Patent classifications
G01N21/74
Method for evaluating the quality of steam-treated products
The present invention provides a method for evaluating the quality of steam-treated products, allowing easy, quick and precise evaluation of the quality of oxide films in steam-treated products such as black coated steel sheets. Specifically, the present invention provides a method for evaluating the quality of steam-treated products with a surface oxide film formed during steam treatment, wherein test pieces (100) are cut out from said steam-treated products to measure the amount of oxygen in said test pieces (100) as a basis for evaluating the brightness of the surface(s) of said test pieces and/or the thickness of the oxide film of said test pieces.
Method for Quantitative Analysis of Hydrogen in Porous Silica
A method for quantitative analysis of hydrogen gas generated due to the decomposition of SiOH (silanol) in porous silica, which is a support of a metallocene catalyst is provided. The analysis enables the measurement of the content of hydrogen present in trace amounts in silica by employing an inert gas fusion-infrared absorption (IGFIA) method under specific pressure and temperature conditions.
ATOMIC ABSORPTION SPECTROPHOTOMETER
An atomization unit has a tube-shaped furnace, and heats and atomizes a sample injected into the furnace. A light source unit emits light having a wavelength to be measured toward the atomization unit such that light passes through the furnace. An optical system transmits the light having the wavelength to be measured, of light passing through the furnace. A detection unit detects the light transmitted by the optical system. A light transmission plate is provided at a position in an optical path of the light passing through the furnace toward the detection unit, to obliquely cross an optical axis of the light. An image capturing unit is arranged outside the optical path, and captures an image inside the furnace by receiving light reflected by the light transmission plate, of the light passing through the furnace.
ATOMIC ABSORPTION SPECTROPHOTOMETER
An atomization unit has a tube-shaped furnace, and heats and atomizes a sample injected into the furnace. A light source unit emits light having a wavelength to be measured toward the atomization unit such that light passes through the furnace. An optical system transmits the light having the wavelength to be measured, of light passing through the furnace. A detection unit detects the light transmitted by the optical system. A light transmission plate is provided at a position in an optical path of the light passing through the furnace toward the detection unit, to obliquely cross an optical axis of the light. An image capturing unit is arranged outside the optical path, and captures an image inside the furnace by receiving light reflected by the light transmission plate, of the light passing through the furnace.
METHOD FOR EVALUATING THE QUALITY OF STEAM-TREATED PRODUCTS
The present invention provides a method for evaluating the quality of steam-treated products, allowing easy, quick and precise evaluation of the quality of oxide films in steam-treated products such as black coated steel sheets. Specifically, the present invention provides a method for evaluating the quality of steam-treated products with a surface oxide film formed during steam treatment, wherein test pieces (100) are cut out from said steam-treated products to measure the amount of oxygen in said test pieces (100) as a basis for evaluating the lightness of the surface(s) of said test pieces and/or the thickness of the oxide film of said test pieces.
Atomic absorption spectrophotometer
The atomic absorption spectrophotometer is provided with an atomization unit, a light source, a detector, an optical system, a camera, and a captured image data storage unit. The atomization unit has a tube-like furnace and atomizes the sample injected into the furnace by heating the sample. The light source emits light of a wavelength of a measurement target toward the atomization unit so that the light passes through the furnace. The detector detects the light passed through the furnace. The camera captures an image of an inside of the furnace before performing a measurement process in which a sample is atomized in the furnace and its absorbance is measured. The captured image data storage unit stores the captured image data obtained by capturing the image by the camera in association with the measurement data corresponding to the captured image data.
Atomic absorption spectrophotometer
The atomic absorption spectrophotometer is provided with an atomization unit, a light source, a detector, an optical system, a camera, and a captured image data storage unit. The atomization unit has a tube-like furnace and atomizes the sample injected into the furnace by heating the sample. The light source emits light of a wavelength of a measurement target toward the atomization unit so that the light passes through the furnace. The detector detects the light passed through the furnace. The camera captures an image of an inside of the furnace before performing a measurement process in which a sample is atomized in the furnace and its absorbance is measured. The captured image data storage unit stores the captured image data obtained by capturing the image by the camera in association with the measurement data corresponding to the captured image data.
TUBE FURNACE DEVICE FOR AN ATOMIZING FURNACE
The invention relates to a tube furnace device for an atomizing furnace and to an analyzing apparatus comprising an atomizing furnace and a tube furnace device, in particular for atomic absorption spectrometry, the tube furnace device comprising a sample carrier means (11) and a bearing means (12) for supporting and forming electrical contact with the sample carrier means, the sample carrier means having a receiving tube (16) forming a tubular receiving space (17) for receiving an analyte, the sample carrier means having two bearing protrusions on the receiving tube for forming a connection with the bearing means, the bearing protrusions extending perpendicularly, preferably orthogonally, in relation to a longitudinal axis of the receiving tube, wherein the tube furnace device has a contact pressure means (13) via which a contact pressure force (14) can be exerted on the bearing protrusions in the direction of a passant line (20) in relation to a circular cross section (21) of the receiving tube.
TUBE FURNACE DEVICE FOR AN ATOMIZING FURNACE
The invention relates to a tube furnace device for an atomizing furnace and to an analyzing apparatus comprising an atomizing furnace and a tube furnace device, in particular for atomic absorption spectrometry, the tube furnace device comprising a sample carrier means (11) and a bearing means (12) for supporting and forming electrical contact with the sample carrier means, the sample carrier means having a receiving tube (16) forming a tubular receiving space (17) for receiving an analyte, the sample carrier means having two bearing protrusions on the receiving tube for forming a connection with the bearing means, the bearing protrusions extending perpendicularly, preferably orthogonally, in relation to a longitudinal axis of the receiving tube, wherein the tube furnace device has a contact pressure means (13) via which a contact pressure force (14) can be exerted on the bearing protrusions in the direction of a passant line (20) in relation to a circular cross section (21) of the receiving tube.
HEATING CHAMBER, HEATING FURNACE, ANALYSIS DEVICE, AND METHOD FOR ANALYZING FOREIGN MATTER CONTENTS IN SAMPLES
A heating chamber (1) for a heating furnace is proposed, with which electrothermal vaporization of impurities from samples can be effected in order to be able to then analyze them spectrometrically. The heating chamber has a wall (3), a sample reception area (5), a nozzle area (7) and two electrical connection areas (9, 11). The heating chamber (1) is specially configured such that an electric current flows through the wall (3) in such a way that a heating capacity caused by it is higher in the nozzle area (7) than in the sample reception area (5). For example, the electrical connection areas (9, 11) may be arranged in a radial direction remoter from the longitudinal axis (8) than a part of the wall (3) surrounding the nozzle area (7), and the heating chamber (1) may be configured, for example by means of a locally constricted area (13), in such a way that the current between the two electrical connection areas (9, 11) is predominantly conducted radially inwards towards the part of the wall (3) surrounding the nozzle area (7). Advantageous heat distribution in the heating chamber (1) achievable thereby may have a positive effect on the analysis of sample impurities.