G01N15/065

METHODS AND SYSTEMS FOR COLLECTING PARTICLES AND GASEOUS CHEMICALS

A method for collecting particles or gaseous chemicals is provided. The method includes providing liquid to a tube of a droplet generator, heating, with a heater of the droplet generator, the tube to provide vapor to a gas flow channel inside the tube, passing a gas flow containing the particles or gaseous chemicals through the gas flow channel inside the tube to obtain droplets including the particles or gaseous chemicals, and passing the droplets including the particles or gaseous chemicals to a wall of a collecting device such that the droplets including the particles or gaseous chemicals hit the wall. The temperature inside the gas flow channel is higher than a temperature inside the collecting device.

Volatility-resolved chemical characterization of airborne particles

A method and apparatus for evaluating the chemical composition of airborne particles by sequentially collecting and analyzing airborne particles in-situ. The method includes: collecting particles; enlarging the particles through water condensation; accelerating the enlarged particles onto a surface to collect enlarged particles; and analyzing the enlarged particles by: isolating the surface; passing a carrier gas over the surface; heating the surface to thermally desorb collected particles into the carrier gas; transporting this evolved vapor into detectors; and assaying the evolved vapor as a function of a desorption temperature. The apparatus includes: a sample flow inlet; a condensational growth tube; a collection and thermal desorption (CTD) cell; a carrier gas source; a heater coupled to the CTD; one or more gas detectors; and a controller configured to operate valves, the heater, the growth tube, and the CTD cell in at least an in-situ sequential collection mode and analysis mode.

PULSED DIFFUSION CONDENSATION PARTICLE COUNTER

A method and apparatus to create water vapor supersaturation and particulate counts from an air sample. The method and apparatus include introducing an air sample into a chamber connected to an optical detector and an outlet by pumping at the outlet. The method further includes passing air through the chamber and optical detector in a steady flow, and subsequently closing the inlet while continuing the pumping to expand the air sample and exhaust a portion of the air sample through the optical detector. The walls of the particle chamber are wetted with a fluid such as water, and one portion of the wall is warmer than the other portions such that there is some condensational growth prior to the expansion, and yet more condensational growth during the expansion. The cycles are repeated by continuously repeating the introducing, passing and closing.

PULSED CONDENSATION PARTICLE COUNTER

A method and apparatus to create water vapor supersaturation and particulate counts from an air sample. The method and apparatus include introducing an air sample into a chamber by passing a flow into the chamber through the inlet by pumping at the outlet. The method further includes closing the inlet while continuing the pumping to exhaust the air sample from the chamber through the outlet. The pumping is performed at a rate operable to reduce pressure inside the chamber such that the air sample in the central portion of the chamber cools, and water vapor from walls of the chamber has time to diffuse into the air sample in the chamber from the walls. The cycles are repeated by continuously repeating the introducing and closing. The walls of the chamber may be wet or dry.

Particle number counting device and particle number counting method
11187641 · 2021-11-30 · ·

The present invention reduces the effects from variations in the outside air pressure on particle number counting, and is provided with an exhaust gas processing unit that performs predetermined processing on exhaust gas, a particle number counting unit that counts a number of particles contained in exhaust gas that has passed through the exhaust gas processing unit, a fluid resistance element that is provided downstream from the particle number counting unit, a suction pump that is provided downstream from the fluid resistance element, a gas supply path that is connected to a flow path between the fluid resistance element and the suction pump, and supplies gas to a downstream side of the fluid resistance element, and a flow rate adjustment unit that is provided on the gas supply path, and adjusts a flow rate of the gas that is supplied to the downstream side of the fluid resistance element.

Compact condensation particle counter technology
11181459 · 2021-11-23 · ·

A particle vapor reactor (PVR) includes a reactor body with a fluid flow conduit having an inlet end and an outlet end, the crossection of the conduit having a circular geometry at the inlet end, a rectangular geometry at its midsection, and a circular geometry at its outlet end. The PVR conduit defines a saturator section and a condenser section. A compact condensation particle counter (CPC) including the reactor is also disclosed. The CPC also includes a sample inlet, a fluid inlet section, a heater section, and a detector section.

REDUCING FALSE COUNTS IN CONDENSATION PARTICLE COUNTERS
20210356375 · 2021-11-18 ·

Various embodiments include methods and apparatuses to reduce false-particle counts in a water-based condensation particle counter (CPC). In one embodiment, a cleanroom CPC has three parallel growth tube assemblies. A detector is coupled to an outlet of each of the three parallel growth tube assemblies, and is used to compare the particle concentrations measured from each of the three growth tube assemblies. An algorithm compares the counts from the three detectors and determines when the particles counted are real and when they are false counts. Any real particle event shows up in all three detectors, while false counts will only be detected by one detector. Statistics are used to determine at which particle count levels the measured counts are considered to be real versus false. Other methods and apparatuses are disclosed.

HIGH-TEMPERATURE CONDENSATION PARTICLE COUNTER
20210356374 · 2021-11-18 ·

Various embodiments include an exemplary design of a high-temperature condensation particle counter (HT-CPC) having particle-counting statistics that are greatly improved over prior art systems since the sample flow of the disclosed HT-CPC is at least eight times greater than the prior art systems. In one embodiment, the HT-CPC includes a saturator block to accept directly a sampled particle-laden gas flow, a condenser block located downstream and in fluid communication with the saturator block, an optics block located downstream and in fluid communication with the condenser block, and a makeup-flow block having a concentric-tube design located in fluid communication with and between the condenser block and the optics block. The makeup-flow block being configured to reduce volatile contents from re-nucleating in the optics block. Other designs and apparatuses are disclosed.

Condensation particle counter with flood protection

A condensation particle counter includes a saturation section, an aerosol inlet assigned to the saturation section, a condensation section, a measuring section for condensation particles, and an outlet section. The aerosol inlet allows a flow of an aerosol loaded with particles. Each of the condensation section, the measuring section and the outlet section are arranged downstream of the saturation section. A critical nozzle is arranged in the outlet section. The critical nozzle includes a critical nozzle inlet. A pump suctions the aerosol. An outlet line extends from the critical nozzle to the pump. A valve device is arranged in the outlet line between the critical nozzle and the pump. A pressure measuring device is arranged upstream of the critical nozzle inlet. The outlet line is entirely closed or partially closed by the valve device depending on a measurement value of the pressure measuring device.

Pulse counting coincidence correction based on count rate and measured live time

An approach for counting particles suspended in a flow of gas or liquid in instruments that direct the flow through an illuminated region. Pulses are detected when the signal is below a threshold amplitude and moves above the threshold amplitude. This movement above the threshold creates a dead time during which only one pulse is detected until the signal amplitude moves sufficiently below the threshold such that a subsequent particle creates a distinct pulse. After counting the number of pulses, and determining the measured live time that the signal is below the threshold value, an initial particle concentration is calculated, and the calculation corrected for coincidence by calculating an actual live time as a measured live time minus a constant multiplied by the number of distinctly counted pulses, where the constant has the units of time. From this, particle concentrations in a volume can be determined.