The present disclosure discloses a reciprocating rock fracture friction-seepage characteristic test device and method. The test device includes an X-axis shear system, a Y-axis stress loading system, a Z-axis stress loading system, a servo oil source system, 5 a pore pressure loading system, and a host. The X-axis shear system includes an X-axis EDC controller, an upper shear box, a lower shear box, an X-axis left hydraulic cylinder, an X-axis right hydraulic cylinder, an X-axis left pressure head, an X-axis right pressure head, an X-axis left pressure sensor, an X-axis right pressure sensor, an X-axis displacement sensor, and an X-axis 10 displacement sensor. The pore pressure loading system includes an air cylinder, a pressure gauge, a pressure reducing valve, a fluid inlet pipeline, a fluid outlet pipeline, and a flowmeter.

A standard sample for measuring rock porosity by helium method is disclosed, which includes a cylinder body open above and a cover body matching the cylinder body. The center of the cover body is provided with a vent hole. The cylinder body is filled and tamped with filled sand body so that theoretical porosity in the cylinder body is 5%-10%. The filled sand body includes mixed sand body and quartz cotton. The mixed sand body includes coarse-grained high-purity quartz sand, medium-grained high-purity quartz sand and fine-grained silicon micropowder. By mixing, filling and tamping high-purity quartz sand with different particle sizes, silicon micropowder and quartz cotton, the porosity and permeability of the standard sample are reduced, so that the standard sample is closer to the physical properties of the actual shale geological samples to verify the method or calibrate the instrument for measuring rock porosity with helium method.

The present invention relates to a multi-capillary force curve averaging method based on the overall virtual measurement of a plurality of samples. The method includes the following steps: 1, taking m types of rock samples, obtaining a capillary force-saturation curve, an apparent volume and a porosity of each sample; 2, inspecting the quality of the capillary force-saturation curve of each sample and preprocessing the end points of each curve; 3, calculating an averaged wet phase saturation corresponding to different capillary force values of the plurality of samples under the overall virtual measurement of a plurality of samples; and 4, denoting data points on a graph by using the wet phase saturation as the abscissa and capillary force as the ordinate, and finally connecting all data points smoothly to obtain the averaged capillary force curve. This method of the present invention is reliable in principle and easy to operate, can be directly operated on the capillary force curves, is also suitable for various types of samples with different physical properties in consideration of the influence of the numbers of reservoirs represented by samples, has a wide range of applications, and accurate and convenient calculation results, and is more consistent with actual working conditions.

The present invention discloses a device and method for measuring a horizontal/vertical permeability of a hydrate reservoir. The device includes a cooling water/saturated methane water tank, a water injection pump, a methane gas tank, a booster pump, an air compressor, a high-pressure gas tank, a back pressure valve, a gas tank, a data acquisition instrument, a constant-temperature water bath and a hydrate reservoir horizontal/vertical permeability measuring apparatus provided in the constant-temperature water bath, where the cooling water/saturated methane water tank is provided with a water circulation inlet and an intake line at an upper part and a water circulation outlet at the bottom; the intake line is provided thereon with an intake control gate valve; the bottom of the cooling water/saturated methane water tank is in communication with the water injection pump.

To separate porosity from surface roughness, length scales for pore size and surface roughness are identified. These length scales are determined from surface roughness measurements and confirmed via NMR pore body calculations and pore size capillary pressure measurements. A filter removes pore contribution to surface roughness measurements and delivers intrinsic surface roughness. Additional filters and methods determine the minimum magnification on which to base surface roughness calculation, based on size of the field of view and where measured surface roughness approaches intrinsic surface roughness as magnification increases but larger magnification increase sampling time and difficulty. Sample irregularities, such as saw marks, are also filtered out or determined to be too large to remove via filter and another area of measurement is located. With the pore corrected quantification of surface roughness, surface relaxivity and pore distribution can be calculated with greater accuracy.

Determination of transport phenomena properties in porous media is one major objective of core analysis studies in petrophysics, reservoir engineering, and groundwater hydrology. Porosity measurement may be considered as a key factor to identify the hydraulic performance of a low permeable porous medium (e.g. rock or concrete). Additionally, the rate of absorption under pressure depends on the permeability, which is related to the connectivity between the existing pores within the porous structure. An alternative Gas Expansion Induced Water Intrusion Porosimetry (GEIWIP) method and apparatus is useful to measure the total porosity and pore size distribution, using a gas/water intrusion apparatus for water tight materials.

The present invention discloses a shale stress sensitivity testing device and method. The testing device comprises a support table. The left and right ends of the upper surface of the support table are respectively provided with a left side plate and a right side plate. The top of the left and right side plates are connected with the left and right ends of the top plate. The chucks of the clamps are capable of reciprocating motion in the horizontal direction and circular motion in the front-rear direction. The present invention can change the intensity and direction of the effective stress of the rock sample, and determine the permeability of the rock sample under different effective stresses, thus enabling comprehensive testing of the stress sensitivity of shale in different directions and enhancing the accuracy of shale stress sensitivity testing.

A system and method for high-throughput, high-resolution gas sorption screening are provided. An example system includes a sample chamber with a hermetic seal and a heat exchanger system. The heat exchanger system includes a heat exchanger disposed in the sample chamber, a coolant circulator fluidically coupled to the heat exchanger, and a sample plate comprising sample wells in contact with the cooling fluid from the coolant circulator. The system also includes a gas delivery system. The gas delivery system includes a gas source and a flow regulator. A temperature measurement system is configured to sense the temperature of the sample wells.

The invention relates to a method for determining a loading of a soot filter with soot particles from an exhaust gas mass flow of an internal combustion engine in a motor vehicle, a control device for an internal combustion engine having a soot filter, and a computer program product for carrying out the method. In the first step 100 of the method a characteristic curve for the relationship between the exhaust gas mass flow, exhaust gas temperature, ambient pressure, and pressure drop across the soot filter without loading is determined; in the second step 200 a second exhaust gas mass flow and a second pressure drop that occurs during loading of the soot filter are determined; in the third step 300, from the characteristic curve the first pressure drop is determined for which the first and second exhaust gas mass flows have the same value; in the fourth step 400 an estimated value for the loading of the soot filter is computed via a real-time parameter estimation, preferably by use of the gradient method, based on the previously determined parameters. The method allows a reliable determination of the instantaneous loading of a particulate filter, regardless of the type of measuring signals used in each case for characterizing the loading behavior of the soot filter.

A coupling device for a mask test means is disclosed. Provided according to an embodiment of the present invention is a coupling device for a mask test means, comprising: a pressing member which can receive a first member of a mask test means on one side thereof and can move up and down; and a support member which can receive a second member of the mask test means on one side thereof and is disposed below the pressing member, wherein the support member includes a lower member having a perforation means for forming a perforation in a mask, and the pressing member includes an upper member into which at least a portion of the perforation means can be inserted.