An apparatus for distillation at cryogenic temperatures can include a cold box module comprising framing and having an upper module section and a lower module section, wherein the upper module comprises a roof; an upper column section disposed within the upper module section; a lower column section disposed within the lower module section; a plurality of support saddles attached to the upper and lower module sections that are configured to provide structural support for the upper and lower column sections when the upper and lower column sections are in a horizontal position during transportation; and means for limiting longitudinal movement of the lower column section when the lower module section is in a horizontal position during transport, wherein the means for limiting longitudinal movement are connected to the lower column section and the lower module section.

A method for constructing a cold box module and resulting apparatus is provided. The method can include providing a cold box module having framing and an upper and lower module sections, introducing an upper column section longitudinally into the upper module section while the upper module section is substantially horizontal; introducing a lower column section longitudinally into the lower module section while the lower module section is substantially horizontal; releasably attaching the lower column section to the lower module section using shipping saddle spacers and support saddles; and attaching a skirt attachment to the lower column section and the lower module section, wherein the skirt attachment is configured to limit longitudinal movement of the lower column section when the lower module section is in a horizontal position during transport. After erecting the cold box module at the installation site, the shipping saddle spacers can be removed and the upper column section is lowered using a jacking system located on the roof of the cold box module.

A method for installation of a cryogenic distillation apparatus is provided. The method can include the steps of: providing an upper module section having an upper column section disposed within and secured to the upper module section, wherein the upper module comprises a roof; providing a lower module section having a lower column section disposed within and secured to the lower module section; erecting the lower module section from a horizontal position to a vertical position at an installation site; lifting the upper module section from a horizontal position and attaching the upper module section, while in a vertical position, to a top portion of the lower module section; lowering the upper column section, independent of the upper module section, toward the lower column section; and welding the upper column section and the lower column section together.

The jacking system and method for using it to lower an upper column section without the use of a crane is provided. The jacking system is configured to be disposed on a roof of a cold box module and may include: a structural assembly; and a plurality of suspension rods supported at an upper end by the structural assembly, wherein the plurality of suspension rods is configured to provide support to the upper column section

A cryogenic air separation method and apparatus in which first and second liquid streams are produced. The first liquid stream has a higher oxygen content than air and can consist of a higher pressure distillation column bottoms and the second liquid stream, for instance, air, has a lower oxygen content than the first liquid stream and an argon content no less than the air. The second liquid stream is subcooled through indirect heat exchange with the first liquid stream and both of such streams are introduced into the lower pressure column. The second liquid stream is introduced into the lower pressure column above that point at which the crude liquid oxygen column bottoms or any portion thereof is introduced into the lower pressure column to increase a liquid to vapor ratio below the introduction of the second liquid stream and therefore, reduce the oxygen present within the column overhead.

A method for the cryogenic fractionation of air, in which a liquid volume present in a vaporization chamber in a distillation column system of an air fractionation plant is fed by means of a cryogenic liquid and in which a proportion of the liquid volume is continuously transferred into the gas phase by vaporization, wherein, in addition to oxygen, the cryogenic liquid contains components, including xenon, which are higher-boiling than oxygen. The content of xenon in the cryogenic liquid is determined and used as a measure of any enrichment of the components which are higher-boiling than oxygen in the cryogenic liquid. A corresponding air fractionation plant is also described.

A system and method serve generate oxygen by low-temperature air separation in a distillation column system having a high-pressure column and a low-pressure column, a main condenser which is constructed as a condenser-evaporator, and an auxiliary column. A gaseous oxygen-containing fraction is introduced into the auxiliary column. A nitrogen-containing liquid stream from the high-pressure column, the main condenser or the low-pressure column is applied as reflux to the top of the auxiliary column. An argon-rich stream from an intermediate site of the low-pressure column is introduced into an argon removal column that has an argon removal column top condenser. The low-pressure column is arranged beside the high-pressure column, the main condenser is arranged over the high-pressure column, the auxiliary column is arranged over the main condenser, the argon removal column is arranged over the auxiliary column and the argon removal column top condenser is arranged over the argon removal column.

The invention relates to a cryogenic distillation apparatus for a gas mixture, including a purification apparatus for purifying a gas mixture in a system with a plurality of adsorbant bottles, a column system, a capacity, means for feeding a cryogenic liquid to the capacity, means for feeding a vaporized liquid from the capacity to a column of the system, a vaporizer in the capacity for vaporizing the contained liquid; means for feeding a calorigenic gas to the vaporizer, and means for drawing a liquid from the capacity.

A system and method of ultra-high purity (UHP) oxygen production from an argon and oxygen producing cryogenic air separation unit incorporating a dedicated methane rejection column or column section having a liquid to vapor (L/V) ratio lower than the L/V ratio in the associated argon rectifier is provided.