A self-healing method for fractured single crystal SiC nanowires. A hair in a Chinese brush pen of yellow weasel's hair moves and transfers nanowires, which are placed on an in-situ TEM mechanical microtest apparatus. An in-situ nanomechanical tension test is realized. The nanowires are loaded. Displacement is 0-200 nm. Fracture strength of the single crystal nanowires is 12-15 GPa. After the nanowires are fractured, unloading causes slight contact between the fractured end surfaces, electron beam is shut off, and self-healing of the nanowires is conducted in a vacuum chamber. Partial recrystallization is found at a fracture after self-healing through in-situ TEM representation. A fracture strength test is conducted again after self-healing. A fractured position after healing is the same as the position before healing. The fracture strength of the single crystal nanowires after self-healing is 1-2.5 GPa. The recovery ratio of the fracture strength is 10-20%.

A method of in-situ TEM nanoindentation for a damaged layer of silicon is disclosed. Wet etching and ion beam lithography are used for preparing a silicon wedge sample. An etched silicon wedge is thinned and trimmed by a focused ion beam; thinning uses ion beam of 30 kV: 50-80 nA, and trimming uses ion beam of 5 kV: 1-6 pA; and the top width of the silicon wedge is 80-100 nm. The sample is fixed on a sample holder of an in-situ TEM nanomechanical system by using a conductive silver adhesive. The sample is indented with a tip in the TEM, so that the thickness of the damaged layer of the sample is 2-200 nm; and an in-situ nanoindentation experiment is conducted on the damaged layer of the sample in the TEM.

A method for measuring micro-scale strength and residual strength of brittle rocks, including: performing micro-CT scanning on a target area; obtaining loading and unloading curves and an elastic modulus of the rock via micro indentation experiment; performing dimensionless analysis based on Buckinham's -theorem to obtain relation between the loading and unloading curves and elastic modulus, indentation depth, initial and residual strengths; reconstructing a grid model of micro rock matrix at the target area and indenter; performing micro indentation numerical simulation based on Mohr-Coulomb criterion to obtain loading and unloading curves under different strengths and residual strengths; fitting a formula between simulated work of the indenter and initial and residual strengths at h/R of 0.1 and 0.15; and substituting experimental values of the work into the formula to plotting curves of initial and residual strengths under two indentation depths, where coordinates of an intersection point represent micro-scale initial and residual strengths.

A rock sample is nano-indented from a surface of the rock sample to a specified depth less than a thickness of the rock sample. While nano-indenting, multiple depths from the surface to the specified depth and multiple loads applied to the sample are measured. From the multiple loads and the multiple depths, a change in load over a specified depth is determined, using which an energy associated with nano-indenting rock sample is determined. From a Scanning Electron Microscope (SEM) image of the nano-indented rock sample, an indentation volume is determined responsive to nano-indenting, and, using the volume, an energy density is determined. It is determined that the energy density associated with the rock sample is substantially equal to energy density of a portion of a subterranean zone in a hydrocarbon reservoir. In response, the physical properties of the rock sample are assigned to the portion of the subterranean zone.

Methods of using micro-specimens for testing an additive manufactured material or a part made from the additive manufactured material. The methods include testing small and large test specimens taken from an additive manufactured part and from a blank constructed from the additive manufactured material. Correction factors based on the test specimens are calculated and applied to a calculated material property of the additive manufactured material.

Methods of using micro-specimens for testing an additive manufactured material or a part made from the additive manufactured material. The methods include testing small and large test specimens taken from an additive manufactured part and from a blank constructed from the additive manufactured material. Correction factors based on the test specimens are calculated and applied to a calculated material property of the additive manufactured material.

A measuring device for detecting measuring signals during either a scanning across a surface to determine a surface profile or a penetration movement of an indenter into a surface of the specimen to determine hardness, and, scanning with sufficient force to determine the scratch resistance of the specimen is described. All of the measurements can be done on the same specimen without unmounting the specimen from a holder. A camera mounted to the same framework as the measuring device enables further documentation of the specimen being tested.

The present invention provides a self-healing method for fractured SiC amorphous nanowires. A goat hair in a Chinese brush pen of goat hair moves and transfers single crystal nanowires under an optical microscope. On an in-situ nanomechanical test system of a TEM, local single crystal nanowires are irradiated with an electron beam for conducting amorphization transformation. Amorphous length of a single crystal after transformation is 60-100 nm. A fracture strength test is conducted on the amorphous nanowires in the single crystal after transformation in the TEM; and fracture strength of the amorphous nanowires is 9-11 GPa. After the amorphous nanowires are fractured, unloading causes a slight contact between the fractured end surfaces; and self-healing of the nanowires is conducted after waiting for 16-25 min in a vacuum chamber of the TEM. Atom diffusion is found at a healed fracture through in-situ TEM representation; and recrystallization is found in the amorphous nanowires. The present invention provides a method for realizing self-healing for fractured SiC amorphous nanowires without external intervention.

The present invention relates to a test system and method capable of simultaneously carrying out a high-throughput test of mechanical properties for miniature specimens. The system comprises one workstation (17) and a plurality of specimen test modules (16) installed horizontally or vertically on a workbench (15), wherein the workstation (17) comprises an operation interface, a data processing unit and a load output unit; each specimen test module (16) comprises a drive unit (5), an interchangeable to clamp unit (8), a displacement sensor (2), and a load sensor (14); the workstation (17) controls the drive unit (5) of the specimen test module (16) and receives detection data of the displacement sensor (2) and the load sensor (14); each specimen test module (16) optionally performs mechanical property testing independently; and the workstation (17) is controls simultaneously started testing of a plurality of specimens (9). The present invention can achieve tensile, bending, compression bending, stress-rupture, relaxation, and fatigue strength tests on a plurality of specimens at the same time.

Nano-indentation test to determine mechanical properties of reservoir rock can be implemented as multi-stage or single-stage tests. An experimental nano-indentation test (multi-stage or single-stage) is performed on a solid sample. A numerical nano-indentation test (multi-stage or single-stage) is performed on a numerical model of the solid sample. One or more experimental force-displacement curves obtained in response to performing the experimental nano-indentation test and one or more numerical force-displacement curves obtained in response to performing the numerical test are compared. Multiple mechanical properties of the solid sample are determined based on a result of the comparing.