A titration module includes a base, at least one titration unit, a contact angle measuring module, and a computing unit. The at least one titration unit is disposed above the base for titrating a globule onto a device under test. The contact angle measurement module is disposed above the base for measuring a first height and a first radius of the globule. The computing unit can calculate a second radius according to the first height and the first radius, and can calculate a contact angle of the globule according to the first height and the second radius. Also disclosed are a test apparatus, and a method for measuring titration contact angles.

An embodiment provides a method for measuring a characteristic of an aqueous sample, including: introducing the aqueous sample to a titration region and a reaction region of a measurement device, wherein the titration region comprises a pH electrode and a protonator electrode contacting a first portion of an aqueous sample, wherein the reaction region comprises a counter electrode contacting a second portion of the aqueous sample; placing an electrolyte reservoir in a state of electrical continuity with the titration region and the reaction region, wherein the electrolyte reservoir comprises a reference electrode, wherein the volume of the electrolyte reservoir comprises a large volume of an electrolyte; and determining a characteristic of the aqueous sample by measuring an electrochemical characteristic between the reference electrode and at least one of: the pH electrode and the counter electrode. Other aspects are described and claimed.

The present invention discloses a spectral-potentiometric-thermometric multi-dimensional titration analysis instrument, which comprises a spectral titration measurement device, a thermometric titration measurement device and a potentiometric titration measurement device which are arranged in parallel, meets the simultaneous measurement requirements of different analysis methods in chemical analysis, improves the measurement precision of different measurement methods, and effectively reduces the workload of separate experiments. The present invention further provides a usage method of the analysis instrument, provides analysis results of different angles and different characterization parameters for the change process of the material structure in the chemical reaction by conducting comparison analysis on data obtained using different measurement techniques, and effectively reduces the workload of titration analysis.

The present invention discloses a spectral-potentiometric-thermometric multi-dimensional titration analysis instrument, which comprises a spectral titration measurement device, a thermometric titration measurement device and a potentiometric titration measurement device which are arranged in parallel, meets the simultaneous measurement requirements of different analysis methods in chemical analysis, improves the measurement precision of different measurement methods, and effectively reduces the workload of separate experiments. The present invention further provides a usage method of the analysis instrument, provides analysis results of different angles and different characterization parameters for the change process of the material structure in the chemical reaction by conducting comparison analysis on data obtained using different measurement techniques, and effectively reduces the workload of titration analysis.

A first method for determining an amount of water in a sample includes the step of providing a reagent comprising: sulfur dioxide or a derivative thereof; a base; an optional hydrogen halide or hydrogen halide donor; a solvent; and a sulfonic acid; and the step of titrating the sample with the reagent. A second method for determining an amount of water in a sample includes the step of providing the aforementioned reagent, combining the sample with the reagent; and adding a source of iodine to the sample and/or the reagent. The reagent may alternatively consist essentially of sulfur dioxide or a derivative thereof; imidazole and/or a derivative thereof; an optional hydrogen halide or hydrogen halide donor; acetonitrile; methane sulfonic acid; and methanol and/or ethanol.

Disclosed are methods and systems for the use of titration-gas chromatography (TGC) to differentiate and quantify metallic substances (M.sup.0) and ionic metal (Mn.sup.+) in an anode material, such as in rechargeable-battery anodes of metal type (e.g., Li, Na, K, Mg, Ca, Fe, Zn, Al, etc.) or compound type (e.g., Li.sub.xC6, Li.sub.xSi, LixSn, etc) by using the proper titrant.

Disclosed are methods and systems for the use of titration-gas chromatography (TGC) to differentiate and quantify metallic substances (M.sup.0) and ionic metal (Mn.sup.+) in an anode material, such as in rechargeable-battery anodes of metal type (e.g., Li, Na, K, Mg, Ca, Fe, Zn, Al, etc.) or compound type (e.g., Li.sub.xC6, Li.sub.xSi, LixSn, etc) by using the proper titrant.

A titration system is disclosed for determining content of an analyte in a sample. The titration system comprises: a controller; a reaction vessel; a titration vessel and an indicator vessel in fluid communication with the reaction vessel; a spectroscopy unit; a sensor for outputting a signal to the controller based on a force exerted by the reaction vessel on the sensor. The controller executes a stored program to: (i) perform titration by delivering to the reaction vessel a first mass of a first fluid comprising the sample, a second mass of a second fluid comprising indicator, and a third mass of a third fluid comprising titrant; (ii) detect color change in the mixture in the reaction vessel based on a signal from the spectroscopy unit and stop titration; and (iii) calculate content of the analyte in the sample based on the first mass, the second mass, and the third mass.

A titration system is disclosed for determining content of an analyte in a sample. The titration system comprises: a controller; a reaction vessel; a titration vessel and an indicator vessel in fluid communication with the reaction vessel; a spectroscopy unit; a sensor for outputting a signal to the controller based on a force exerted by the reaction vessel on the sensor. The controller executes a stored program to: (i) perform titration by delivering to the reaction vessel a first mass of a first fluid comprising the sample, a second mass of a second fluid comprising indicator, and a third mass of a third fluid comprising titrant; (ii) detect color change in the mixture in the reaction vessel based on a signal from the spectroscopy unit and stop titration; and (iii) calculate content of the analyte in the sample based on the first mass, the second mass, and the third mass.

Provided herein are cellulose acetate tow bands having less than 0.1 wt. % titanium dioxide, wherein the content of titanium dioxide is measured by ashing and/or by titanium particle count density. Also provided herein is a method of measuring the titanium dioxide content of cellulose acetate tow by ashing. Also provided herein is a method for measuring the color of cellulose acetate tow.