F25J2200/06

METHOD AND APPARATUS FOR SEPARATING AIR BY CRYOGENIC DISTILLATION

In a method for separating air by cryogenic distillation using a column system consisting of a higher pressure column operating at a first pressure and a lower pressure column operating at a second pressure, a first air flow constituting between 75% and 98% of the air sent to the column system compressed to a third pressure above the first pressure, is sent to the higher pressure column, a second air flow constituting between 5% and 25% of the air sent to the column system is compressed to a fourth pressure above the second pressure but lower than the third pressure, is sent to the lower pressure column, a third column separates an argon-enriched flow and the air sent to the lower pressure column constitutes between 10% and 25% of the total air sent to the column system.

PROCESS FOR SUPPLYING OXYGEN AND/OR NITROGEN AND ALSO ARGON TO A GEOGRAPHIC ZONE

In a process for supplying oxygen and/or nitrogen and also argon to a geographic zone, the geographic zone comprising n units for air separation by cryogenic distillation, of which a first unit and n-1 second units produce oxygen and/or nitrogen but do not produce argon, the oxygen and/or nitrogen for at least certain clients come from at least one of the n-1 second, non-argon-producing units, and argon for these clients comes from the first unit, where the first unit operates by means of a column system comprising a double column composed of a higher pressure column operating at a first pressure and a lower pressure column, whose bottom is connected thermally to the top of the higher pressure column, operating at a second pressure, which is lower than the first pressure, and of an argon-producing column and a mixing column, wherein the mixing column is fed at the bottom with an auxiliary gas consisting of gaseous nitrogen from the first or the lower pressure column, and at the top with a liquid which is richer in oxygen than the auxiliary gas and is taken from the lower part of the low-pressure column, and impure oxygen constituting a production gas is withdrawn at the top of the mixing column, the argon-producing column is fed with an argon-enriched gas flow from the lower pressure column, and an argon-rich product is withdrawn from the argon-producing column.

ENHANCEMENTS TO A MODERATE PRESSURE NITROGEN AND ARGON PRODUCING CRYOGENIC AIR SEPARATION UNIT

Enhancements to the distillation column system and cycles for an argon and nitrogen producing cryogenic air separation unit are provided. The enhancements include systems and methods for: (i) recovery of xenon and krypton; (ii) production of oxygen product substantially free of hydrocarbons; and (iii) improvement in the design and performance of the super-stage argon column. The present systems and methods are further characterized in an oxygen enriched stream from the lower pressure column of the air separation unit is an oxygen enriched condensing medium used in the argon condenser.

ARGON ENHANCING METHOD AND DEVICE

An air separation apparatus is provided, including an air separation unit including a low-pressure column, a mixing column, and a pure nitrogen column, wherein the low-pressure column has a first nominal diameter, the pure nitrogen column has a second nominal diameter which is smaller than the first nominal diameter, wherein the mixing column has an open cylindrical shape, with the inner diameter nominally greater than the second nominal diameter, with the pure nitrogen column located within the mixing column interior.

PROCESS AND APPARATUS FOR CRYOGENIC SEPARATION OF AIR WITH MIXED GAS TURBINE
20230358468 · 2023-11-09 ·

In this process and apparatus for cryogenic separation of air, the separation column system comprises a high-pressure column, a low-pressure column and a crude argon column. A mixed gas stream produced by mixing gaseous oxygen and a gas stream from the evaporation space of the argon top condenser, is work expanded in a mixed gas turbine.

GAS PROCESSING METHODOLOGY UTILIZING REFLUX AND ADDITIONALLY SYNTHESIZED STREAM OPTIMIZATION
20230375263 · 2023-11-23 ·

Gas processing methodology for high efficiency recovery of propane and/or ethane from a natural gas feed stream. The method is conducted without turboexpansion. A natural gas stream is processed to have gas and liquid portions. The gas portion is cooled and flows to a refluxed absorber column and the liquid portion flows to a lower pressure distillation column. Bottoms of the absorber column are depressurized directly into a lower pressure distillation column and the overhead vapor stream is used to cool the feed and/or reflux streams. The overhead vapour stream from the lower pressure distillation column split into at least two streams with one being depressurized into the absorber to provide reflux and the second passed into the absorber column to provide further reflux.

Atmospheric Water Harvester with Cryogenic System
20230021519 · 2023-01-26 ·

An atmospheric water harvesting system includes a water-harvesting unit with an air mover and a heat exchanger. The water-harvesting unit may also include one or more screens on which water can condense. The water-harvesting unit is supplied by a coolant pathway, in which a non-cryogenic fluid coolant flows. A cryogenic cell is in the coolant pathway. The cryogenic cell receives the fluid coolant and removes heat from it by causing or allowing a controlled heat transfer between the fluid coolant and a first cryogen sealed within an inner vessel in the cryogenic cell. The coolant may be a liquid at operating temperatures, and the cryogenic cell may cool it to an appropriate temperature without a phase change, essentially acting as a “cold battery” to remove heat from the coolant.

PROCESS AND PLANT FOR LOW-TEMPERATURE FRACTIONATION OF AIR
20220260312 · 2022-08-18 ·

A SPECTRA process for low-temperature fractionation of air, in which bottoms liquid from an additional second rectification column used to obtain oxygen is evaporated in a second condenser-evaporator. In this second condenser-evaporator, gas that has been evaporated beforehand in a first condenser-evaporator, which is used for condensation of tops gas from a first rectification column, is condensed at the pressure level of the previous evaporation. The invention likewise provides a corresponding plant.

PURIFICATION OF CARBON MONOXIDE BY CRYOGENIC DISTILLATION

In a process for the separation of a flow containing at least 97% mol of carbon monoxide containing at least one lighter compound and at least one heavier compound, the flow is separated in a column and a column, one of the columns being a denitrogenation column and the other a column for purification in argon, in order to form a flow very rich in carbon monoxide.

FLUID RECOVERY PROCESS AND APPARATUS

A process for recovering at least one fluid (e.g. argon gas and/or nitrogen gas, etc.) from a feed gas (e.g. air) can include utilization of a compression system, primary heat exchanger unit, plant processing units to separate and recover at least one desired fluid (e.g. nitrogen gas, argon gas, etc.). In some embodiments, the process can be configured so that fluid flows output from a low pressure column and/or high pressure column of the plant can provide a condensation duty or refrigeration duty that is utilized to process certain fluid flows for recovery of argon and/or nitrogen gases. Some embodiments can be configured to provide an improved recovery of argon and/or nitrogen as well as an improvement in operational efficiency by reducing an amount of power (e.g. electrical power) needed to recover the nitrogen and/or argon.