A method of determining a peak intensity in an optical spectrum is described. The method includes producing a two-dimensional array of spectrum values by imaging the optical spectrum onto a detector array. An offset using an actual location and an expected location of a peak of an interpolated subarray is used to adjust an expected location of another peak that is within another two-dimensional subarray. Interpolated spectrum values are then used to produce a peak intensity value of the second peak.

A method of determining a peak intensity in an optical spectrum is described. The method includes producing a two-dimensional array of spectrum values by imaging the optical spectrum onto a detector array. An offset using an actual location and an expected location of a peak of an interpolated subarray is used to adjust an expected location of another peak that is within another two-dimensional subarray. Interpolated spectrum values are then used to produce a peak intensity value of the second peak.

A device and method is described for analysing the elemental composition of a liquid sample utilizing a combination of electrochemical pre-concentration followed by spectrochemical analysis of analytes in a single device. The device consists of two electrodes for the purpose of pre-concentration of the analyte ions by electrodeposition, a DC power supply/potentiostat/galvanostat, a high voltage power supply capable of creating an electrical discharge such as arc, spark, glow discharge or plasma, a spectrometer capable of recording a spectrum generated during such discharges as well as a pump(s) for pumping the analyte containing solution. Such a device is autonomous, field-deployable and capable of providing online analysis.

A device and method is described for analysing the elemental composition of a liquid sample utilizing a combination of electrochemical pre-concentration followed by spectrochemical analysis of analytes in a single device. The device consists of two electrodes for the purpose of pre-concentration of the analyte ions by electrodeposition, a DC power supply/potentiostat/galvanostat, a high voltage power supply capable of creating an electrical discharge such as arc, spark, glow discharge or plasma, a spectrometer capable of recording a spectrum generated during such discharges as well as a pump(s) for pumping the analyte containing solution. Such a device is autonomous, field-deployable and capable of providing online analysis.

There is provided a method for measuring a composition of a gas circulating through a plasma-based detector, the plasma-based detector having a discharge chamber defining an internal volume and having discharge electrodes configured to apply a plasma-generating field across the discharge chamber. The method includes ramping a voltage until it reaches a breakdown voltage to generate a plasma, detecting the presence of the plasma, determining a pressure based on the breakdown voltage upon detection of the presence of the plasma, operating the detector at an operation voltage greater than the breakdown voltage, performing measurement(s) on the plasma, generating a detector signal based the measurement(s) and compensating the detector signal based on the determined pressure to obtain a compensated detector signal, the compensated detector signal being representative of the composition of the gas. A plasma-based detector for measuring the composition of the gas is also provided.

There is provided a method for measuring a composition of a gas circulating through a plasma-based detector, the plasma-based detector having a discharge chamber defining an internal volume and having discharge electrodes configured to apply a plasma-generating field across the discharge chamber. The method includes ramping a voltage until it reaches a breakdown voltage to generate a plasma, detecting the presence of the plasma, determining a pressure based on the breakdown voltage upon detection of the presence of the plasma, operating the detector at an operation voltage greater than the breakdown voltage, performing measurement(s) on the plasma, generating a detector signal based the measurement(s) and compensating the detector signal based on the determined pressure to obtain a compensated detector signal, the compensated detector signal being representative of the composition of the gas. A plasma-based detector for measuring the composition of the gas is also provided.

An aspect of some embodiments of the present invention relates to a plasma chamber for containing a solution electrode glow discharge (SEGD) apparatus, the plasma chamber comprising a hollow body and a lens. The hollow body is configured to enclose a plasma generated between a solid electrode and a solution electrode, and includes at least one viewing port for letting light generated from the plasma leave the hollow body. The lens is disposed at or near the viewing port, the lens being configured to collect light from the plasma and direct the light onto a light receiving unit.

An aspect of some embodiments of the present invention relates to a plasma chamber for containing a solution electrode glow discharge (SEGD) apparatus, the plasma chamber comprising a hollow body and a lens. The hollow body is configured to enclose a plasma generated between a solid electrode and a solution electrode, and includes at least one viewing port for letting light generated from the plasma leave the hollow body. The lens is disposed at or near the viewing port, the lens being configured to collect light from the plasma and direct the light onto a light receiving unit.

The present invention relates to an apparatus for demolding and analyzing a direct analysis sample formed from a molten metal material contained within a sample chamber assembly, wherein the sample chamber assembly comprises at least a sample housing, a cover plate and closing means, comprising: a cabinet defining an interior and comprising at least one opening for the sample housing to enter the cabinet, and analyzing means located inside the cabinet for analyzing an analysis surface of the sample; demolding means adapted to remove at least the closing means to expose at least part of the analysis surface of the sample; and transporting means adapted to hold and transport the sample housing at least between a sample demolding position, where the closing means is removed by the demolding means, and a sample analysis position, where the analysis surface of the sample is analyzed by the analyzing means, and wherein the sample demolding position and the sample analysis position are different from each other. The invention also relates to a system and method for demolding and analyzing a direct analysis sample.

The present disclosure is for a tool and a method using or making the tool for detection of production or formation water in drilling fluid. The tool includes a sampling chamber to receive a bypass line from a flow line at a well site. The tool further includes spectroscopy components to perform spectroscopy of the drilling fluid bypassed from a flow line into the bypass line. Processing components are provided in the tool to process spectra from the spectroscopy of the drilling fluid and to generate data associated with at least identification formation or production water in the drilling fluid. The tool includes a communication module to transmit the data externally from the tool.