G01N30/8624

ULTRASMALL NANOPARTICLES AND METHODS OF MAKING, USING AND ANALYZING SAME

The present disclosure provides methods of analyzing and/or purifying inorganic nanoparticles that may be functionalized with one or more dye group. Analyzing and/or purifying the inorganic nanoparticles includes utilizing liquid chromatography, such as, for example, high performance liquid chromatography (HPLC). Methods of the present disclosure may be used to determine the location of one or more dye groups on and/or in the inorganic nanoparticles. The present disclosure also provides methods of making inorganic nanoparticles and compositions of inorganic nanoparticles.

Waveform data processing device and waveform data processing program
10371676 · 2019-08-06 · ·

A waveform data processing device 30 capable of accessing a storage device 40 for storing data on an observed waveform such as a chromatogram, information on a starting point and an ending point of a peak cluster consisting of a plurality of peaks close one another present on the observed waveform, and information on a position of each peak included in the peak cluster and a positive/negative direction of the each peak, includes baseline determination means for determining, based on the data and the information stored in the storage device 40, a shortest straight line or shortest line segments from the starting point of the peak cluster as a beginning point to the ending point of the peak cluster as a finishing point satisfying all following conditions, and determining the straight line or the line segments to be a baseline of the peak cluster: (1) in a section where positive peaks are contiguous, a baseline passes below the observed waveform, becoming a straight line or line segments convex downward; (2) in a section where negative peaks are contiguous, a baseline passes above the observed waveform, becoming a straight line or line segments convex upward; and (3) in a section where positive and negative peaks are contiguous, the shape of a baseline is not influenced by the observed waveform.

ORGANIC AMMONIUM SALTS WITH TRACEABILITY AND DETERGENT DISPERSANT PROPERTIES TO LIQUID FUELS AND PROCESSES FOR THEIR SYNTHESIS

The present invention is related to a process for obtaining organic ammonium salts (OAS) and their derivatives, supramolecular surfactants (SS), which simultaneously present the properties of traceability and detergents dispersant of organic scales. Organic ammonium salts (OAS) and their derivatives supramolecular surfactants (SS) have applications as differentiators, markers, or tracers in fuels derived from hydrocarbons; and also to disperse organic scales or inhibit the gums precipitation both in injectors and intake valves of automotive vehicle engines. Organic ammonium salts (OAS) are obtained through an acid-base reaction between a molecule from the azo family and an amine. Once the OAS is obtained, it reacts with an organic compound (OC) so that through non-covalent interactions, a self-assembly process occurs that gives rise to the SS. Said process is based on green chemistry, that is, in the absence of solvents. These OAS and SS are quantified through the analytical techniques of ultraviolet-visible (UV-VIS) and high-performance liquid chromatography (HPLC) through a calibration curve. Additionally, its performance as a gum-dispersing agent in a single-cylinder engine is evaluated.

DATA PROCESSING DEVICE AND DATA PROCESSING METHOD
20190113487 · 2019-04-18 · ·

When a peak in a chromatogram is automatically detected by an automatic waveform processing unit and a user thereafter performs a manual operation on the peak, a manual waveform processing unit changes peak information on the peak. A time difference calculation unit calculates an elution time difference between peaks of the same component in two pieces of analyzed data. A peak selection unit selects, for the target data, a peak of the same component as the peak in the analyzed data based on analysis dates and times, namely the sequence of generation dates and times of the pieces of chromatogram data. Based on the elution time difference and the analysis dates and times, a peak information reflection unit reflects the change, made in peak information on the peak in the analyzed data, in peak information on the peak selected in the target data.

IDENTIFICATION METHOD OF MATURITY OF ACACIA HONEY

The present disclosure relates to the technical field of food detection, in particular to an identification method of maturity of acacia honey. In the present disclosure, the identification method of maturity of acacia honey includes the following steps: detecting an acacia honey sample using turanose as a characteristic marker; where if the acacia honey sample to be identified has a turanose content of no less than 0.5%, it is determined that the acacia honey sample to be identified is mature acacia honey; if the acacia honey sample to be identified has a turanose content of no less than 0.3% but less than 0.5%, it is determined that the acacia honey sample to be identified is semi-immature acacia honey; and if the acacia honey sample to be identified has a turanose content of less than 0.3%, it is determined that the acacia honey sample to be identified is immature acacia honey.

METHODS AND APPARATUS FOR MEASURING GAS FLUX

Systems and methods for measuring turbulent gas flux using high-speed vertical wind speed measurements (e.g., on the order of 5-10 Hz or more frequently) and low-speed gas content measurements (e.g., on the order of 5 Hz or less frequently), without the need for the sophisticated and expensive high-speed hardware to separate gas samples (e.g., into accumulation bags) according to updrafts and downdrafts. A time series of high-speed vertical wind speed data is used as a guide to distinguish between updrafts and downdrafts. When vertical wind speed is upward (updraft), the low-speed gas content is recorded into a data structure in one location, or marked with one flag. When vertical wind speed is downward (downdraft), the low-speed gas content is recorded into a different location, or marked with a different flag. Eddy Accumulation or Relaxed Eddy Accumulation computations can be performed using the stored gas content data to determine gas flux.

TECHNIQUES FOR DETERMINING EQUILIBRATION AND STABILITY IN SCIENTIFIC INSTRUMENT SYSTEMS

A method of performing experiments on samples may include receiving criteria defining a starting state for performing an experiment in a system including a scientific instrument; determining whether the starting state is established in the system; and, responsive to the starting state being established, allowing the experiment, that analyzes a sample using the scientific instrument, to proceed. Determining whether the starting state is established may include automated monitoring of at least one parameter for at least one data channel, and determining whether all such parameters simultaneously meet associated conditions of the criteria for specified time periods. The method may include automatically monitoring the system and re-establishing the starting state prior to performing each of one or more subsequent experiments. The method may include automatically monitoring and establishing a second starting state prior to performing each of one or more additional experiments.

Liquid chromatography-mass spectrometry (LC-MS) methods for analyzing ampholyte lot variation

The disclosure relates to methods of characterizing ampholyte compositions suitable for downstream applications such as capillary isoelectric focusing using liquid-chromatography-mass spectrometry.

Sulfur-containing volatile organic compounds in cannabis

An edible composition, an aerosol composition, a flavor composition, a fragrance composition, or an inhalable composition includes an organosulfur compound such as prenyl mercaptan, 2-methylthiophene, 3-methylthiophene, dimethyl disulfide, diprenyl disulfide, 3-methyl-2-buten-1-yl thiolacetate, 3-methyl-1-[(3-methyl-2-buten-1-yl)sulfanyl]-2-butene, prenylmethylthiol (1-(methylsulfanyl)-3-methyl-2-butene), prenyl thioacetate, thiogeraniol, dimethyl sulfide, or a combination of any two or more thereof, and a primary terpene compound selected from the group consisting of myrcene, ?-caryophyllene, limonene, ?-pinene, ?-pinene, valencene, ocimene, terpinolene, or a combination of any two or more thereof.

Methods and apparatus for measuring gas flux

Systems and methods for measuring turbulent gas flux using high-speed vertical wind speed measurements (e.g., on the order of 5-10 Hz or more frequently) and low-speed gas content measurements (e.g., on the order of 5 Hz or less frequently), without the need for the sophisticated and expensive high-speed hardware to separate gas samples (e.g., into accumulation bags) according to updrafts and downdrafts. A time series of high-speed vertical wind speed data is used as a guide to distinguish between updrafts and downdrafts. When vertical wind speed is upward (updraft), the low-speed gas content is recorded into a data structure in one location, or marked with one flag. When vertical wind speed is downward (downdraft), the low-speed gas content is recorded into a different location, or marked with a different flag. Eddy Accumulation or Relaxed Eddy Accumulation computations can be performed using the stored gas content data to determine gas flux.