A high-temperature and high-pressure equipment and method for microscopic visual sulfur deposit seepage test is provided by the present disclosure, the equipment comprises an injection system, a high-temperature and high-pressure visual kettle, a pressure supply system, a data acquisition and analysis system, a fluid recovery system, and an injection branch pipe; the injection system comprises an ISCo micro-injection pump, an intermediate container, a thermostatic heating oven and a pressure meter; the intermediate container is arranged in the thermostatic heating oven, the ISCo micro-injection pump is connected to the intermediate container; the data acquisition and analysis system comprises a microscope, a high-brightness light source and a computer; the pressure supply system comprises an annular pressure tracking pump, a back pressure pump, a back pressure valve and a pressure gauge; the fluid recovery system comprises a wide neck flask with rubber stopper, a balance, a flowmeter and an exhaust gas absorber tank.

Determination of transport phenomena properties in porous media is one major objective of core analysis studies in petrophysics, reservoir engineering, and groundwater hydrology. Porosity measurement may be considered as a key factor to identify the hydraulic performance of a low permeable porous medium (e.g. rock or concrete). Additionally, the rate of absorption under pressure depends on the permeability, which is related to the connectivity between the existing pores within the porous structure. An alternative Gas Expansion Induced Water Intrusion Porosimetry (GEIWIP) method and apparatus is useful to measure the total porosity and pore size distribution, using a gas/water intrusion apparatus for water tight materials.

The present invention discloses a shale stress sensitivity testing device and method. The testing device comprises a support table. The left and right ends of the upper surface of the support table are respectively provided with a left side plate and a right side plate. The top of the left and right side plates are connected with the left and right ends of the top plate. The chucks of the clamps are capable of reciprocating motion in the horizontal direction and circular motion in the front-rear direction. The present invention can change the intensity and direction of the effective stress of the rock sample, and determine the permeability of the rock sample under different effective stresses, thus enabling comprehensive testing of the stress sensitivity of shale in different directions and enhancing the accuracy of shale stress sensitivity testing.

A system and method for high-throughput, high-resolution gas sorption screening are provided. An example system includes a sample chamber with a hermetic seal and a heat exchanger system. The heat exchanger system includes a heat exchanger disposed in the sample chamber, a coolant circulator fluidically coupled to the heat exchanger, and a sample plate comprising sample wells in contact with the cooling fluid from the coolant circulator. The system also includes a gas delivery system. The gas delivery system includes a gas source and a flow regulator. A temperature measurement system is configured to sense the temperature of the sample wells.

The invention relates to a method for determining a loading of a soot filter with soot particles from an exhaust gas mass flow of an internal combustion engine in a motor vehicle, a control device for an internal combustion engine having a soot filter, and a computer program product for carrying out the method. In the first step 100 of the method a characteristic curve for the relationship between the exhaust gas mass flow, exhaust gas temperature, ambient pressure, and pressure drop across the soot filter without loading is determined; in the second step 200 a second exhaust gas mass flow and a second pressure drop that occurs during loading of the soot filter are determined; in the third step 300, from the characteristic curve the first pressure drop is determined for which the first and second exhaust gas mass flows have the same value; in the fourth step 400 an estimated value for the loading of the soot filter is computed via a real-time parameter estimation, preferably by use of the gradient method, based on the previously determined parameters. The method allows a reliable determination of the instantaneous loading of a particulate filter, regardless of the type of measuring signals used in each case for characterizing the loading behavior of the soot filter.

A method includes determining a perforation tunnel geometry of a perforation tunnel in a solid sample, the perforation tunnel created by activating a shaped charge in proximity to the solid sample. The method also includes performing a first flow test on the solid sample and creating an analog aperture having an aperture geometry in a solid sample analog of the solid sample, wherein the aperture geometry and the perforation tunnel geometry satisfies a similarity threshold. The method also includes performing a second flow test on the solid sample analog and determining a shaped charge effect based on a comparison between a second flow test result and a first flow test result.

Systems and methods are disclosed for using downhole plasma discharge effects to determine porosity and/or permeability of formation material. In some embodiments, a method includes determining a concentration of at least one chemical reaction product in a drilling fluid that has interacted with a plasma discharge proximate formation material. A relation between arc and spark of the plasma discharge is determined based, at least in part, on the at least one chemical reaction product, and at least one of porosity and permeability of the formation material is determined based, at least in part, on the relation between arc and spark.

A coupling device for a mask test means is disclosed. Provided according to an embodiment of the present invention is a coupling device for a mask test means, comprising: a pressing member which can receive a first member of a mask test means on one side thereof and can move up and down; and a support member which can receive a second member of the mask test means on one side thereof and is disposed below the pressing member, wherein the support member includes a lower member having a perforation means for forming a perforation in a mask, and the pressing member includes an upper member into which at least a portion of the perforation means can be inserted.

The present invention provides a composite oxide that can achieve a high low-temperature output characteristic, a method for manufacturing the same, and a positive electrode active material in which the generation of soluble lithium is suppressed and a problem of gelation is not caused during the paste preparation. A positive electrode active material for non-aqueous electrolyte secondary batteries, including a lithium-metal composite oxide powder including a secondary particle configured by aggregating primary particles containing lithium, nickel, manganese, and cobalt, or a lithium-metal composite oxide powder including both the primary particles and the secondary particle. The secondary particle has a porous structure inside as a main inside structure, the slurry pH is 11.5 or less, the soluble lithium content rate is 0.5 [% by mass] or less, the specific surface area is 3.0 to 4.0 [m.sup.2/g], and the porosity is more than 50 to 80 [%].

The present invention provides a composite oxide that can achieve a high low-temperature output characteristic, a method for manufacturing the same, and a positive electrode active material in which the generation of soluble lithium is suppressed and a problem of gelation is not caused during the paste preparation. A positive electrode active material for non-aqueous electrolyte secondary batteries, including a lithium-metal composite oxide powder including a secondary particle configured by aggregating primary particles containing lithium, nickel, manganese, and cobalt, or a lithium-metal composite oxide powder including both the primary particles and the secondary particle. The secondary particle has a porous structure inside as a main inside structure, the slurry pH is 11.5 or less, the soluble lithium content rate is 0.5 [% by mass] or less, the specific surface area is 3.0 to 4.0 [m.sup.2/g], and the porosity is more than 50 to 80 [%].