nitrogen, the cold box comprising a first cooling stage of the working gas comprising a first exchanger disposed at the output of the compression station as well as a second heat exchanger and a third heat exchanger, the first heat exchanger being of the aluminum plate-fin type, the second heat exchanger being of the tube or welded plate type, characterized in that the second and third heat exchangers are connected both serially and in parallel on the working circuit downstream of the first heat exchanger.

A method for cryogenic cooling without fouling is disclosed. The method comprises providing a first cryogenic liquid saturated with a dissolved gas; expanding the first cryogenic liquid into a separation vessel, separating into a vapor, a second cryogenic liquid, and a first solid; drawing the vapor into a heat exchanger and the second cryogenic liquid and the first solid out of the separation vessel; cooling the vapor against a coolant through the heat exchanger, causing the vapor to form a third cryogenic liquid and a second solid, the second solid dissolving in the third cryogenic liquid; and combining the second cryogenic liquid and the first solid with the third cryogenic liquid, producing a final cooled slurry. In this manner, the cryogenic cooling is accomplished without fouling.

An enclosure for a column for low-temperature distillation comprises a distillation column, which has a circular cross section and is to be thermally insulated, the column containing liquid during use, at least one pipe attached to the column for transporting a liquid, a parallelepipedal casing enclosing the column in a sealed manner, pulverulent thermal insulation filling the space between the column or columns and the casing, a liquid-retaining tank, which has a flat bottom and four side walls, defining a liquid-retaining space, the tank being arranged inside the casing below the column in order to collect liquid that has leaked from the column, the tank being made from stainless steel or from aluminium and the casing being made from carbon steel, the column resting on the bottom of the tank through a skirt, the skirt being a cylinder made from stainless steel and having the same diameter as the column, the liquid-retaining space containing pulverulent thermal insulation.

Disclosed are a helium gas liquefier and a method for liquefying a helium gas. The disclosed helium gas liquefier includes: a first cooling part including a first cooling column; a first cold head installed on the first cooling column, and a first cylinder in which the first cooling column and the first cold head are built; a second cooling part including a second cooling column, a second cold head installed on the second cooling column, and a second cylinder in which the second cooling column and the second cold head are built; and a liquid helium storage disposed under the second cooling part.

A device for refrigerating and/or liquefying a working gas comprising helium, the device comprising a looped working circuit for the working gas includes, in series, a compression station, a cold box, a heat exchange system exchanging heat between the cooled working gas and a user, the device further comprising an additional pre-cooling system comprising at least one tank of auxiliary cryogenic fluid, such as liquid nitrogen, the cold box comprising a first cooling stage of the working gas comprising a first exchanger disposed at the output of the compression station as well as a second heat exchanger and a third heat exchanger, the first heat exchanger being of the aluminum plate-fin type, the second heat exchanger being of the tube or welded plate type, characterized in that the second and third heat exchangers are connected both serially and in parallel on the working circuit downstream of the first heat exchanger.

An air-sparged hydrocyclone for separating a vapor from a carrier gas is disclosed. The cyclone comprises a porous sparger covered by an outer gas plenum. A cryogenic liquid is injected to a tangential feed inlet at a velocity that induces a tangential flow and a cyclone vortex in the air-sparged hydrocyclone. The carrier gas is injected into the cyclone through the porous sparger. The vapor dissolves, condenses, desublimates, or a combination thereof, forming a vapor-depleted carrier gas and a vapor-enriched cryogenic liquid. The vapor-depleted carrier gas is drawn through a vortex finder and the vapor-enriched cryogenic liquid is drawn through an apex nozzle outlet. In this manner, the vapor is removed from the carrier gas.

The invention relates to a coupling which includes at least: a tubular coupling member suitable for receiving a pipe and comprising one or more annular ribs, and a crimping ring arranged on the coupling member and translatably movable between a position for inserting the pipe into the coupling member, and a crimping position, in which the crimping ring immobilizes the pipe relative to the coupling member after the deformation of the one or more ribs. Recesses are formed between the coupling member and the pipe in the crimping position. The coupling has at least one exhaust opening arranged such as to provide fluid communication between said at least one recess and the outside of the coupling.