G01N2203/0286

Method for moving and transferring nanowires using tapered hair of diameter on micron range

The present invention provides a method for moving and transferring nanowires using tapered hair of diameter in micron range. The nanowires have a diameter of 60-150 nm. The tapered hair has a diameter of 1-100 m, a tip curvature radius of 0.8-3 m and a length of 4-10 mm. A plastic film on a copper grid used for a TEM is removed, the copper grid is reserved, and holes have a diameter of 50-100 m. The copper grid after ultrasonic cleaning gains the nanowires from the acetone liquid with ultrasonic dispersed nanowires. The copper grid with distributed nanowires and the tapered hair are respectively placed on mobile platforms of two different optical microscopes. Millimeter movement and micron movement of the tapered hair are realized, thereby realizing movement and transfer operation for the nanowires. The tip of the tapered hair is dipped in a small drop of conductive silver epoxy, and the conductive silver epoxy is respectively dropped on both ends of the nanowires; and the radius of the dropped conductive silver epoxy is 4-8 m. The present invention realizes a method for moving and transferring nanowires using tapered hair through the mobile platforms of the two optical microscopes.

MEMS-BASED NANOINDENTATION FORCE SENSOR WITH ELECTRO-THERMAL TIP HEATING
20200249254 · 2020-08-06 ·

A MEMS microforce sensor for high temperature nanoindentation is used for determining a mechanical property of a sample by sensing a deflection and measuring a force. The MEMS microforce sensor includes at least a cold movable body, a heatable movable body, a heating resistor and capacitor electrodes. The cold movable body and the heatable movable body are mechanically connected by at least one bridge and the capacitor electrodes measure a force applied on the sample by sensing the deflection of the cold movable body relative to the outer frame by a change of electrical capacitance.

DEVICE AND METHOD FOR DETERMINING MECHANICAL PROPERTIES OF NANOMATERIALS
20200240887 · 2020-07-30 ·

The invention relates to a device (10) for determining the mechanical properties of nanomaterials comprising a substrate (30) onto which a nanomaterial specimen (40) can be anchored, wherein said substrate (30) is mechanically connected to an actuator (20) on one side and to a sensor (50) on the opposite side, and wherein the substrate (30) is configured to generate a fracture line (32) in a pre-determined position which divides the substrate (30) into two parts (31,31), wherein a first part (31) is connected to the actuator (20) and a second part (31) is connected to a sensor (50), in order to allow a relative movement between the actuator (20) and the sensor (50).

Apparatus and methods of mechanical testing materials
10684202 · 2020-06-16 · ·

An apparatus and method to strength test porous ceramic honeycomb bodies. The apparatus includes an interlayer between at least one platen and a surface of the high porosity honeycomb body to be tested. The method includes disposing at least one interlayer between at least one platen and an end face of the body, applying a force to the high porosity ceramic honeycomb body and monitoring a result of applying the force. The interlayer comprises a surface weight of about 350 g/m.sup.2 and a thickness in a direction N between facing surfaces load platens of at least about 20 mm. Axial and radial localized stamping tests also strength test porous ceramic honeycomb bodies.

Measurement apparatus, test method, and physical property evaluation program for indentation creep test, and recording medium recording physical property evaluation program

A measurement apparatus for carrying out an indentation creep test on a specimen, including a measurement control apparatus that includes a load measurement device, a constant-load compression device configured to compress a tip of a transparent indenter to a surface of the specimen, and an image capturing device configured to optically capture an image including a contact area portion which is a part of the specimen to which the load is applied by the constant-load compression device. The apparatus also includes an information processing apparatus that includes an image analysis unit configured to analyze a contact area, and a physical property value calculation unit. The physical property value calculation unit conducts linear regression with respect to a plot of a logarithmic value of the contact stress and a logarithmic value of the contact strain rate so as to determine a creep index n and creep constant k.

SYSTEM AND METHOD FOR DETERMINATION OF VISCOELASTIC PROPERTIES FROM GIVEN TIME-DEPENDENT PENETRATION OF A TEST LIQUID CREEPING INSIDE A CHANNEL
20200158612 · 2020-05-21 · ·

Disclosed is a system and method for determination of the viscoelastic properties of a viscoelastic substance based on the type of non-mechanical forces which drive the viscoelastic substance inside a channel. These forces may comprise capillary, gravitational, electric, magnetic, or any other type where neither a pump nor any relative velocity between solid surfaces is needed to induce the transport of fluid medium. As a result, the design of the system remains simple, and the system is capable of yielding results devoid of noise produced by mechanical forcing. The present disclosure a general analysis describing extraction of viscoelastic properties by observing flow-systems driven by any non-mechanical means, including capillary force and electro-osmotic force. Such time-dependent penetration depth may be recorded by optical, electrical or mechanical means and may further include the use of a computing device.

NANO-INDENTATION TESTS TO CHARACTERIZE HYDRAULIC FRACTURES

A rock sample is nano-indented from a surface of the rock sample to a specified depth less than a thickness of the rock sample. While nano-indenting, multiple depths from the surface to the specified depth and multiple loads applied to the sample are measured. From the multiple loads and the multiple depths, a change in load over a specified depth is determined, using which an energy associated with nano-indenting rock sample is determined. From a Scanning Electron Microscope (SEM) image of the nano-indented rock sample, an indentation volume is determined responsive to nano-indenting, and, using the volume, an energy density is determined. It is determined that the energy density associated with the rock sample is substantially equal to energy density of a portion of a subterranean zone in a hydrocarbon reservoir. In response, the physical properties of the rock sample are assigned to the portion of the subterranean zone.

Active mechanical-environmental-thermal MEMS device for nanoscale characterization

A microelectromechanical system (MEMS) device can be used for quantitative mechanical testing of materials within a controlled (chemical and temperature) environment, with the ability for electrochemical control to the specimen, that is coupled with a complimentary in-situ characterization technique.

DEVICE FOR MECHANICALLY CHARACTERIZING AN ELEMENT OF INTEREST SUCH AS AN OOCYTE
20200131464 · 2020-04-30 ·

Disclosed is a device for mechanically characterizing an element of interest, for example an oocyte. The mechanical characterization device includes: a support receiving a container suitable for containing a liquid medium; a holder for holding the element of interest; an indenting member; a magnet for generating a magnetic field in which the indenting member is intended to move and which participates in suspending the indenting member with an unstable horizontal direction oriented coaxially to the longitudinal axis; a controller to control the magnet to maneuver the indenting member in translation along the unstable horizontal direction; and a component for determining the mechanical characteristics of the element of interest.

TEM ELECTROMECHANICAL IN-SITU TESTING METHOD OF ONE-DIMENSIONAL MATERIALS
20200132574 · 2020-04-30 ·

A TEM electromechanical in-situ testing method of one-dimensional materials is provided. A multi-function sample stage which can compress, buckle and bend samples is designed and manufactured. A carbon film on a TEM grid of Cu is eliminated, and the TEM grid of Cu is cut in half through the center of the circle. The samples are dispersed ultrasonically in alcohol and dropped on the edge of the semicircular grid of Cu with a pipette. A single sample is fixed on the edge of a substrate of the sample stage with conductive silver epoxy by using a micromechanical device under an optical microscope, and conductive silver paint is applied to the surface of the substrate of the sample stage; and an electromechanical in-situ testing is conducted in a TEM. This provides a simple and efficient sample preparation and testing method for a TEM electromechanical in-situ observing experiment.