F25J3/0406

Process for obtaining one or more air products and air separation plant
11098950 · 2021-08-24 · ·

The invention proposes a process and an air separation plant comprising a rectification column system comprising a high-pressure column, a low-pressure column, a main heat exchanger, and a main air compressor. The total air supplied to the rectification column system is compressed in the main air compressor to a first pressure level. The high-pressure column is operated at a second pressure level, at least 3 bar below the first pressure level. A gaseous, nitrogen-rich fluid is removed from the high-pressure column and warmed up in the gaseous state without prior liquefaction. A first partial quantity of the gaseous, nitrogen-rich fluid is warmed to a first temperature level of −150 to −100° C., supplied at this first temperature level to a booster and compressed further to a third pressure level. The first partial quantity is then warmed to a second temperature level and discharged from the air separation plant.

CRYOGENIC LIQUEFIER BY INTEGRATION WITH POWER PLANT

A method for producing liquid nitrogen using a residual gas stream derived from a flue gas of a power plant is provided. The residual gas stream is purified in a front-end purification unit to remove freezable components and then the purified stream is compressed. Following compression, the stream can be divided into a first portion and a second portion, wherein the first portion is cooled and sent to a distillation column, wherein oxygen and argon are separated, thereby leaving an essentially pure gaseous nitrogen stream. The gaseous nitrogen stream can then be liquefied using refrigeration provided by expanding the second portion of the purified stream. In a preferred embodiment, the second portion is expanded in two turbines, and the gaseous nitrogen is compressed in a cold nitrogen booster, which is powered by one of the two turbines. In an additional embodiment, after warming, the expanded second portion of the purified stream can be used to regenerate the front-end purification unit.

Device and method for separating air by cryogenic distillation

Method for separating air by cryogenic distillation, wherein at least part of the air to be distilled is boosted in an air booster, compressed air is allowed to expand in at least one expansion turbine and, if the pressure drop between two points of the booster passes under a threshold and/or a flow of the booster passes under a minimum flow of the booster, part of the air boosted in the booster is allowed to expand without having been cooled between the booster and the expansion turbine and the boosted expanded air is sent upstream or downstream of the at least one turbine, without having been cooled in the heat exchanger, after having been boosted.

METHOD AND DEVICE FOR SEPARATING AIR BY CRYOGENIC DISTILLATION
20200333069 · 2020-10-22 ·

A method for separating air by cryogenic distillation, wherein air is compressed in a first compressor, cooled in a heat exchanger and then separated in a system of columns, liquid oxygen is vaporized in the heat exchanger countercurrent to a flow of pressurized gas which pseudo-condenses, a flow of gas which is air or a gas delivered from the system of columns is expanded in a cryogenic expansion turbine having a single wheel, the turbine having an inlet temperature lower than 100 C., a gas which is air or a gas delivered from the system of columns is compressed in a first booster compressor having a single wheel, with an inlet temperature higher than 50 C., a gas which is air or a gas delivered from the system of columns.

Method and device for separating air by cryogenic distillation

Method for separating air by cryogenic distillation, wherein air is compressed in a compressor and is subsequently sent to a heat exchanger, with the air cooled in the exchanger being sent to a check valve downstream of the heat exchanger and subsequently to a turbine, the valve being positioned so that air from a short-circuiting duct cannot return to the exchanger from the compressor.

METHOD AND APPARATUS FOR ELIMINATING HEAT BUMPS FOLLOWING REGENERATION OF ADSORBERS IN AN AIR SEPARATION UNIT

A method for reducing heat bumps following regeneration of adsorbers in an air separation unit is provided. The air separation unit can include a front end purification unit, a main air compressor, a main heat exchanger, a distillation column system, a regeneration gas heater, and a regeneration gas cooler, wherein the front end purification unit comprises a first adsorber and a second adsorber. The method can include the steps of: regenerating the first adsorber while the second adsorber operates in an adsorption cycle, wherein the step of regenerating the first adsorber further includes the steps of heating the first adsorber and then cooling the first adsorber, wherein during the step of cooling the first adsorber, a regeneration gas sourced from the distillation column system and cooled in the main heat exchanger is further cooled in a regeneration gas cooler prior to being used to cool the first adsorber.

METHOD AND APPARATUS FOR AIR SEPARATION BY CRYOGENIC DISTILLATION

A method for separating air by cryogenic distillation in a system of columns comprising a first column and a second column operating at a lower pressure than the first column, comprising the steps of compressing all of the feed air in a first compressor to a first output pressure of at least 1 bar greater than the pressure of the first column, sending a first portion of the air under the first output pressure to the second compressor, and compressing the air to a second output pressure, cooling and condensing at least a portion of the air under the second output pressure in a heat exchanger, withdrawal of a liquid from a column of the system of columns, pressurising the liquid and evaporating the liquid by heat exchange in the heat exchanger, and pressure reduction of a portion of the compressed air to a second output pressure, at least partially evaporating said air in the heat exchanger, optionally additional heating of said air in the heat exchanger, and sending at least a portion of this air to the second compressor.

System and method for recovery of nitrogen, argon, and oxygen in moderate pressure cryogenic air separation unit

A moderate pressure nitrogen and argon producing cryogenic air separation unit is provided that includes a three distillation column system and turbine air stream bypass arrangement or circuit. The turbine air stream bypass arrangement or circuit is configured to improve argon and nitrogen recoveries in select operating modes by optionally diverting a portion of the turbine air stream to a nitrogen waste stream circuit drawn from the lower pressure column of the cryogenic air separation unit such that the diverted portion of the turbine air stream bypasses the distillation column system.

System and method for recovery of neon and helium from an air separation unit

A system and method for neon recovery in a double column or triple column air separation unit is provided. The neon recovery system comprises a non-condensable stripping column configured to produce a liquid nitrogen-rich liquid column bottoms and a non-condensable gas containing overhead and one or more condensing units arranged to produce a crude neon vapor stream that contains greater than about 50% mole fraction of neon with the overall neon recovery exceeding 95%. In addition, there is minimal liquid nitrogen consumption and since much of the liquid nitrogen is recycled back to the lower pressure column of the air separation unit, there is minimal impact on the recovery of other products from the air separation unit.

Method and device for separating air by cryogenic distillation

The invention relates to a method for separating air by cryogenic distillation in a set of columns including a first column operating at a first pressure, a second column operating at a second pressure which is lower than the first pressure, and a third column operating at a third pressure, which is lower than the second pressure, wherein the third column includes first and second evaporator-condensers, and nitrogen from a cold compressor is sent to one of the evaporator-condensers.