An automatic vacuum preheating furnace comprises a furnace box, a vacuum extraction device used to evacuate the furnace box, a transporting device located inside the furnace box and used to transport materials, two opposite end of the furnace box have an opening respectively, an automatic sealing door is located on the opening, the automatic vacuum preheating furnace further includes preheating devices, each preheating devices includes a blasting device which is located under the furnace box and connected with the furnace box, and a wind returning device which is located upon the furnace box and connected with the furnace box, each blasting device includes a heating unit and a wind adjusting unit. Each wind adjusting unit includes wind boards, the wind boards are movably connected with two opposite sidewalls of the furnace box through hinges, the wind boards are multiple, and axes of the hinges of the wind boards are parallel to each other, and located on a same plane, the plane is parallel to a bottom of the furnace box. The structure of the automatic vacuum preheating furnace can vacuum preheat the materials the materials efficiently before vacuum drying.

Method and apparatus for drying granular resin material by drawing vacuum over heating resin material in a vessel, while periodically purging the vessel with the material therein with dry air and bathing the vacuum dried material with dry air until furnished to a processing machine.

A drying apparatus includes a drying chamber configured to be connected to a decompression section, and a moving section configured to move a target object in the interior of the drying chamber. With this structure, the pressure in the interior of the drying chamber can be reduced and the target object can be dried in the interior of the drying chamber, and thereby the drying efficiency of the target object can be increased.

A method of using a vacuum chamber to assist in detecting moisture on an instrument, removing moisture from the instrument, and confirming dryness of the instrument is disclosed. The method may include the steps of opening a vacuum chamber; placing an instrument into the chamber, closing the chamber, withdrawing a first volume of air from the chamber; changing a volume of liquid water into vapor, introducing a second volume of air into the chamber, withdrawing the second volume of air from the chamber, changing a second volume of liquid water into vapor, introducing a third volume of air into the chamber, opening the chamber, and removing the instrument from the chamber in a dry state. This method may also include the steps of collecting pressure data corresponding to the pressure within the chamber while withdrawing the second volume of air from the chamber, calculating a first second-derivative value of pressure with respect to time corresponding to a pressure greater than approximately the triple-point pressure of water, calculating a second second-derivative value of pressure with respect to time corresponding to a pressure greater than approximately the triple-point pressure of water and a time subsequent to the time corresponding to the first second-derivative value, calculating a third second-derivative value of pressure with respect to time corresponding to a pressure less than approximately the triple-point pressure of water and a time subsequent to the time corresponding to the second second-derivative value, calculating a fourth second-derivative value of pressure with respect to time corresponding to a pressure less than approximately the triple-point pressure of water and a time subsequent to the time corresponding to the third second-derivative value, determining that the fourth second-derivative value is less than or equal to the third second-derivative value, determining that the second second-derivative value is less than or equal to the first second-derivative value. The vacuum chamber may include a rack for hanging instruments having lumens, such as endoscopes.

Vacuum rotary automatic dryers for fruits, vegetables, grains, herbs, medicines and granulate, is composed of the box frame (5), the loading conveyor (6) and the hopper (7), whereby on the box frame (5) in the upper horizontal sector is the shaft (18), mounted to which the frame (8) is attached, in which a cylinder (4) is mounted with the cover (32), which rotates around its axis using an electric motor (11). In the cylinder (4) are small cylinders (1) inserted in which the products for drying are loaded. In the process of loading the products, cylinder (4) with the cylinders (1) is placed in a vertical position, and then, in the drying process, it is rotated into a horizontal position by a pneumatic cylinder (19). Low-pressure in smaller cylinders (1) is achieved using a vacuum pump (2), and the warm water is fed through a swivel joint (25) through a hollow shaft (9) in the central tube (26) and the space of cylinder (4) and flows around the outer surface of small cylinders (1). The area under the cover (32) and in small cylinders (1) is connected with the circulating pump (21) which pushes water while washing the products through a vacuum distributer (20) filling about of useful volume. Through the PLC controller (22) cycles of washing and drying of the product, as well as washing of small cylinders (1), take place automatically. In accordance with the idea of the invention, the vacuum is achieved only in small cylinders (1), which reduces the dimensions and quantity of materials for the construction of dryers, as well as the energy consumption, because the design allows the evaporation with low-pressure below 50 millibars and a heating temperature below 40 C. The product quality is also improved because of the slight movement of the products prevents them from sticking to the inner walls of the smaller cylinders (1) and the walls of the augers (3,41) and thus prevents damage to the membrane, which is especially important when drying fruits. The invention also allows, that in the same device, washing of products before drying and washing of small cylinders (1) and augers (3, 41) after unloading of dried products, which is very important, because hand washing with existing dryers significantly increases the time between two drying cycles. The invention also allows that the space for the products, i.e. in smaller cylinders (1), is fed with chemical solutions in liquid or gaseous state using a circulating pump (21), e.g. i

A reduced-pressure drying apparatus, for drying solution on a substrate in a chamber in a depressurized state, includes a solvent collecting unit that is a net-shaped plate configured to temporarily collect a solvent in the solution vaporized from the substrate. The solvent collecting unit is provided to face the substrate in the chamber, and the net-shaped plate has an opening ratio of 60% to 80% and a thermal capacity of 850 J/K or less per 1 m.sup.2.

An embodiment of the present invention provides a vacuum drying apparatus and a vacuum drying method. The vacuum drying apparatus includes a chamber in which a substrate table is arranged, the chamber being provided with a wind deflector therein, wherein the wind deflector comprises a top opening, a bottom opening and a body part connecting the top opening with the bottom opening. During the vacuum drying, the bottom opening is in tight contact with a surface of the substrate table, and there is a gap between the top opening and the top of the chamber and a material on the substrate table is covered by the wind deflector.

Provided herein is a method of drying electrode assembly of lithium-ion battery, comprising the steps of vacuum drying the electrode assembly in an oven at elevated temperature; filling the oven with hot, dry air or inert gas; repeating the steps of vacuum drying and gas filling 2 or more times. The method disclosed herein can provide the electrode assembly having a water content of less than 20 ppm.

Provided herein is a method of drying an electrode assembly of lithium-ion battery, comprising drying the electrode assembly in two successive stages under vacuum at elevated temperature; filling the oven with hot, dry air or inert gas; repeating the steps of vacuum drying and gas filling several times. The method disclosed herein is particularly suitable for drying electrode assemblies using aqueous binders.

The invention relates to a device for freeze-drying a liquid-containing composition, including but not limited to injectable compositions, in particular pharmaceutical compositions, biological compositions, cosmetic compositions or medical nutritional products. In particular, the present disclosure relates to a device suitable for freeze-drying liquid-containing compositions in a continuous process and to methods therefore. The device for freeze-drying a liquid containing composition in a continuous process comprises one or more, preferably three or more, of a spinner, a transportation mechanism, a vial handler, a vacuum door, and a stoppering system.