Patent classifications
G01N31/168
VIAL-HANDLING MECHANISM FOR AN AUTOMATED KARL FISCHER TITRATION SYSTEM
A mechanism (10) for an automated Karl Fischer (KF) titration system (1) includes a support console (6), a first vertical guide rail element (11), solidly attached to the support console, and a carriage unit (12), slidably constrained to the first vertical guide rail element, allowing the carriage unit a first degree of linear vertical mobility relative to the support console. The carriage unit holds a vial lift unit (13) with a lift platform (14) for a sample vial (18). The carriage unit, in a downward movement phase, lowers the lift platform from a starting position into an oven cavity of the titration system. A subsequent upward movement phase raises the lift platform to the starting position. A second vertical guide rail element, solidly connected to the lift platform and slidably constrained to the carriage unit, enables a second degree of linear vertical mobility of the lift platform.
OVEN INSULATION ARRANGEMENT
An analytical device has an oven arrangement (1) with an oven (2), an insulation system, a ventilation system and a housing. The ventilation system has a first convection system that uses natural convection, arranged to keep the housing cool, as well as a second convection system that uses forced convection, arranged to reduce the temperature in the oven (2). In particular, the analytical device is a component of a Karl Fischer titration instrument.
Integrated sediment and water analysis device and method
Provided herein are methods and devices for determining water and sediment content in a hydrocarbon fluid sample. The methods and devices for determining water and sediment content in a hydrocarbon fluid sample include a Karl Fischer titration device and a titration vessel configured to implement a Karl Fischer titration and an ultrasonic particle detector configured to identify sediment in the hydrocarbon fluid sample.
OVEN FOR AN ANALYSIS SYSTEM, TITRATION SYSTEM AND TITRATION METHOD
The invention relates to an oven (1, 1) for an analytical system, in particular for a titration system and especially for a Karl Fischer titration system. The oven (1, 1) comprises a housing, an insulation system (2a, 2a, 2b, 2b, 2c, 2c) and an insert (3, 3) for a sample vessel. The insulation system (2a, 2a, 2b, 2b, 2c, 2c) is arranged at least partially around the insert (3, 3). At least one heating element is arranged between the insulation system (2a, 2a, 2b, 2b, 2c, 2c) and the insert (3, 3) and at least partially surrounding the insert (3, 3). The invention also relates to a titration system with such an oven (1, 1) and a titration method.
METHOD OF MEASURING QUANTITY OF MOISTURE IN ELECTRODE, METHOD OF MANUFACTURING ELECTRODE FOR LITHIUM-ION SECONDARY BATTERY, MOISTURE QUANTITY MEASURING APPARATUS, AND METHOD OF MEASURING MOISTURE QUANTITY
A method of measuring a quantity of moisture in an electrode includes at least three steps as follows: disposing an electrode, which is a measurement target sample, inside a container provided with a gas introduction pipe and a gas discharge pipe; heating the electrode by supplying inert gas heated to a predetermined temperature in advance to the inside of the container through the gas introduction pipe, and vaporizing moisture adsorbed to the electrode; and collecting the moisture vaporized from the electrode, together with the inert gas through the gas discharge pipe and determining the quantity of the collected moisture. In addition, a moisture quantity measuring apparatus includes a container that has a gas introduction pipe and a gas discharge pipe, a heating unit, and a moisture quantity measuring unit that collects moisture vaporized from a sample, through the gas discharge pipe and determines the quantity of collected moisture.
INTEGRATED SEDIMENT AND WATER ANALYSIS DEVICE AND METHOD
Provided herein are methods and devices for determining water and sediment content in a hydrocarbon fluid sample. The methods and devices for determining water and sediment content in a hydrocarbon fluid sample include a Karl Fischer titration device and a titration vessel configured to implement a Karl Fischer titration and an ultrasonic particle detector configured to identify sediment in the hydrocarbon fluid sample.
ONLINE AND OFFLINE MEASUREMENTS OF GLYCOLS STRENGTHS WITH ANALYSIS PROCEDURE
A method for measuring the purity of a glycol sample includes measuring the purity of the glycol sample via gas chromatography, measuring the purity of the glycol sample via evaporation, measuring the purity of the glycol sample via titration, and comparing the purity of the glycol sample from gas chromatography, evaporation, and titration to obtain an accurate purity. A system for measuring the purity of a glycol sample in a pipeline includes at least one type of testing equipment connected to the pipeline via at least one test line and an interfacial online data processor in communication with the at least one type of testing equipment. The at least one type of testing equipment includes a gas chromatography instrument, an evaporation instrument, and a titration instrument.
INSPECTION METHOD OF ELONGATED COATED SHEET
An inspection method of an elongated coated sheet including: (i) at a starting end position located at a position of a starting-end predetermined distance from a coating starting end, measuring a starting-end moisture amount and comparing the starting-end moisture amount with a starting-end specified value; (ii) at a terminal end position located at a position of a terminal-end predetermined distance from a coating terminal end, measuring a terminal-end moisture amount and comparing the terminal-end moisture amount with a terminal-end specified value; and (iii) when the starting-end moisture amount is smaller than the starting-end specified value and the terminal-end moisture amount is smaller than the terminal-end specified value, regarding the elongated coated sheet between the starting end position and the terminal end position as an acceptable product.
Method for diagnosing film degradation
An object of the present invention is to provide a novel method for diagnosing film degradation which can identify the degraded state of a film based on a resin more efficiently and reliably than ever. In order to attain this object, a method for diagnosing the degradation of a film based on a resin is adopted, the method comprising using the following analysis method A and/or analysis method B, which is a non-destructive analysis method: analysis method A: confirming the presence or absence of abnormality in the film by visual observation and olfactometry, and analysis method B: confirming the presence or absence of an acid anhydride and a sign of hydrolysis reaction as to the film by Fourier transform infrared spectroscopy analysis.