F25J3/04884

Condenser-reboiler system and method

A system and method for the concurrent condensation of a nitrogen-rich vapor and vaporization of an oxygen-rich liquid in a distillation column based air separation unit is provided. The disclosed system includes a condenser-reboiler heat exchanger located between a lower pressure column and a higher pressure column and configured to condense a nitrogen-rich vapor from the higher pressure column and partially vaporize an oxygen-rich liquid from the lower pressure column. Within the condenser-reboiler heat exchanger, the nitrogen-rich vapor flows in an upward direction such that any non-condensables present in the nitrogen-rich vapor will accumulate proximate the upper portion or top of the condenser-reboiler modules where they can be easily removed through venting.

Method and apparatus for argon recovery in a cryogenic air separation unit integrated with a pressure swing adsorption system

A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.

Method and apparatus for argon recovery in a cryogenic air separation unit integrated with a pressure swing adsorption system

A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.

System and method for generation of oxygen by low-temperature air separation

A system and method serve generate oxygen by low-temperature air separation in a distillation column system having a high-pressure column and a low-pressure column, a main condenser which is constructed as a condenser-evaporator, and an auxiliary column. A gaseous oxygen-containing fraction is introduced into the auxiliary column. A nitrogen-containing liquid stream from the high-pressure column, the main condenser or the low-pressure column is applied as reflux to the top of the auxiliary column. An argon-rich stream from an intermediate site of the low-pressure column is introduced into an argon removal column that has an argon removal column top condenser. The low-pressure column is arranged beside the high-pressure column, the main condenser is arranged over the high-pressure column, the auxiliary column is arranged over the main condenser, the argon removal column is arranged over the auxiliary column and the argon removal column top condenser is arranged over the argon removal column.

Main heat exchange system and method for reboiling

A method and main heat exchange system for use in a cryogenic air separation plant in which down-flow and thermosiphon heat exchangers are employed to partially vaporize an oxygen-rich liquid produced in a lower pressure column and to condense the nitrogen-rich vapor in a higher pressure column. A greater proportion of the oxygen-rich liquid can be partially vaporized in the down-flow heat exchangers than in the thermosiphon heat exchangers and the nitrogen-rich vapor condensed in the thermosiphon heat exchangers can have a higher oxygen content than the nitrogen-rich vapor condensed in the down-flow heat exchangers. This allows the higher pressure column to operate at a lower pressure than would otherwise be possible. A central conduit can extend from the higher pressure column into the lower pressure column to introduce the nitrogen-rich vapor into at least the down-flow heat exchangers for purposes of reducing pressure drop and column height.

Liquid nitrogen production
20170299261 · 2017-10-19 ·

An improved process for liquid nitrogen production by cryogenic air separation using a distillation column system to enhance the product recovery.

PROCESS AND APPARATUS FOR PRODUCING PRESSURIZED GASEOUS NITROGEN BY CRYOGENIC SEPARATION OF AIR
20170211879 · 2017-07-27 ·

Process and apparatus for producing pressurized gaseous nitrogen by cryogenic separation of air. The distillation column system includes a high pressure column, a medium pressure column, a main condenser and top condenser both being condenser-evaporators. Compressed and purified feed air is cooled in a heat exchanger and introduced to the distillation system. A gaseous nitrogen stream from the high pressure column is condensed in the main condenser. Bottom liquid of the medium pressure column is evaporated and gaseous nitrogen from the medium pressure column is condensed in the top condenser. Liquid nitrogen from the medium pressure column is pressurized and introduced to the high pressure column. A second gaseous nitrogen stream from the high pressure column is recovered as pressurized gaseous nitrogen product. A portion of the compressed and purified feed air is work-expanded and then warmed in the main heat exchanger.

METHOD FOR THE CRYOGENIC SEPARATION OF AIR, AND AIR SEPARATION PLANT

A method for the cryogenic separation of air, in which method an air separation plant with a rectification column arrangement is used, which plant has a pressure column, a low-pressure column, a raw argon column and pure argon column. In the method, evaporation gas from a head gas condensation device associated with the raw argon column is partially or completely fed into the low-pressure column in a first feed-in region, whereas evaporation gas from a head gas condensation device associated with the pure argon column and excess liquid from this head gas condensation device are partially or completely fed into the low-pressure column in a shared second feed-in region. In one embodiment, flash gas forming during the expansion of cooling fluid into the head gas condensation device associated with the raw argon column can be partially or completely fed into the low-pressure column in the second feed-in region.

System and method for production of crude argon by cryogenic rectification of air

A system and method for producing argon that uses a higher pressure column, a lower pressure column, and an argon column collectively configured to produce nitrogen, oxygen and argon products through the cryogenic separation of air. The present system and method also employs a once through argon condensing assembly that is disposed entirely within the lower pressure column that is configured to condense an argon rich vapor stream from the argon column against the oxygen-enriched liquid from the higher pressure column to produce an argon liquid product. The control system is configured for optimizing the production of argon product by ensuring an even flow split of the oxygen-enriched liquid is distributed to the argon condenser cores and by adjusting the flow rate of the argon removed from the argon condensing assembly to maintain the liquid/vapor balance in the argon condensing assembly within appropriate limits.

METHOD AND APPARATUS FOR ARGON REJECTION AND RECOVERY
20170030638 · 2017-02-02 ·

A method and apparatus for argon rejection and recovery in which argon is separated from air within a cryogenic air separation plant having a divided wall argon rejection column and condensed using an argon condenser disposed internally within the lower pressure column. The resulting argon stream is subsequently rejected or recovered and optionally purified within an integrated adsorbent based argon refining and purification subsystem to produce product grade argon.