Patent classifications
F25J3/04181
Method and apparatus for eliminating heat bumps following regeneration of adsorbers in an air separation unit
A method for reducing heat bumps following regeneration of adsorbers in an air separation unit is provided. The air separation unit can include a front end purification unit, a main air compressor, a main heat exchanger, a distillation column system, a regeneration gas heater, and a regeneration gas cooler, wherein the front end purification unit comprises a first adsorber and a second adsorber. The method can include the steps of: regenerating the first adsorber while the second adsorber operates in an adsorption cycle, wherein the step of regenerating the first adsorber further includes the steps of heating the first adsorber and then cooling the first adsorber, wherein during the step of cooling the first adsorber, a regeneration gas sourced from the distillation column system and cooled in the main heat exchanger is further cooled in a regeneration gas cooler prior to being used to cool the first adsorber.
SYSTEM AND METHOD FOR RECOVERY OF NITROGEN, ARGON, AND OXYGEN IN MODERATE PRESSURE CRYOGENIC AIR SEPARATION UNIT
A moderate pressure nitrogen and argon producing cryogenic air separation unit is provided that includes a three distillation column system and turbine air stream bypass arrangement or circuit. The turbine air stream bypass arrangement or circuit is configured to improve argon and nitrogen recoveries in select operating modes by optionally diverting a portion of the turbine air stream to a nitrogen waste stream circuit drawn from the lower pressure column of the cryogenic air separation unit such that the diverted portion of the turbine air stream bypasses the distillation column system.
METHOD AND APPARATUS FOR IMPROVING EFFICIENCY OF A FRONT-END PURIFICATION UNIT OF AN AIR SEPARATION PLANT
A method and apparatus for reducing heat bumps following regeneration of adsorbers in an air separation unit is provided. Certain embodiments of the current invention utilize the two waste streams available at very different temperatures from the two main exchangers (low-pressure and high-pressure core exchangers) for regeneration of the front-end purification adsorbers in the air separation unit (ASU) to reduce its energy consumption without compromising the stability of process. Certain embodiments help to eliminate/minimize high air temperature disturbance (heat bump) for the process downstream of the front-end purification unit during the transition from offline to online.
Method and apparatus for reducing process disturbances during pressurization of an adsorber in an air separation unit
A method for reducing process disturbances during pressurization of an adsorber in an air separation unit is provided, in which the air separation unit includes a front end purification unit and an air buffer tank. In one embodiment, the method can include the steps of: pressurizing a first adsorber while a second adsorber operates in an adsorption cycle, wherein the step of pressurizing the first adsorber further includes the steps of withdrawing a pressurized air stream from the air buffer tank and introducing the pressurized air stream to the first adsorber until the first adsorber is at a target pressure, wherein the air buffer tank is in fluid communication with the booster air compressor, wherein the method further includes the step of continually sending a first portion of air flow from the booster air compressor to the air buffer tank and continually sending a second portion of air flow from the booster air compressor to a system of columns within a cold box for rectification therein.
METHOD FOR THE PRODUCTION OF AIR GASES BY THE CRYOGENIC SEPARATION OF AIR WITH IMPROVED FRONT END PURIFICATION AND AIR COMPRESSION
A method and apparatus for the production of air gases by the cryogenic separation of air with front end purification and air compression can include using an available compressed dry gas such as nitrogen, oxygen, stored purified air, or synthetic air to repressurize the adsorber without diverting any of the purified air just exiting the currently on-line adsorber or changing the flow rate of the main air compressor or air sent to the cold box. This enables the main air compressor (MAC) to operate at a relatively constant flow rate while also sending a relatively constant air flow to the cold box during this repressurization step, thereby reducing the risks of process upsets and minimizing capital expenditures related to the MAC and other warm-end equipments.
PRESSURE EQUALIZING SYSTEM FOR AIR SEPARATION PURIFICATION AND CONTROL METHOD
Disclosed in the present invention are a pressure equalizing system for air separation purification, and a control method. The system comprises: a first air main pipe; a pressurizing gas pipeline, which is connected to the first air main pipe and used for receiving a pressurizing gas and delivering same to the first air main pipe; and a control valve, located on the pressurizing gas pipeline, and having a degree of opening regulated by the flow regulator, thereby regulating an air intake amount of the pressurizing gas pipeline. The present invention solves the problem of an air separation rectification process being affected when dry nitrogen is used for pressure equalization of an adsorber; in the switching process of entering an adsorption stage from a regeneration stage, pressurizing dry nitrogen used in a pressure equalizing step previously mixes with damp air from a main air compressor before entering the adsorber, such that the gas components flowing towards an air separation cold box remain substantially unchanged, in order to reduce disturbance in conditions of gas entering a rectification column to take part in rectification due to a gas component gradually changing from dry nitrogen to dry air in the prior art, thus stabilizing the process conditions of the air separation cold box.
System and method for enhanced recovery of argon and oxygen from a nitrogen producing cryogenic air separation unit
A moderate pressure air separation unit and air separation cycle is disclosed that provides for up to about 96% recovery of argon, an overall nitrogen recovery of 98 percent or greater and limited gaseous oxygen production. The air separation is configured to produce a first high purity oxygen enriched stream and a second lower purity oxygen enriched stream from the lower pressure column, one of which is used as the refrigerant to condense the argon in the argon condenser, with the resulting vaporized oxygen stream used to regenerate the temperature swing adsorption pre-purifier unit. All or a portion of the first high purity oxygen enriched stream is vaporized in the main heat exchanger to produce the gaseous oxygen products.
System and method for enhanced recovery of liquid oxygen from a nitrogen and argon producing cryogenic air separation unit
A moderate pressure, argon and nitrogen producing cryogenic air separation unit and air separation cycle having a higher pressure column, a lower pressure column and an argon column arrangement is disclosed. The moderate pressure, argon and nitrogen producing cryogenic air separation unit is configured to take a first portion of an oxygen enriched stream from the lower pressure column, which together with an external source of liquid nitrogen is used as the boiling side refrigerant to condense the argon in the argon condenser. Use of the external source of liquid nitrogen in the argon condenser allows a second portion of the oxygen enriched stream from the lower pressure column to be taken as a liquid oxygen product stream.
UTILIZATION OF NITROGEN-ENRICHED STREAMS PRODUCED IN AIR SEPARATION UNITS COMPRISING SPLIT-CORE MAIN HEAT EXCHANGERS
An air separation apparatus and process, which produces gaseous oxygen and/or nitrogen products at an elevated pressure through internal compression of respective liquid products, are disclosed. Split-core main heat exchangers are employed to warm up product streams generated in an air rectification unit against 1) a main feed air stream in the low-pressure heat exchanger and 2) at least one boosted pressure air stream in the high-pressure exchanger. Because the boosted pressure air stream is at a higher pressure and temperature than the main feed air stream, after separate heat exchange in the split main heat exchangers, the subsidiary waste nitrogen stream exiting the high-pressure heat exchanger is also warmer than the subsidiary waste nitrogen stream exiting the low-pressure heat exchanger. The warmer waste nitrogen stream is fed into the air purification unit for regeneration purposes and the cooler waste nitrogen stream is introduced into the nitrogen water tower to perform cooling duty. The two subsidiary waste nitrogen streams are also connected on the warm side of the main heat exchangers to allow flexible distribution of the flow.
Method for the production of air gases by the cryogenic separation of air with improved front end purification and air compression
A method and apparatus for the production of air gases by the cryogenic separation of air with front end purification and air compression can include using an available compressed dry gas such as nitrogen, oxygen, stored purified air, or synthetic air to repressurize the adsorber without diverting any of the purified air just exiting the currently on-line adsorber or changing the flow rate of the main air compressor or air sent to the cold box. This enables the main air compressor (MAC) to operate at a relatively constant flow rate while also sending a relatively constant air flow to the cold box during this repressurization step, thereby reducing the risks of process upsets and minimizing capital expenditures related to the MAC and other warm-end equipments.