An element analysis method is capable of maintaining accuracy of zero-point correction equivalent to that in the related art while shortening the time required for element analysis. The method includes heating a sample placed in a crucible in a heating furnace, and measuring an amount of an element contained in a gas discharged from the heating furnace by an analysis mechanism to analyze the element contained in the sample. The method includes: a blank measurement step of measuring the amount of the element contained in the gas discharged from the heating furnace when only the crucible is heated; and a step of setting an amount of zero-point correction based on a measurement value in a transient state region where the measurement value rises in blank data obtained in the blank measurement step.

In order to provide an elemental analysis device that includes an electrode having a housing recess where a crucible is housed during an elemental analysis, and that is capable of making only the part of a consumed electrode tip replaceable, an elemental analysis device including a first electrode and a second electrode between which a crucible MP containing a sample is nipped, and that heats the sample by applying a current between the first electrode and the second electrode, the first electrode includes: a first electrode main body that is provided with a housing recess where the crucible MP is housed; and a first electrode tip that is provided removably to the first electrode main body in such a manner that a part thereof is exposed inside the housing recess.

The present invention relates to a method of characterizing organic hydrocarbon compounds contained in a solid deposit of a geothermal plant, by measuring a quantity of organic hydrocarbon compounds released by a solid deposit sample during heating by pyrolysis according to a temperature sequence such that: from a temperature (T1) ranging between 50° C. and 120° C., the temperature of a rock sample is raised to a temperature (T2) ranging between 180° C. and 220° C. This temperature (T2) is then maintained for a predetermined duration. The temperature of the sample is raised to a temperature (T3) ranging between 330° C. and 370° C. This temperature (T3) is maintained for a predetermined duration. The temperature of the sample is thereafter raised to a temperature (T4) ranging between 630° C. and 670° C.

An open system pyrolysis of a first hydrocarbon source rock sample obtained from a natural system is performed within a pyrolysis chamber by maintaining the pyrolysis chamber at a substantially constant temperature. Hydrocarbons are recovered from the pyrolysis chamber released by the first hydrocarbon source rock sample. A thermo-vaporization is performed within the pyrolysis chamber on the pyrolyzed sample at a substantially constant temperature. A first hydrocarbon expulsion efficiency of hydrocarbon source rock is determined. A second hydrocarbon rock sample is ground to a grain size less than or equal to or less than 250 micrometers. A second pyrolysis is performed on the ground hydrocarbon source rock sample by maintaining the chamber at a substantially constant temperature. A second hydrocarbon expulsion efficiency of the hydrocarbon source rock in the natural system is determined. The first hydrocarbon expulsion efficiency is verified using the second hydrocarbon expulsion efficiency.

An open system pyrolysis of a first hydrocarbon source rock sample obtained from a natural system is performed within a pyrolysis chamber by maintaining the pyrolysis chamber at a substantially constant temperature. Hydrocarbons are recovered from the pyrolysis chamber released by the first hydrocarbon source rock sample. A thermo-vaporization is performed within the pyrolysis chamber on the pyrolyzed sample at a substantially constant temperature. A first hydrocarbon expulsion efficiency of hydrocarbon source rock is determined. A second hydrocarbon rock sample is ground to a grain size less than or equal to or less than 250 micrometers. A second pyrolysis is performed on the ground hydrocarbon source rock sample by maintaining the chamber at a substantially constant temperature. A second hydrocarbon expulsion efficiency of the hydrocarbon source rock in the natural system is determined. The first hydrocarbon expulsion efficiency is verified using the second hydrocarbon expulsion efficiency.

A hydrocarbon generation pyrolysis simulation experimental device for centrifugal continuous gas sampling of a hydrocarbon source rock, including a centrifugal turntable, a motor, a quartz sample tube, a heating set, a cooling set, a rotary joint mounted coaxially with a rotating shaft of the centrifugal turntable, a vacuum pump, and vacuum gas collecting pipes, wherein a sealing plug is arranged at an orifice of the quartz sample tube, a thermocouple and a first exhaust pipeline connected with an inlet of the rotary joint are mounted on the sealing plug, the rotary joint is communicated with a vacuum pump through a second exhaust pipeline, a plurality of vacuum gas collecting pipes are respectively communicated with the second exhaust pipeline through an electromagnetic valve, a vacuum pump switching valve is mounted on the second exhaust pipeline at an inlet end of the vacuum pump, and a control circuit board is mounted on the centrifugal turntable.

A device and a method for detecting cigarette fly ash by a gray-scale difference based on machine vision (MV) are provided. A manipulator holds a cigarette as a detection sample to simulate a human smoking action, and multiple groups of cameras track a simulated smoking process of the detection sample synchronously in real time. It is determined whether fly ash appears based on a gray-scale difference of burning ash columns, produced without being subjected to flicking, in acquired images. A fly ash area of the burning ash columns of the cigarette is calculated by an area with the gray-scale difference of the burning ash columns of the cigarette in two sequential images of the burning ash columns of the cigarette, and a fly ash amount is further determined. The detection of the amount of fine fly ash is converted into the detection of the gray-scale difference.

A device and a method for detecting cigarette fly ash by a gray-scale difference based on machine vision (MV) are provided. A manipulator holds a cigarette as a detection sample to simulate a human smoking action, and multiple groups of cameras track a simulated smoking process of the detection sample synchronously in real time. It is determined whether fly ash appears based on a gray-scale difference of burning ash columns, produced without being subjected to flicking, in acquired images. A fly ash area of the burning ash columns of the cigarette is calculated by an area with the gray-scale difference of the burning ash columns of the cigarette in two sequential images of the burning ash columns of the cigarette, and a fly ash amount is further determined. The detection of the amount of fine fly ash is converted into the detection of the gray-scale difference.

An elemental analysis device includes a heating furnace in which a test sample that is placed in a crucible is heated so that a sample gas is generated from the test sample, an inflow path through which a carrier gas is introduced into the heating furnace, an outflow path through which a mixture gas made up of the carrier gas and the sample gas is led out from the heating furnace, a dust filter that is provided on the outflow path, an analysis mechanism that is provided on the outflow path on a downstream side from the dust filter, and that detects one or a plurality of predetermined components contained in the mixture gas, and a cleaning gas supply mechanism that supplies cleaning gas to the dust filter in an opposite direction from a direction in which the mixture gas is flowing.

An apparatus for generating gas from a sample (battery) by pyrolysis of the sample in order to collect or analyze gas generated inside the sample due to the thermal behaviors of the sample. More specifically, provided is an apparatus wherein not only gas generated due to the thermal behaviors of a sample (battery) can be generated by heating the sample (battery itself), but also a series of processes provided to collect or analyze the generated gas can be automatically controlled.