The present disclosure relates to devices and methods for the storage of material at cryogenic temperatures. Such devices may be useful for storing materials in the vapor space of a cryogenic dewar at a stable temperature and for preventing temperature excursions that may otherwise occur during refilling of a dewar with liquid cryogen. In some implementations, the devices may include a cryogen space holding liquid cryogen and gas, a separate storage space containing only gas, and a separate path for gas to leave the cryogen space during cryogen refills without passing through or substantially disturbing the temperature of the storage space. Some implementations further provide for passage of gas from the cryogen space to the storage space between cryogen refills to improve cryogen utilization efficiency.

A system is described wherein a cryogenic liquid transport fluid is used as in thermal communication with a volatile gas as a second cryogenic liquid. The volatile gas in the liquid state enables transport of additional volatile substances that cannot be transported in the liquid state employing only the cryogenic liquid. The thermal communication between cryogenic liquids is a thermal cascade.

A sterilized-liquefied gas apparatus of the invention includes: a liquefied gas reservoir; a source-gas supplier that supplies a source gas to the liquefied gas reservoir; a cooler that cools down an inside of the liquefied gas reservoir and thereby liquefies the source gas; a supply pipe that connects the source gas supplier and the liquefied gas reservoir; a sterilization filter provided in the supply pipe; a sterilizer that sterilizes, by a sterilizing gas, a sterilization region that is located further downstream than the sterilization filter; and a sterilizing-gas remover that removes the sterilizing gas after sterilization.

The invention relates to a head (5) for a storage container for fluids, comprising a head body, characterised in that a through sleeve (10) is located inside the head body, wherein a protection tube (2) is coupled to the through sleeve (10) in the lower part of the head body, and a liquid level capacitive sensor (3) is mounted in the lower part of the body, a gland coupled with a flange to an electronic junction box (4) powered by a battery or an accumulator, the gland is located in the upper part of the body, the junction box comprising a circuit board equipped with a microcontroller and a diode gauge (6), and conduits ended with a plug extend from the electronic junction box (4).

A sealed container having gloves attached thereto is provided as part of a physical properties measuring system (PPMS). The PPMS includes a sealed pressurized portion that is pressurized with a gas to purge out air from inside the sealed pressurized portion to reduce water vapor inside the sealed pressurized portion below a water vapor threshold. The system further includes a cryogenic tank having a cryostat disposed therein. The cryogenic tank contains a cryogenic liquid cooled to a cryogenic temperature. Test samples are placed inside the sealed pressurized portion in preparation of measuring physical properties of the test samples. One of the test samples is immersed in the cryogenic liquid to measure the physical properties. The test sample is removed from the cryogenic liquid and is exchanged for another test sample inside the sealed pressurized portion to prevent ice formation inside the cryostat.

A method of servicing a cryo-EM storage system includes identifying an element of the storage system, the element including at least one of a dewar, a rack, a puck, a gridbox, and a grid, marking the element for additional action via a user device, and sending a request to another party via a network to perform the additional action.

A dewar vessel storage apparatus configured to hold at least two dewar vessels containing liquefied gas or cryo-compressed gas, comprising; a box having an outer, thermally insulating, wall; the box comprising a plurality of insulating cavities, each cavity configured to receive a single dewar vessel and is thermally insulated from each other cavity; a thermally insulating closure arrangement configured to close an open end of each cavity; a ventilation assembly comprising at least one conduit within the box configured to provide for venting of gas released from the dewar vessels when stored in the respective cavities of the box, the ventilation assembly configured to provide a gas outlet flow path from each cavity.

Provided is a manifold attachment assembly for attachment to a cryogenic cylinder. The assembly includes a knuckle configured to be attached to the cryogenic cylinder and a manifold configured to be attached to the knuckle. The manifold has an upper surface, a lower surface configured to abut an upper surface of the knuckle, a plurality of gas passages extending through the manifold for aligning with a corresponding one of a plurality of gas passages in the knuckle, and a plurality of valve seats in the upper surface each in communication with one of the plurality of gas passages in the manifold. The assembly also includes a plurality of valves respectively secured to the manifold in one of the plurality of valve seats. The attachment assembly provides a modular assembly that reduces refurbishment and requalification time, reduces assembly labor, and simplifies servicing.

A tube-array-type liquid nitrogen container includes a container body having a mouth; a tube array component received in the container body; and a top cap sealing the mouth from above. The top cap is rotatable in the mouth. The tube array component is composed of a plurality of holding tubes. The holding tube is opened at one end thereof, wherein the opening thereof faces the top cap. The top cap has at least one tube access passing therethrough. Each tube access is atop covered by a tube access cover. The tube-array-type liquid nitrogen container uses a tube-array component composed of the a plurality of holding tubes to store the freezing tubes, and is cooperated with the rotatable top cap and an external robotic arm, thereby improving space utilization and thermal insulation, effectively ensuring safety of the freezing tubes, and facilitating automatic storage of freezing tubes.

A system for recalibrating a temperature reading of a dewar includes a vapor plug and an electronic device. The vapor plug includes a vapor plug cover, a neck extending from the vapor plug cover, and a sensor positioned on the neck. The neck is configured to be inserted into an opening of the dewar. The sensor is configured to detect at least one parameter associated with the dewar. The electronic device is in communication with the sensor, and is configured to receive, recalibrate, and transmit the at least one parameter from the sensor.