G01N24/082

Method For The Non-Destructive Testing Of An Elastomer Cable Insulation Sheath, Device And Programme
20210262956 · 2021-08-26 · ·

The invention relates to a method for non-destructive testing of an insulating sheath (G) of a cable (CB) made of a material of elastomeric polymer. The invention is characterized by a step (E2) of measurement using proton nuclear magnetic resonance on the insulating sheath (G) in order to measure at least a first parameter (P1) characterizing the elastically active chains (A) of the macromolecular network of the elastomeric polymer, comprising the fraction (FCEA) of elastically active chains (A) of the network and/or the average molar mass (M.sub.c) of the elastically active chains (A), and by an assessment step (E3) including a comparison of the first parameter (P1) characterizing the elastically active chains (A) and/or of a second parameter (P2), having been determined from the first parameter (P1) characterizing the elastically active chains (A), with at least one prescribed assessment threshold (S) in order to determine that the cable (CB) is at the end of its life when the first parameter (P1) and/or the second parameter (P2) is/are below the prescribed assessment threshold.

NMR measurement method and apparatus
11067518 · 2021-07-20 · ·

A whole measurement process includes a plurality of step combinations. Each of the step combinations is composed of a solution-state measurement step and a solid-state measurement step. In the solution-state measurement step, solution-state NMR measurement is performed such that magnetization that is to be used in the solid-state measurement step remains. In the solid-state measurement step, solid-state NMR measurement is performed by using the magnetization that remains. No waiting time for recovering magnetization is provided between the solution-state measurement step and the solid-state measurement step. The solid-state measurement step may be performed earlier, and the solution-state measurement step may be performed later. Alternatively, the two steps may be performed simultaneously.

MINIATURE STOCHASTIC NUCLEAR MAGNETIC RESONANCE
20210231760 · 2021-07-29 ·

A nuclear magnet resonance (NMR) system probes samples using a stochastically pulsed radio-frequency magnetic field. The NMR system uses active shims to compensate for spatial inhomogeneity in the bias magnetic field applied by a small permanent magnet. The active shim, made of a flexible conductor, creates a magnetic field when current is passed through it. The magnetic field created by the active shim can compensate for a first, second or third order spherical harmonic spatial inhomogeneity. The NMR system may have an array of active shims, with each active shim compensating for a spherical harmonic spatial inhomogeneity. The array of active shims may be arranged within the NMR system so as to increase power efficiency. The NMR system can accommodate a standard NMR sample tube and can be used to measure nuclear spin density or acquire an NMR spectrum.

NMR-based non-invasive and quantitative food attribute measurement apparatus and method

A non-invasive NMR based apparatus for measuring a food attribute (moisture, sugar content) in food products comprises a magnetic chamber, an RF pulsing device attached to the magnetic chamber, a sensor receiver, and a data processing unit in communication with the sensor receiver. The pulsing device exposes the food ingredients/snacks to an RF field and produces an NMR response signal that is detected by the sensor receiver. The data processing unit quantitatively measures a food attribute of the food product based on the NMR response signal.

Method for Measuring Terephthalic Acid Content and Solvent for Use in Measurement
20210181131 · 2021-06-17 ·

In a first step, a sample liquid is fabricated by mixing a sample formed of a polyester or decomposition products of a polyester into a solvent. The solvent used here contains chloroform and 2,2,2-trifluoroethanol and has an organic base added thereto. The organic base is at least one of a primary amine, a secondary amine, a tertiary amine and a heterocyclic amine. In a second step, the amount of terephthalic acid in the sample liquid is measured through a nuclear magnetic resonance spectroscopy aiming at hydrogen atoms

Nuclear magnetic resonance gas isotherm technique to evaluate reservoir rock wettability

Nuclear magnetic resonance (NMR) gas isotherm techniques to evaluate wettability of porous media, such as hydrocarbon reservoir rock, can include constructing a NMR gas isotherm curve for a porous media sample gas adsorption under various pressures. A hydrophobic or hydrophilic nature of the porous media sample can be determined using the NMR gas isotherm curves. A wettability of the porous media sample can be determined based on the NMR gas isotherm curve. The wettability can be determined for porous media samples with different pore sizes. In the case of reservoir rock samples, the determined wettability can be used, among other things, to model the hydrocarbon reservoir that includes such rock samples, to simulate fluid flow through such reservoirs, or to model enhanced hydrocarbon recovery from such reservoirs.

Methods and systems for determining bulk density, porosity, and pore size distribution of subsurface formations

Herein methods and systems for determining matrix or grain density of a subsurface formation are described. This includes measuring in-air mass of a fluid-saturated sample of the subsurface formation, wherein the in-air mass comprises mass of matrix or grains of the sample, mass of a fluid surrounding the sample, and mass of the fluid inside the sample. The volume of the fluid inside the sample, V.sub.ϕ, and volume of the fluid surrounding the sample, V.sub.sur, are determined using nuclear magnetic resonance (NMR). The fluid-saturated sample can then be submerged in a predetermined volume of a weighing fluid and mass of the fluid-saturated sample without the surrounding fluid in the weighing fluid, m.sub.f is measured. Using the measured and determined values one can determine the volume of the sample without the surrounding fluid, V.sub.c, the bulk density of the fluid-saturated sample without the surrounding fluid, ρ.sub.b, the volume of the matrix, V.sub.m, and the matrix or grain density of the subsurface formation, ρ.sub.m.

Methods and systems for determining bulk density, porosity, and pore size distribution of subsurface formations

Herein methods and systems for determining matrix or grain density of a subsurface formation are described. This includes measuring in-air mass of a fluid-saturated sample of the subsurface formation, wherein the in-air mass comprises mass of matrix or grains of the sample, mass of a fluid surrounding the sample, and mass of the fluid inside the sample. The volume of the fluid inside the sample, V.sub.ϕ, and volume of the fluid surrounding the sample, V.sub.sur, are determined using nuclear magnetic resonance (NMR). The fluid-saturated sample can then be submerged in a predetermined volume of a weighing fluid and mass of the fluid-saturated sample without the surrounding fluid in the weighing fluid, m.sub.f is measured. Using the measured and determined values one can determine the volume of the sample without the surrounding fluid, V.sub.c, the bulk density of the fluid-saturated sample without the surrounding fluid, ρ.sub.b, the volume of the matrix, V.sub.m, and the matrix or grain density of the subsurface formation, ρ.sub.m.

SELECTIVE INFLOW CONTROL DEVICE USING NUCLEAR MAGNETIC RESONANCE MEASUREMENTS FOR HYDROCARBON PRODUCTION WITHOUT WATER

An apparatus for extracting a fluid from a formation includes an inflow control device (ICD) coupled to a production tubular disposed in a borehole penetrating the formation and configured to control flow into the production tubular and a nuclear magnetic resonance (NMR) front-end component assembly disposed in the borehole, the NMR front-end component assembly having a sensitive volume in a flow path leading to and/or coming through the ICD. The apparatus also includes a controller receiving input from an NMR electronics module coupled to the NMR front-end component assembly and providing output to the ICD based on the input from the NMR electronics module.

Online analysis in a gas oil separation plant (GOSP)

A gas oil separation plant (GOSP) and method for receiving crude oil from a wellhead and removing gas, water, and salt from the crude oil, and discharging export crude oil. The GOSP includes online analyzer instruments for performing online analysis of salt concentration in multiple streams in the GOSP. Based in part on the online analysis, the salt content in the export crude oil may be determined and the flowrate for wash water supplied to the desalter vessel may be specified.