A method for operating a reagent metering system which meters a reagent into an exhaust duct of an internal combustion engine upstream of an SCR catalytic converter, in which, after the metering operation is ended, at least part of the reagent metering system is emptied by back-suction by means of a reciprocating pump. The procedure according to the invention is distinguished in that during the back-suction, a stop determination determines the flight time of a reciprocating piston of the reciprocating pump from a starting time as far as the stop time, in that a comparator compares the flight time determined with a flight time threshold value, and in that the activation power of the reciprocating pump is reduced if the flight time determined is less than the flight time threshold value.

A method for operating a reagent metering system which meters a reagent into an exhaust duct of an internal combustion engine upstream of an SCR catalytic converter, in which, after the metering operation is ended, at least part of the reagent metering system is emptied by back-suction by means of a reciprocating pump. The procedure according to the invention is distinguished in that during the back-suction, a stop determination determines the flight time of a reciprocating piston of the reciprocating pump from a starting time as far as the stop time, in that a comparator compares the flight time determined with a flight time threshold value, and in that the activation power of the reciprocating pump is reduced if the flight time determined is less than the flight time threshold value.

The exemplary embodiments control solvent pumps so that system flow is constant. One or more controllers may control the flow rate produced by the pumps over time. The one or more controllers control a first pump so that, as the first pump is refilling, a second pump maintains a sufficient flow rate to compensate for the lost flow due to the refilling event. In some exemplary embodiments, the one or more controllers control the timing of the refilling event for the first event such that the refilling event overlaps with the equilibrating of the chromatography column with solvent(s) from the second pump. Similarly, the one or more controllers control the timing of the refilling event for the second pump such that the refilling event overlaps with the equilibrating of the chromatography column.

The exemplary embodiments control solvent pumps so that system flow is constant. One or more controllers may control the flow rate produced by the pumps over time. The one or more controllers control a first pump so that, as the first pump is refilling, a second pump maintains a sufficient flow rate to compensate for the lost flow due to the refilling event. In some exemplary embodiments, the one or more controllers control the timing of the refilling event for the first event such that the refilling event overlaps with the equilibrating of the chromatography column with solvent(s) from the second pump. Similarly, the one or more controllers control the timing of the refilling event for the second pump such that the refilling event overlaps with the equilibrating of the chromatography column.