A microscopic observation system with a temperature-pressure-controllable sample cell and methods. The system can be configured to perform common optical microscopic observation and polarizing microscopic observation. The system is composed of a visual autoclave, a temperature control component, a rapid cooling component, a pressure control component and an optical imaging system, and can be configured to observe an evolution process of microstructures of polymer materials in specific atmosphere and rapid temperature and pressure changing environments in a scale of 1 m-1 cm. A novel characterization means for researching a condensed state evolution law of polymers in high-pressure environments, and also a new thought for deep reveal of the polymer crystallization mechanism and regulation of crystallization and phase separation behaviors of the polymer materials.

A liquid directing sample container includes a well. The well has sides and a floor. The sides having a non-circular profile having an interior angle that, at a target location within the well, is smaller than other interior angles of the profile to wick liquid towards the target location. The floor is sloped downward towards the target location.

A microscopic observation system with a temperature-pressure-controllable sample cell and methods. The system can be configured to perform common optical microscopic observation and polarizing microscopic observation. The system is composed of a visual autoclave, a temperature control component, a rapid cooling component, a pressure control component and an optical imaging system, and can be configured to observe an evolution process of microstructures of polymer materials in specific atmosphere and rapid temperature and pressure changing environments in a scale of 1 m-1 cm. A novel characterization means for researching a condensed state evolution law of polymers in high-pressure environments, and also a new thought for deep reveal of the polymer crystallization mechanism and regulation of crystallization and phase separation behaviors of the polymer materials.

A small angle laser scatterometer with a temperature-pressure-controllable sample cell and a characterization method, the scatterometer formed by sequentially arranging a laser source, an adjustable attenuator, a beam expanding lens, a polarizer, the temperature-pressure-controllable sample cell, an analyzer, a transmission-type projection screen and an image acquisition device. The temperature-pressure-controllable sample cell is composed of a visual autoclave, a temperature control component, a rapid cooling component and a pressure control component. An evolution process of microstructures of polymer materials in specific atmosphere and rapid temperature and pressure changing environments on a scale of 0.5 m to 10 m. Researching a condensed state evolution law of the polymer materials in high-pressure environments can provide a process solution for regulating crystallization and phase separation of the polymer materials and new thought for further and deep reveal of a polymer material crystallization mechanism.

A system and method for determining impurities in a beverage grade gas such as CO.sub.2 or N.sub.2 relies on a coupling of FTIR analysis and UV fluorescence detection. Conversion of reduced sulphur present in some impurities to SO.sub.2 can be conducted using a furnace. In some cases, CO.sub.2% also is determined.

A flow cell can comprise a high-pressure, fluidic, flow-through housing that encloses and auto-aligns a heavy-walled, internally reflective low-cost glass capillary for concentrating and amplifying laser-excited spectra. The containment housing that encloses the capillaries can optionally sustain operational pressures of at least 10,000 psi. The pressure housing can be fitted with transparent optical windows that can accommodate laser-safe injection and spectra collection. The flow-cell design can adaptably accommodate different optical sampling configurations such as transmissive (forward scattering), reflective (backward scattering), or multipass, combined scattering. The flow cell size is scalable (lengthwise) to accommodate different applications or installations such as benchtop (lab), permanent (industrial), and portable (field). With new, miniaturized spectrometers, the flow cell can optionally be configured for transport as a real-time, high-sensitivity gas-analysis sensor aboard compact aerial or otherwise mobile systems (e.g., drones) for remote or hazardous applications.

A flow cell device including a spherical optical element is disclosed. The spherical lens can be sealed to the body of the flow cell device in a manner that provides external optical access to a fluid in an analysis region of a flow path through the flow cell device. The seal can be provided by an elastomer, a polymer, or a deformable metal. The disposition of the spherical lens to the flow path enables in situ optical analysis of the fluid. An optical analysis device can be removably connected to the flow cell device to provide the optical analysis. In some embodiments the optical analysis device is a portable Raman spectrometer. The flow cell device can provide a supplementary interrogation interface, and/or an on board sensor device(s) to enable multivariate analysis and/or advanced triggering.

The present invention relates to a pressure vessel (1) having a pressure vessel wall (1a) which completely surrounds a reaction chamber (2) as a pressure space for the initiation and/or promotion of chemical and/or physical pressure reactions of a sample (P) to be heated which is accommodated in the reaction chamber (2), wherein the pressure vessel wall (1a) has an infrared-permeable high-pressure window (30) which extends away outward in a direction from the reaction chamber (2) and which is supported in the pressure vessel wall (1a) with respect to a pressure in the reaction chamber (2), wherein the pressure vessel (1) furthermore has an infrared to temperature sensor (40) which is situated directly opposite the high-pressure window (30), in order to measure the temperature of a sample (P), accommodated in the reaction chamber (2), during a pressure reaction through the high-pressure window (30).

A system and method for determining impurities in a beverage grade gas such as CO.sub.2 or N.sub.2 relies on a coupling of FTIR analysis and UV fluorescence detection. Conversion of reduced sulphur present in some impurities to SO.sub.2 can be conducted using a furnace. In some cases, CO.sub.2% also is determined.

A system is presented. The system includes an electromagnetic radiation source configured to generate a mode matched electromagnetic radiation that irradiates a gas mixture filled in a gas compartment at a determined pressure P bars, an intensity enhancement mechanism that internally reflects the mode-matched electromagnetic radiation a plurality of times to achieve an effective intensity E, of reflected electromagnetic radiation in a region of interest, that is N times an intensity of the mode-matched electromagnetic radiation, and a detection subsystem that analyses the gas-mixture based upon Raman Scattered photons emitted from the region of interest, wherein a product of the P and the N is at least 30.