A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.

An exchange column having at least a first layer of structured packing and a second layer of structured packing, each layer formed from corrugated plates, the corrugated plates of the second layer having an orientation that is rotated at an angle relative to the corrugated plates of the first layer from 20 to 90, wherein the vertical height of the first layer and/or the vertical height of the second layer is greater than 350 mm or greater than 400 mm.

An exchange column having at least a first layer of structured packing and a second layer of structured packing, each layer formed from corrugated plates, the corrugated plates of the second layer having an orientation that is rotated at an angle relative to the corrugated plates of the first layer from 20 to 90, wherein the vertical height of the first layer and/or the vertical height of the second layer is greater than 350 mm or greater than 400 mm.

The plant is used for producing oxygen by cryogenic air separation. The plant has a high-pressure column, a low-pressure column and a main condenser. An argon-elimination column is in fluid connection with an intermediate point of the low-pressure column and is connected to an argon-elimination column head condenser. An auxiliary column has a sump region, into which gas is introduced from the argon-elimination column head condenser. The head of the auxiliary column is connected to a return flow liquid line, in order to introduce a liquid stream from the high-pressure column or the head condenser. The liquid stream has an oxygen content which is at least equal to that of air. At least one part of the crude liquid oxygen from the sump of the high-pressure column is fed to the auxiliary column at a first intermediate point.

A distillation column system and a plant are for production of oxygen by cryogenic fractionation of air. The distillation column system has a high-pressure column and a low-pressure column, a main condenser, and an argon column with an argon column top condenser. The low-pressure column comprises an upper mass transfer region, a lower mass transfer region and a middle mass transfer region. The argon column top condenser is arranged within the low-pressure column between the upper and middle mass transfer regions and is configured as a forced-flow evaporator.

A method and apparatus for argon rejection and recovery in which argon is separated from air within a cryogenic air separation plant having a divided wall argon rejection column and condensed using an argon condenser disposed internally within the lower pressure column. The resulting argon stream is subsequently rejected or recovered and optionally purified within an integrated adsorbent based argon refining and purification subsystem to produce product grade argon.

A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.

A method and apparatus for increasing argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit and purified within an integrated, multi-stage pressure swing adsorption system to produce product grade argon with high argon recovery levels.

A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having an argon rejection column and a reflux type argon condenser disposed internally within the lower pressure column. An impure argon stream is subsequently recovered from the argon rejection column and purified within an integrated adsorbent based argon refining and purification subsystem to produce product grade argon. The waste stream from the adsorbent based argon refining and purification subsystem is recycled back to the argon rejection column so as to improve the argon recovery.

A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.